Evaluation of TEM samples of an Mg-Al alloy prepared using FIB milling at the operating voltages of 10 kV and 40 kV

Transmission electron microscopy (TEM) samples of an Mg-Al alloy has been prepared using a Ga-focused ion beam (FIB) milling at two different operating voltages of 10 kV and 40 kV to investigate the influence of the FIB energy on the sample quality. The fine structures of the samples have been studied using a high resolution TEM, and the concentration of the implanted Ga was analysed using an energy dispersive X-ray (EDX) analysis. The result of the TEM observation revealed that point defects were introduced to the sample finally milled at 40 kV but not at 10 kV. However, crystal lattice images and electron diffraction patterns were clearly observed on both the samples. The typical influence of the FIB energy was indicated in the elemental analysis. The relative Ga concentration in the thin sample finally milled at 10 kV was 1.0-2.0 at% that is less than half of 4.0-6.0 at% of the Ga concentration in the sample finally milled at 40 kV. A comparison between the experimental results of the Ga concentration measurement with simulation was also discussed.     

A Unified Gradient-Based Approach for Combining ASM into AAM

Active Appearance Model (AAM) framework is a very useful method that can fit the shape and appearance model to the input image for various image analysis and synthesis problems. However, since the goal of the AAM fitting algorithm is to minimize the residual error between the model appearance and the input image, it often fails to accurately converge to the landmark points of the input image. To alleviate this weakness, we have combined Active Shape Models (ASM) into AAMs, in which ASMs try to find correct landmark points using the local profile model. Since the original objective function of the ASM search is not appropriate for combining these methods, we derive a gradient based iterative method by modifying the objective function of the ASM search. Then, we propose a new fitting method that combines the objective functions of both ASM and AAM into a single objective function in a gradient based optimization framework. Experimental results show that the proposed fitting method reduces the average fitting error when compared with existing fitting methods such as ASM, AAM, and Texture Constrained-ASM (TC-ASM) and improves the performance of facial expression recognition significantly.     

中国液态锂铅包层材料研究进展

液态锂铅包层是国际上普遍关注和最有发展潜力的聚变堆包层概念设计之一,而包层材料是液态锂铅包层的核心问题之一.目前,液态锂铅包层普遍选用低活化铁素体/马氏体钢(RAFM钢)作为结构材料,液态锂铅作为中子倍增剂及氚增殖剂.另外,部分设计采用了耐高温、电绝缘流道插件作为功能材料,以降低磁流体动力学效应及提高冷却剂出口温度(高于700℃).为适应液态包层的发展需求,中国科学院等离子体物理研究所FDS团队联合国内外相关研究单位,进行了具有中国自主知识产权的中国低活化马氏体钢(CLAM钢)及液态锂铅包层功能材料研发,并开展了锂铅热对流及强迫对流回路的设计、研制及腐蚀实验研究,以研究液态金属锂铅的流动特性及其与结构和功能材料的相容性.同时建立了聚变堆材料数据库平台,为促进中国聚变堆液态包层及材料技术的研究和发展提供数据支持.     

Upgrading of X-ray CT technology for analyses of irradiated FBR MOX fuel

The X-ray CT technology previously developed by JAEA was upgraded. The shape of the X-ray source beam was changed from a circular shape to an elliptical one and the collimator slit width was decreased from 0.3 to 0.1 mm. The X-ray detector was improved by changing a CdWO₄ scintillator to a highly sensitive silicon semiconductor detector. The analysis code of X-ray CT image was revised with respect to the number of points by using two kinds of experimental results and taking into account the effects of crack existence and deviation of the central void position from the radial center of a fuel pellet. As a result, high resolution X-ray CT images could be obtained on the transverse cross section of irradiated fuel assemblies. The error of the dimensional measurement was improved from ±0.1 to ±0.03 mm by upgrading the instrument and revising the analysis code of X-ray CT image. The discriminating accuracy of density difference could be increased, and the low density region (undisturbed region) and high density region (equi-axial and columnar regions) in the X-ray CT image on the cross section of irradiated fuel could be discriminated from each other. The reliability of fuel performance analysis improves because a large number of PIE data can be collected, compared with the conventional destructive PIE.     

Radiation-induced polymerization of ethylene in pilot plant. III. Heavy-phase recycling process

Radiation-induced polymerization of ethylene using aqueous tert-butyl alcohol as medium was carried out in a large-scale pilot plant with a 50-liter central source-type reactor at a pressure of 105 to 395 kg/cm², temperature of 30° to 80°C, mean dose rate of 4.5 × 10⁴ to 1.9 × 10⁵ rads/hr, ethylene feed rate of 5.5 to 23.5 kg/hr, and medium feed rate of 21 to 102 l./hr. The space–time yield and molecular weight of the polymer were in the range of 4.7 to 16.8 g/l.-hr and 1.3 × 10⁴ to 8.9 × 10⁴, respectively. The space–time yield and molecular weight increased with mean residence time at 30°C, whereas at 80°C they became almost independent of the time. The space–time yield increased with pressure and dose rate, slightly decreased with temperature, and was maximum at ethylene molar fraction of 0.5. The polymer molecular weight increased with pressure and ethylene molar fraction, and decreased with dose rate and temperature. The total amount of deposited polymer on the reactor wall, source case wall, and scraping blades was usually less than 1 kg, which was negligibly small for the analysis of polymerization. Continuous discharge of the polymer slurry and production of fine-powder polyethylene were successfully carried out. In the central source-type reactor, a dose rate of 1.9 × 10⁵ rads/hr was obtained with a ⁶⁰Co source of ca. 12 kCi.     

Spherical approximation for multiple cameras in motion estimation: Its applicability and advantages

Estimating motions of a multi-camera system which may not have overlapping fields of view is generally complex and computationally expensive because of the non-zero offset between each camera’s center. It is conceivable that if we can assume that multiple cameras share a single optical center, and thus can be modeled as a spherical imaging system, motion estimation and calibration of this system would become simpler and more efficient.     

UV Light-Generated Superhydrophilicity of a Titanium Surface Enhances the Transfer,Diffusion and Adsorption of Osteogenic Factors from a Collagen Sponge

It is a significant challenge for a titanium implant, which is a bio-inert material, to recruit osteogenic factors, such as osteoblasts, proteins and blood effectively when these are contained in a biomaterial. The objective of this study was to examine the effect of ultraviolet (UV)-treatment of titanium on surface wettability and the recruitment of osteogenic factors when they are contained in an atelocollagen sponge. UV treatment of a dental implant made of commercially pure titanium was performed with UV-light for 12 min immediately prior to the experiments. Superhydrophilicity on dental implant surfaces was generated with UV-treatment. The collagen sponge containing blood, osteoblasts, or albumin was directly placed on the dental implant. Untreated implants absorbed only a little blood from the collagen sponge, while the UV-treated implants absorbed blood rapidly and allowed it to spread widely, almost over the entire implant surface. Blood coverage was 3.5 times greater for the UV-treated implants (p < 0.001). Only 6% of the osteoblasts transferred from the collagen sponge to the untreated implants, whereas 16% of the osteoblasts transferred to the UV-treated implants (p < 0.001). In addition, a weight ratio between transferred albumin on the implant and measured albumin adsorbed on the implant was 17.3% in untreated implants and 38.5% in UV-treated implants (p < 0.05). These results indicated that UV treatment converts a titanium surface into a superhydrophilic and bio-active material, which could recruite osteogenic factors even when they were contained in a collagen sponge. The transfer and subsequent diffusion and adsorption efficacy of UV-treated titanium surfaces could be useful for bone formation when titanium surfaces and osteogenic factors are intervened with a biomaterial.