Waste Eggshell-Derived Calcium Oxide and Nanohydroxyapatite Biomaterials for the Preparation of LLDPE Polymer Nanocomposite and Their Thermomechanical Study

Waste eggshells were utilized to make calcium oxide (E-CaO) and hydroxyapatite (E-HAP). E-CaO obtained by heat treatment to eggshells was utilized for the synthesis of E-HAP. Melt compounding of E-CaO/E-HAP was performed with linear low-density polyethylene (LLDPE) on a Brabender Plastograph and ground the obtained formulation for injection molding. Addition of E-CaO/E-HAP in the LLDPE significantly enhanced the flame retardant ability and thermal stability of resultant composites. In the comparative study, E-HAP nanopowder-containing polymer composite showed increment in thermal and mechanical properties than the composite prepared using E-CaO.     

Frequency regularization of a linked wind–diesel system using dual structure fuzzy with ultra-capacitor

Microgrids (μ-grids) are gaining increased interest around the world for supplying cheap and clean energy. In this paper, a μ-grid comprising a wind turbine generator (WTG) and diesel generator (DG) is considered. It is one of most practical and demanding systems suitable for the present energy crisis in isolated or rural areas. However, wind energy is intermittent in nature while load demand changes frequently. Therefore, a µ-grid can experience large frequency and power fluctuations. The speed governor of the DG tries to minimize the frequency and power deviations in µ-grid though its operation is slow and cannot adequately minimize system deviations. The paper proposes a novel arrangement based on a dual structured fuzzy (DSF) whose structure changes according to the switching limit with a reduced rule base. It has the capability to switch between proportional and integral actions and hence improves the frequency regularization of the μ-grid. The proposed strategy is tested in a μ-grid and the results considering step load alteration, load alteration at different instants of time, nonstop changing load request are compared with some of the well published methods to validate the effectiveness and simplicity of the present design. In addition, it shows that ultra-capacitor establishment in a μ-grid has a positive impact in minimizing system deviations with DSF for the studied cases.     

An experimental investigation of the optimum geometry for the cold end orifice of a vortex tube

A vortex tube is a simple mechanical device, which splits a compressed gas stream into a cold and hot stream without any chemical reactions or external energy supply. This paper presents the results of a series of experiments focusing on various geometries of the “cold end side” for different inlet pressures and cold fractions. Specifically, the tests were conducted using different cold end orifice diameters.Energy separation and energy flux separation efficiencies are defined and used to recover characteristic properties of the vortex tube. These are used to show an appropriate scale to non-dimensionalize the energy separation effect. The experimental results indicate that there is an optimum diameter of cold end orifice for achieving maximum energy separation. The results also show that the maximum value of energy separation was always reachable at a 60% cold fraction irrespective of the orifice diameter and the inlet pressure. The results are compared with the previous studies on internal flow structure, and optimal operating parameters are shown to be consistent with a matching of orifice size with the secondary circulation being observed.     

Application of electromagnetic impact technique for welding copper-to-stainless steel sheets

The ability to manufacture a product using different metal combinations greatly increases flexibility in design and production. Joining of dissimilar metal combinations like Copper-to-Stainless Steel (Cu-to-SS) is, however, a challenging task owing to the large differences in physical and chemical properties. The application of electromagnetic (EM) impact technique is demonstrated for welding copper (Cu) to stainless steel (SS) sheets. The welding Cu-to-SS is accomplished by using Al drivers to accelerate Cu and SS work sheets. The tensile shear strength test and the metallographic studies are carried out for Cu-to-SS EM welds.     

Comparison of deformation induced precipitation behaviour in Alloy 718 under two microstructural conditions

Alloy 718 samples under two initial microstructural conditions, viz., solution annealed to form only γ phase (ST) and aged to precipitate only δ particles (DELTA), were deformed in tension till fracture in the temperatures range from 200°C–700°C. From the comparison of the evolved microstructure of deformed and undeformed specimens that have been subjected to similar thermal history, deformation induced precipitation could be identified. Deformation in the range of 550°C to 650°C promoted the precipitation of γ′ and γ″ phases in both structures. In case of DELTA alloy, the γ′ precipitation was found to precede the γ′ phase precipitation while no such preference for precipitation could be identified in ST specimens. This difference in the precipitation behaviour and the sequence of precipitation has been explained on the basis of the relative concentration of solutes in the matrix of the starting microstructures of ST and DELTA specimens.     

From data to diagnosis and control using generalized orthonormal basis filters. Part I: Development of state observers

This work is aimed at the development of a state observer (steady state Kalman filter) for a multivariable system with unknown time delays, which is subjected to unmeasured disturbances. To design such a filter, we explore the feasibility of capturing system dynamics using generalized orthonormal basis filters (GOBF). A two step identification procedure is proposed by exploiting the fact that the GOBF based models have output error structure. The deterministic component of the model is identified in the first step and used to compute a residual signal. In the second step, a filter that whitens the residuals is estimated using GOBF and combined with the deterministic component. A minimal order state realization of the innovation form of the state model is then generated from this high order model using realization based sub-space based state space (4SID) identification algorithm. When time delays are not known a-priori, the similarity between GOBF and Pade approximation is used to estimates time delay matrix directly from multivariate data. The efficacy of the proposed modeling technique is demonstrated by carrying out simulation studies on the benchmark Shell control problem and experimental evaluation on a stirred tank heater (STH) system. From the analysis of simulation and experimental results, it can be inferred that the proposed approach produces fairly accurate estimates of the time delay matrix and the deterministic and stochastic components of the dynamic model.     

Classification of melanoma using tree structured wavelet transforms

This paper presents a wavelet transform based tree structure model developed and evaluated for the classification of skin lesion images into melanoma and dysplastic nevus. The tree structure model utilizes a semantic representation of the spatial-frequency information contained in the skin lesion images including textural information. Results show that the presented method is effective in discriminating melanoma from dysplastic nevus. The results are also compared with those obtained using another method of developing tree structures utilizing the maximum channel energy criteria with a fixed energy ratio threshold.     

Tropospheric ozone variability over the Indian coastline and adjacent land and sea

A tropospheric ozone variability study is carried out to investigate the spatial and temporal distribution over the coastline of the Indian peninsula and adjacent land and sea using NASA Langley Tropospheric Ozone Residual data set for the period 1979–2005. A strong seasonal cycle has been observed with large variation (～ 55%) over the upper eastern coast, followed by the upper and lower western coast, compared to the lower eastern coast (～ 33%). A negative gradient in ozone concentration is observed along eastern and western coasts during summer (slope ～ –0.78 and –0.65) and a positive gradient (slope ～ 0.16 and 0.21) during winter. The same is observed over the adjacent land and sea along the coastline with slight variation. This change in gradient can be attributed to the anthropogenic emission of precursor gases that reinforce localized photochemical production of ozone. In addition, topography, transport, seasonality of emission of precursor gases and the solar insolation cycle play a vital role.     

Review:Mg and Its Alloy——Scope, Future Perspectives and Recent Advancements in Welding and Processing

镁/镁合金焊接与加工的最新进展与未来展望

Sachin Kumar,武传松

（山东大学 材料科学与工程学院,济南 250061）

中文说明：

该文非常详细地综述了镁及镁合金的生产、加工及焊接的研究现状。尤其是在镁合金焊接部分,作者比较详细地阐述了熔化焊、激光焊、固相焊及钎焊等方法在镁合金焊接中的研究现状、存在问题与发展动向。该文对于镁合金焊接研究人员具有重要的参考价值。

关键词：镁;镁合金;加工;焊接;连接;最新进展