镍基催化剂上顺酐液相催化加氢制备γ-丁内酯

研究了负载型镍催化剂对顺酐加氢制备γ-丁内酯的催化性能,考察了镍含量、载体、助剂以及反应条件的影响,并对催化剂进行了XRD、TPR和BET表征.结果表明,20%Ni/活性炭催化剂对该反应具有很高的活性和选择性.钼及钛等过渡金属助剂的添加有利于γ-丁内酯的生成.20%Ni-Mo/活性炭催化剂在180℃、6.0MPa氢压力下,γ-丁内酯收率达97.6%.     

纳豆制备过程中大豆异黄酮的转化条件

使用日本古法制备纳豆,从纳豆中分离筛选出高活性的纳豆菌为实验菌株。研究了纳豆制备过程中大豆异黄酮的转化情况,发酵液中的大豆异黄酮在大豆异黄酮糖苷酶的水解作用下水解掉侧链糖基,转化为活性更高的大豆异黄酮苷元。根据薄层层析法确定了大豆异黄酮转化为大豆异黄酮苷元的最佳培养条件:培养温度为37℃,培养时间2 d,pH 7.0,含水质量分数60%。发酵液中大部分的大豆异黄酮苷转化为大豆异黄酮苷元,从而得到更利于人体吸收的大豆异黄酮苷含量较高的纳豆制品。     

移动容迟传感网络拓扑覆盖建模与统计特征*

移动容迟传感网络的拓扑覆盖研究对于相关工程系统设计具有重要意义。针对当前研究没有很好地刻画区域动态覆盖特征的问题,提出基于排队网络的建模方法。进而利用随机几何学和排队论方法,以定理形式提出关于二维平面上区域覆盖的首达时间、覆盖度分布等统计特征的理论结果。结合典型移动场景,仿真验证了上述结果的合理性和应用价值。     

基于Kubelka-Munk理论光谱反射比重建算法的研究

由于常规的K/S空间的光谱反射比重建算法不能满足高精度重建光谱反射比的需求,因此基于Kubelka-Munk理论的光谱反射比重建算法被提出来.本文的重点是提出应用Kubelka-Munk理论对物体表面的光谱反射比进行重建,并针对该算法进行数学上的推导.     

Effects of chromium on the corrosion and electrochemical behaviors of ultra high strength steels

The effects of chromium on the corrosion and the electrochemical behaviors of ultra high strength steels were studied by the salt spray test and electrochemical methods. The results show that ultra high strength steels remain martensite structures and have anodic dissolu-tion characteristic with an increase of chromium content There is no typical passive region on the polarization curves of an ultra high strength stainless steel, AerMet 100 steel, and 300M steel However, chromium improves the corrosion resistance of the stainless steel re-markably. It has the slowest corrosion rate in the salt spray test, one order of magnitude less than that of AerMet 100 and 300M steels. With the increase of chromium content, the polarization resistance becomes larger, the corrosion potential shifts towards the positive direction with a value of 545 mV, and the corrosion current density decreases in electrochemical measures in 3.5wr% NaCl solutions. Because of the higher content of chromium, the ultra high strength stainless steel has a better corrosion resistance than AerMet 100 and 300M steels.     

Hydrogen induced cracking of X80 pipeline steel

The hydrogen-induced cracking (HIC) behavior of X80 pipeline steel was studied by means of electrochemical charging, hydrogen permeation tests, tension test, and scanning electron microscopy (SEM). The experimental results indicate that the increase of charging time and charging current density or the decrease of the solution pH value leads to an increase of the hydrogen content in X80 steel, which plays a key role in the initiation and propagation of HIC. It is found that the majority of macro-inclusions w...     

基于wordNet的类别可拓展网页分类系统

基于文本写作常采用一个意思由多个不同写法的单词来表述,研究词义文本分类法被用来替代使用关键词分类算法以提高分类准确率.分析wordNet内Synset架构,认为一个兼顾词义以及词义间关系的词义文本分类系统可应用到网页分类中.该系统同时注意到固定的文本类别结构以及结构内不断增长的文件数目间的区别,加入了基于类别信息聚类方法的类别拓展的功能.仿真实验证明,该分类系统与现有的基于语义的分类系统相比,在分类准确度性能上能提高13%.基于类别信息类聚的文本拓展功能与采用基于相似度的类聚方法的系统相比获得了一个质量更高的新增类别.     

可编程控制器对多种物质混合的控制

可编程控制器广泛应用领域中对多种物质混合的控制。以两种液体混合装置的控制为例,分析了控制原理和控制过程以及调试方法,从而总结了可编程控制器灵活性和通用性强,编程语言简单易学,PLC与外部设备的连接简单、使用方便,PLC控制系统的设计、调试周期短,PLC体积小、重量轻、价格低、易于实现机电一体化,抗干扰能力强、可靠性高,PLC的功能强、功能的扩展能力强等特点。     

Corrosion behavior and mechanism of the automotive hot-dip galvanized steel with alkaline mud adhesion

The corrosion behavior and mechanism of hot-dip galvanized steel and interstitial-free (IF) substrate with alkaline mud adhesion were investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), electrochemical impedance spectroscopy (EIS), and linear polarization. The results show that non-uniform corrosion occurs on the galvanized steel and IF substrate during 250 h with the mud adhesion. The corrosion products on the galvanized steel are very loose and porous, which are mainly ZnO, Zn5(OH...     

I386到Alpha动态二进制翻译中的代码缓存管理优化

动态二进制翻译是跨平台软件移植的最重要手段之一,如何对其进行优化,提高翻译效率一直是研究的热点。文章对I386到Alpha平台的动态二进制翻译进行了研究,提出了一种较好的翻译缓存管理策略,在FIFO的基础上将翻译缓存划分为两级进行管理。以QEMU动态二进制翻译器为实验平台进行测试,结果表明,采用此方法可以提升翻译速度约3%。