Influence of the post-deformation annealing heat treatment on the low-cycle fatigue of NiTi shape memory alloys

Shape memory alloys (SMA) suffer from the same impairing mechanisms experienced during cycling loading by classic alloys. Moreover, SMA fatigue behavior is greatly influenced by thermomechanical cycling through the zone of thermoelastic phase transformation, which is the basis of shape memory and superelasticity effects. Since the fatigue resistance of any material can be improved by an appropriate thermomechanical treatment, in the present work combined differential scanning calorimetry and microhardness testing were used to determine an optimum annealing temperature for the cold-worked Ni-50.1%Ti alloy. The optimization is based on the assumption that latent heat of transformation is proportional to the mechanical work generated by SMA upon heating, while material hardness is related to the yield stress of the material. It is supposed that an optimum trade-off in these two properties guarantees the best dimensional and functional stability of SMA devices. The level and stability of the mechanical work generated by the material during low-cycle fatigue testing are considered criteria for the material performance and thus of the validity of the proposed optimization procedure.     

3D thermohydrodynamic analysis of a textured slider

Analysis of a 3D inlet textured slider bearing with a temperature dependent fluid is performed. Numerical simulations are carried out for a laminar and steady flow. Hot and cold lubricant mixing in the groove is modelled and examined for different operating conditions. Thermohydrodynamic performance of the bearing is analyzed for different texture lengths.Results show that texture has a stronger and positive influence on load carrying capacity when thermal effects are considered. This beneficial effect is at a maximum for the longest dimples with a length shorter than the pad length. Texture is also beneficial for the load carrying capacity when the sliding speed and inlet flow rate are varied. The load carrying capacity of the slider can be increased by up to 16% in severe operating conditions (high sliding speed).     

Vacuum compatible sample positioning device for matrix assisted laser desorption∕ionization Fourier transform ion cyclotron resonance mass spectrometry imaging

The high mass accuracy and resolving power of Fourier transform ion cyclotron resonance mass spectrometers (FT-ICR MS) make them ideal mass detectors for mass spectrometry imaging (MSI), promising to provide unmatched molecular resolution capabilities. The intrinsic low tolerance of FT-ICR MS to RF interference, however, along with typically vertical positioning of the sample, and MSI acquisition speed requirements present numerous engineering challenges in creating robotics capable of achieving the spatial resolution to match. This work discusses a two-dimensional positioning stage designed to address these issues. The stage is capable of operating in ～1 × 10(-8) mbar vacuum. The range of motion is set to 100 mm × 100 mm to accommodate large samples, while the positioning accuracy is demonstrated to be less than 0.4 micron in both directions under vertical load over the entire range. This device was integrated into three different matrix assisted laser desorption∕ionization (MALDI) FT-ICR instruments and showed no detectable RF noise. The "oversampling" MALDI-MSI experiments, under which the sample is completely ablated at each position, followed by the target movement of the distance smaller than the laser beam, conducted on the custom-built 7T FT-ICR MS demonstrate the stability and positional accuracy of the stage robotics which delivers high spatial resolution mass spectral images at a fraction of the laser spot diameter.     

A low-wavenumber-extended confocal Raman microscope with very high laser excitation line discrimination

We describe the simple modification of a confocal Raman imaging microscope to incorporate two ultra-narrow holographic notch filters. The modified microscope rejects the laser excitation line (Rayleigh peak) by a discrimination factor of ～10(11) and allows simultaneous measurements of Stokes/anti-Stokes Raman shifts as close as ～10/20 cm(-1) to the Rayleigh line. The extremely high rejection ratio of the Rayleigh peak results in its intensity becoming comparable to typical Raman scattering signals. This is essential for micro-Raman spectroscopy and imaging in the low-wavenumber region. We illustrate the resulting performance with measurements on silicon/silica, sapphire, sulfur, L-cystine, as well as on single-walled carbon nanotubes (SWNTs). We find that both aggregated (bulk) and individual (deposited on substrate) SWNTs demonstrate strong and broad characteristic Raman features below ～100 cm(-1)-in a region which has remained essentially unexplored in measurements of bulk SWNT samples and which has so far been inaccessible for Raman spectroscopy of individual SWNTs.     

A microwave transmission-line network guiding electromagnetic fields through a dense array of metallic objects

We present measurements and simulations of a transmission-line network that has been designed for cloaking applications in the microwave region. Here the network is not used for cloaking but for channelling electromagnetic fields through an electrically dense array of metal objects, which alone is basically impenetrable to the impinging electromagnetic radiation. With the designed transmission-line network the waves emitted by a source placed in an air-filled waveguide are coupled into the network and guided through the array of metallic objects. Our goal is to illustrate the simple manufacturing, assembly, and the general feasibility of cloaking devices based on the transmission-line approach. Most importantly, we demonstrate both with measurements and with numerical simulations the excellent coupling of waves between the network and the surrounding medium.