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81.
M. Saeed Abaee Soodabeh Forghani Mohammad M. Mojtahedi Klaus Harms 《Journal of Sulfur Chemistry》2016,37(6):683-691
A facile procedure is developed for one-pot synthesis of a new group of dicyanoanilines. Tetrahydro-4H-thiopyran-4-one, 1, undergoes a pseudo four-component reaction with various aldehydes bearing different groups and two equivalents of malononitrile in aqueous media in the presence of triethylamine (Et3N). As a result, novel thiopyran-fused dicyanoanilines 4 are formed efficiently in the reaction mixtures in 90–97% yield within 9–12?h mixing at 40°C. Due to the polarity of the medium, products precipitate in the mixture spontaneously allowing for easy purification by recrystallization avoiding cumbersome chromatographic separations. Characterization of the products was performed by spectroscopic methods and, in one case, was further supported by X-ray crystallographic experiments. 相似文献
82.
Mohammadi-Asl Saeed Nourinia Javad Ghobadi Changiz Majidzadeh Maryam Mostafapour Ehsan Haghshenas Alireza 《Wireless Personal Communications》2017,97(2):2131-2144
Wireless Personal Communications - A novel design of double-layer dual-band circularly polarized array antennas (DDCPAAs) is presented in this paper. First, a DDCP single antenna is introduced as... 相似文献
83.
To speed up data‐intensive programs, two complementary techniques, namely nested loops parallelization and data locality optimization, should be considered. Effective parallelization techniques distribute the computation and necessary data across different processors, whereas data locality places data on the same processor. Therefore, locality and parallelization may demand different loop transformations. As such, an integrated approach that combines these two can generate much better results than each individual approach. This paper proposes a unified approach that integrates these two techniques to obtain an appropriate loop transformation. Applying this transformation results in coarse grain parallelism through exploiting the largest possible groups of outer permutable loops in addition to data locality through dependence satisfaction at inner loops. These groups can be further tiled to improve data locality through exploiting data reuse in multiple dimensions. 相似文献
84.
Muhammad Saeed Ji-Yang Yu Aniseh Ahmed Atef Abdalla Xian-Ping Zhong Mahmood Ahmad Ghazanfar 《核技术(英文版)》2017,28(10)
This paper presents the gas distribution analysis by injecting air fountain into the containment and simulations with the HYDRAGON code. Turbulence models of standard k-ε(SKE), re-normalization group k-ε(RNG) and a realizable k-ε(RLZ) are used to assess the effects on the gas distribution analysis during a severe accident in a nuclear power plant. By comparing with experimental data,the simulation results of the RNG and SKE turbulence models agree well with the experimental data on the prediction of dimensionless density distributions. The results illustrate that the turbulence model choice had a small effect on the simulation results, particularly the region near to the air fountain source. 相似文献
85.
In this paper, a laminated composite plate is analyzed using a multiscale method. At first, material properties of a lamina are obtained using an analytical micromechanical approach called simplified unit cell method (SUCM), and then in structural level, the generalized differential quadrature method (GDQM) is used to analyze a laminated composite plate. By means of the Boltzmann superposition principle, the viscoelastic behavior of the matrix is obtained. The Prony series is considered to define the compliance of matrix. To verify the results, graphiteT300/epoxy5208 composite material is analyzed and the results are compared with existing experimental data. The multiscale algorithm includes obtaining overall properties of the composite by SUCM; then, these properties are used to define the bending stiffness. Governing equations of motion of laminated composite plate are solved via GDQM and Newton–Raphson method. Variations of stresses and displacements versus time and volume fraction of the fibers are shown for laminated composite plates with different boundary conditions. 相似文献
86.
Abdulaziz Ali Alghamdi Abdulillah Al-Soulami Wassem Sharaf Saeed Abdel-Basit Al-Odayni Abdelhabib Elsamlali Ahmed Abdulaziz Al-Owaais 《国际聚合物材料杂志》2019,68(5):229-242
A series of poly(acrylic acid-co-methylvinylketone–graft–sulfamethoxazole)(AVMDS) species was synthesized for drug carrier applications. The synthesis involved two steps: copolymerization of acrylic acid(AA) with methyl vinyl ketone(MVK) through the free radical route and subsequent grafting of the sulfamethoxazole (SMX) onto the copolymer via the Schiff base reaction of the primary amine of SMX with the carbonyl groups of the MVK units. The structures and properties of the materials were characterized by nuclear magnetic resonance(NMR), X-ray diffraction(XRD), differential scanning calorimetry(DSC), and scanning electronic microscopy (SEM). An in-vitro cytotoxicity test of the drug-carrier systems via MTT assay revealed no significant cytotoxic effect at concentrations up to 100?µg?·?ml?1. The dynamic release of SMX from these systems through a retro-imidation reaction (inverse Schiff base reaction) was investigated in depth, where the diffusion through the polymer matrix, the enhancement of the water solubility of SMX, the influence of the initial drug concentration, the pH of the medium, and the effect of the degree of swelling of the polymer matrix on the release dynamics were evaluated. The AVMGS4 and AVMGS1 drug carrier systems containing 3.58 and 1.18?wt% of SMX were the best performing systems. 相似文献
87.
88.
Mohammad Javad Jafari Mohammad Esmaeil Azim-Araghi Samira Barhemat 《Journal of Materials Science》2012,47(4):1992-1999
Chemiresistors based on palladium phthalocyanine (PdPc) thin films were investigated as humidity sensors. The samples were
thermally evaporated onto gold electrodes with a thickness about 100 nm. Optical and electrical characteristics of PdPc thin
films were investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), and electrical measurements. The SEM
image demonstrates PdPc (30–60 nm) nanosized particles, and XRD pattern shows that thin films are in α-phase at room temperature. Electrical measurements also confirm that PdPc exhibit semiconducting and photoconducting behaviors,
and thermal activation energies of thin films were calculated. After that, the sensitivity and reversibility of devices were
investigated on exposure to 20–90% RH in various chemical environments at 293 and 323 K. The response time (35–45 s) and recovery
time (75–105 s) of sensors were measured at 293 K with respect to different chemical environments. At last, the stability
of devices versus different RH% and chemical environments were tested. The sensors show very good stability on exposure to
RH for a period of 2 months but their stability has been reduced in ethanol, acetone, and ammonia environments. 相似文献
89.
Solutions containing copper ions are produced at copper mines due to its dissolution from ores and dumps. It is important to recover these ions to prevent this toxic element from entering the environment and because it could be economical. We investigated the use of ion flotation for extracting Cu ions from diluted mine water from the Veshnaveh Mine in Qom, Iran. Experiments were conducted using floatation cells at pH 6, 9, and 12 with diluted solutions containing 10 mg L?1 of Cu. Sodium dodecyl sulfate and hexadecyl trimethyl ammonium bromide (HTAB) were used as collectors and methyl isobutyl carbinol (MIBC) and ethanol were used as frothers. The best result was achieved by maximizing Cu ion recovery and minimizing water recovery at pH 12, using 100 mg L?1 of HTAB and 0.1 % (v/v) of MIBC. Copper and water recovery were 79 and 24 %, respectively. 相似文献
90.
Giovanni Barone Saeed Rahimi Yazdi Søren K. Lillevang Lilia Ahrné 《Comprehensive Reviews in Food Science and Food Safety》2021,20(6):5616-5640
Calcium (Ca) is a key micronutrient of high relevance for human nutrition that also influences the texture and taste of dairy products and their processability. In bovine milk, Ca is presented in several speciation forms, such as complexed with other milk components or free as ionic calcium while being distributed between colloidal and serum phases of milk. Partitioning of Ca between these phases is highly dynamic and influenced by factors, such as temperature, ionic strength, pH, and milk composition. Processing steps used during the manufacture of dairy products, such as preconditioning, concentration, acidification, salting, cooling, and heating, all contribute to modify Ca speciation and partition, thereby influencing product functionality, product yield, and fouling of equipment. This review aims to provide a comprehensive understanding of the influence of Ca partition on dairy products properties to support the development of kinetics models to reduce product losses and develop added-value products with improved functionality. To achieve this objective, approaches to separate milk phases, analytical approaches to determine Ca partition and speciation, the role of Ca on protein–protein interactions, and their influence on processing of dairy products are discussed. 相似文献