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101.
Nitu Bhatnagar Sangeeta Jha Shantanu Bhowmik Govind Gupta J. B. Moon C. G. Kim 《Surface Engineering and Applied Electrochemistry》2012,48(2):117-126
In this work, the effect of low pressure plasma and atmospheric-pressure plasma treatment on surface properties and adhesion characteristics of high performance polymer, Polyether Ether Ketone (PEEK) are investigated in terms of Fourier Transform Infrared Spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), and Atomic Force Microscopy (AFM). The experimental results show that the PEEK surface treated by atmospheric pressure plasma lead to an increase in the polar component of the surface energy, resulting in improving the adhesion characteristics of the PEEK/Epoxy adhesive system. Also, the roughness of the treated surfaces is largely increased as confirmed by AFM observation. These results can be explained by the fact that the atmospheric pressure plasma treatment of PEEK surface yields several oxygen functionalities on hydrophobic surface, which play an important role in increasing the surface polarity, wettability, and the adhesion characteristics of the PEEK/Epoxy adhesive system. 相似文献
102.
Effect of ferrocene concentration on the synthesis of bamboo-shaped carbon-nitrogen nanotube bundles
Yadav RM Shripathi T Srivastava A Srivastava ON 《Journal of nanoscience and nanotechnology》2005,5(5):820-824
We have investigated the effect of ferrocene concentration on the synthesis of carbon-nitrogen (C-N) nanotubes. The bamboo-shaped carbon-nitrogen nanotubes were synthesized by spray pyrolysis of Fe(C5H5)2 and CH3CN solution using argon as a carrier gas at the optimum temperature of approximately 900 degrees C. The effect of ferrocene concentration on the length and concentration of nitrogen in nanotubes was studied. Micro-structural features of the nanotubes were monitored employing scanning and transmission electron microscopic techniques. SEM studies reveal that with decreasing ferrocene concentration from 25 mg ml(-1) to 5 mg ml(-1), the length of the nanotubes vary from 80 microm to 430 microm. A feasible growth model has been described and discussed. X-ray photoelectron spectroscopic studies have confirmed the formation of nitrogen-doped carbon nanotubes. These studies reveal that the nitrogen concentration in the nanotubes decreases with the increase of ferrocene concentration. The present synthesis route also provides means of producing carbon nanotubes with different concentrations of nitrogen. 相似文献
103.
In present communication, we propose a modified resource allocation strategy, namely, hybrid connection algorithm, for achieving efficient restoration in WDM optical networks. The main theme of the algorithm is that, while attempting connection establishment, a wavelength is reserved in advance for providing resources for backup lightpaths. The analysis and the comparison of the proposed strategy with other existing strategies has been undertaken using metrics such as, restoration efficiency, number of wavelength links used by primary and backup lightpaths, and the percent link utilization. The proposed strategy provides 100% restoration efficiency and much better performance than the existing techniques. 相似文献
104.
Sabbi G. DiMarco J. Nobrega A. Ogitsu T. Schlabach P. Tompkins J.C. Yadav S. 《Applied Superconductivity, IEEE Transactions on》2000,10(1):123-126
Superconducting quadrupole magnets with 70 mm aperture and nominal field gradient of 215 T/m are being developed by the US-LHC Accelerator Project for the Interaction Regions of the Large Hadron Collider. Due to large beam size and orbit displacement in the final focusing triplet, these magnets are subject to stringent field quality requirements. For this reason, a correction scheme based on design calculations, fabrication issues and tests results involving magnetic shims 相似文献
105.
Parveen Kumar Sangeeta Singh J.K. Juneja Chandra Prakash K.K. Raina 《Materials Chemistry and Physics》2011
Lanthanum modified Ba0.80Pb0.20Ti0.90Zr0.10O3 (BPZT) ceramics with composition Ba0.80−xLax Pb0.20Ti0.90Zr0.10O3; x = 0–0.01 in steps of 0.0025 were prepared by conventional solid state method. All the samples were sintered at 1325 °C after compacting in circular discs. Detailed structural and ferroelectric properties were carried out for sintered specimens. X-ray diffraction analysis for all the sintered specimens shows tetragonal structure with perovskite. Coercive field (Ec) and remanent polarization (Pr) to spontaneous polarization (Ps) ratio (Pr/Ps) was found to decrease with increase in temperature. Pr/Ps ratio was found to decrease with increase in x, except x = 0.0025. 相似文献
106.
Dhananjay Yadav G.S. Agrawal R. Bhargava 《International Journal of Engineering Science》2011,49(11):1171-1184
In the present paper we have considered thermal instability of rotating nanofluids heated from below. Linear stability analysis has been made to investigate analytically the effect of rotation. The more important effect of Brownian motion and thermophoresis has been included in the model of nanofluid. Galerkin method is used to obtain the analytical expression for both non-oscillatory and oscillatory cases, when boundaries surfaces are free–free. The influence of various nanofluids parameters and rotation on the onset of convection has been analysed. It has been shown that the rotation has a stabilizing effect depending upon the values of various nanofluid parameters. The critical Rayleigh number for the onset of instability is determined numerically and results are depicted graphically. The necessary and sufficient conditions for the existence of over stability are also obtained. 相似文献
107.
Polycrystalline sample of (Na0.5Bi0.5)ZrO3 was prepared using a high-temperature solid-state reaction technique. XRD analysis indicated the formation of a single-phase
orthorhombic structure. Dielectric study revealed the diffuse phase transition at 425 °C. AC impedance plots were used as
tools to analyse the electrical behaviour of the sample as a function of frequency at different temperatures. The ac impedance
studies revealed the presence of grain boundary effect at and above 350 °C. Complex impedance analysis indicated non-Debye
type dielectric relaxation and negative temperature coefficient of resistance (NTCR) character of (Na0.5Bi0.5)ZrO3. AC conductivity data were used to evaluate the density of states at Fermi level and activation energy of the compound. DC
electrical and thermal conductivities of grain and grain boundary have been assessed. 相似文献
108.
A theory has been developed for the absorption of chlorine in aqueous slurries of calcium hydroxide accompanied by a two-step instantaneous reaction and desorption and simulation is carried out to study the effects of various parameters. The rates of absorption of chlorine and desorption of HOC1 from the aqueous slurry are enhanced when fine particles are present in two diffusion film regions on the liquid side. It is concluded that intensification in the rates of absorption of chlorine and rates of desorption can be realized by using high loading of smaller particle size. An optimum kL must be used to enhance rates of Cl2 absorption and HOG desorption in order to permit the formation of two reaction planes in the diffusion film. Rates can be intensified by an order of magnitude by the proper selection of operating conditions. 相似文献
109.
Powder of lanthanum-modified lead zirconate titanate (PLZT) with the composition La/Zr/Ti=8/65/35, was synthesized from aqueous
nitrate solutions. A single-phase PLZT was obtained at ∼550 °C. The reactivity of the powder during low-temperature heating
was determined using X-ray diffraction and various thermal analysis techniques. The dielectric properties of the compound
were also studied at 1 and 10 kHz frequency from room temperature to 200 °C. Diffuse phase transition (DPT) in the material
was observed around 136 °C at 1 kHz. An increase in peak-permittivity temperature (i.e. the transition temperature) with increasing
frequency (a characteristic of relaxor ferroelectrics) was also observed. 相似文献
110.
Rajesh Kumar Rajesh Kumar Singh Pawan Kumar Dubey Dinesh Pratap Singh Ram Manohar Yadav Radhey Shyam Tiwari 《Advanced Materials Interfaces》2015,2(15)
3D hierarchical structures are reported based on graphene–nickel encapsulated nitrogen‐rich aligned bamboo like carbon nanotubes, which show not only high‐performance supercapacitance behavior but also a great robust cyclic stability. A facile synthesis route is developed of 2D nickel oxide decorated functionalized graphene nanosheets (2D‐NiO‐f:GNSs) hybrids and 3D nitrogen doped bamboo‐shaped carbon nanotubes (NCNTs) vertically standing on the functionalized graphene nanosheets (3D‐NCNT@f:GNSs) by using a thermal decomposition method. The chemical reduction and morphology‐dependent electrochemical response are investigated. The enhanced specific capacitance of 3D‐NCNT@f:GNSs as compared to that of 2D‐NiO‐f:GNSs suggests the synergistic effects and indicates the importance of energy storage and superior long‐term cycling performance that are achieved. This 3D‐NCNT@f:GNSs hybrid shows a remarkable cycling stability with a maximum power density of 12.32 kW kg−1 and maximum energy density of 109.13 Wh kg−1 due to the good connection of NCNT and f:GNSs. This unique 3D nano network architecture enables the availability of large surface areas of NCNT, thus endowing the nanohybrids with high specific capacitance and excellent reusability. 相似文献