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11.
Unusual Indentation Behavior of Alkali Metaphosphate Glass Above Glass Transition Temperature
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Jun Endo Seiji Inaba Hiroyuki Muto Setsuro Ito 《Journal of the American Ceramic Society》2017,100(1):81-85
The mixed alkali metaphosphate glass 12.5Li2O–12.5Na2O–12.5K2O–12.5Cs2O–50P2O5 (mol%) compressed under uniaxial stress shows unusually large recovery of its shape during heating above its glass transition temperature (Tg). To clarify the mechanism, the viscous, elastic, and plastic behavior of the metaphosphate glass was investigated with the depth‐sensing indentation method. From the load‐displacement (P–h) curves of the glass, a large recovery of the depth displacement was found during unloading above Tg. By analyzing the P–h curves with a viscous–elastic–plastic model, the large recovery was concluded to be due to larger elastic deformation than viscous deformation even above Tg. The phenomenon can be attributed to relaxation to the randomly oriented ‐P–O–P– chain structure from the oriented chain structure formed under stress in the metaphosphate glass . 相似文献
12.
A shaking vessel with “current pole”, which is a center pole installed at the bottom, had shorter mixing time than a shaking vessel with a cone at the bottom. The mass transfer rate on the suspended particles was also measured in the shaking vessel where ion-exchange resin beads were used as the suspended particles. The dependence of the solid-liquid mass transfer coefficient on the circulating frequency changed at the critical circulating frequency for complete suspension NJS. For a circulating frequency higher than NJS, the mass transfer coefficient was correlated with the power consumption per unit volume, regardless of presence or not of the current pole. 相似文献