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21.
Anodic oxidation effects on the structure of the basal and edge surfaces of pyrolytic graphite in alkaline electrolytes have been studied. Laser Raman spectroscopy, a gas-phase chemical modification method, coupled with X-ray photoelectron spectroscopy and secondary ion-mass spectroscopy techniques, were used. Anodic oxidation of the surfaces of pyrolytic graphite in alkaline electrolytes does not cause destruction of their surface structure, even at a higher level of treatment, unlike oxidation of acid electrolytes. In alkaline electrolytes, the number of hydroxyl groups added on the edge surface gradually increases with the increase in treatment level, whereas the number of carboxyl groups does not increase. It was found that anodic oxidation in alkaline electrolytes has a wider permitted range of treatment, in which hydroxyl groups can be added without destroying the edge surface structure, than that found in acid electrolytes. On the other hand, the number of hydroxyl groups added by treating with alkaline electrolytes is smaller than that with acid electrolytes. At a higher treatment level with acid electrolytes, oxidation occurs, even to a depth of 40 nm from the edge surface, whereas with alkaline electrolytes, oxidation occurs only at the surface. On the basis of these results, the effects of electrolytes on the adhesion between carbon fibres and epoxy resin matrix are discussed. 相似文献
22.
Toshifumi Saigusa
Sakae Shimizu
《Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment》1989,280(2-3):195-197The expectation of LET∞ (unrestricted linear energy transfer) for a tritium beta particle around its parent nucleus in water has been calculated by the use of the energy-range relation of electrons. The amount of energy deposited by a beta particle with a certain initial energy over the interval of one micron at a definite position is obtained from the relation by the calculus of difference, and the probability that the event takes place per decay of tritium is estimated from the energy spectrum of tritium beta particles. The calculated values of expectations of LET∞ are higher at positions close to the parent nucleus. 相似文献
23.
The performance of 40 channel AM-VSB video signal transmission using a Pr3+-doped fluoride fibre amplifier (PDFA) was examined. The PDFA improves the loss budget by 10 dB for 52 dB CNR, and distortion levels almost satisfy the CATV trunk line specifications. The video quality degradation after PDFA amplification was `imperceptible' in subjective tests 相似文献
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Fumio Matsumura Masayuki Fujita Masanao Shimizu 《Electrical Engineering in Japan》1991,111(7):117-124
This paper presents the robust control design of a magnetic suspension system for a flexible beam which is a simplified model of an elastic rotor in a magnetic bearing system. To stabilize this magnetic suspension system which is unstable in nature, the Hinfin; control theory is applied for a design of the control system. To apply the Hinfin; control theory, a statespace model of an augmented plant with frequency-weighting functions is constructed. This augmented plant has two inputs which are the exogenous inputs and the control inputs, and two outputs which are the sensor outputs and the regulated outputs. Here we consider the mixed sensitivity problem. The Hinfin; controller is implemented by a digital controller which is able to execute the computations very quickly. For the evaluation of the control performance, several experiments are made. The robustness of the closed-loop system is confirmed by the experimental results. The result of this study is useful for the control design of a magnetic bearing system. 相似文献
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Takaaki Wajima Tomoe Shimizu Yasuyuki Ikegami 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(6):921-927
BACKGROUND: This study aimed to investigate the synthesis of zeolites from paper sludge ash (PSA) with added diatomite to remove both NH4+ and PO43? for water purification. The PSA had low Si and significant Ca contents. Four types of diatomite: white (T‐W) and brown (T‐B) from deposits of marine origin in Takanosu, and white (S‐W) and gray (S‐G) from lacustrine deposits in Shonai, were added to NaOH solution to increase the Si content and thereby synthesize zeolites with high cation exchange capacity (CEC). RESULTS: The order of the amounts of Si extracted from the diatomite to the alkali solution was S‐W > T‐W = T‐B > S‐G, which correlates with the amorphous SiO2 content of diatomite. The original ash without addition of diatomite yielded hydroxysodalite with CEC of about 1.0 mmol g?1. For all samples, the addition of diatomite to the solution yielded zeolite‐P with a higher CEC, but the addition of excess Si inhibited the synthesis of zeolite‐P, and the CEC of the product was low. A product with high CEC including zeolite‐P was obtained in a solution with around 500 mmol L?1 of Si concentration, and had the ability to remove both NH4+ and PO43?. CONCLUSION: Diatomite has the potential for used as an additive for the synthesis of high CEC zeolite from PSA. The product with zeolite‐P exhibited relatively high CEC, capacity for NH4+ uptake, and the ability to remove PO43? by precipitation, which is preferable for water purification applications. Copyright © 2008 Society of Chemical Industry 相似文献