Hydrothermal Synthesis of Magnesium Aluminate Platelets

Magnesium aluminate (MgAl₂O₄) platelets were first synthesized by hydrothermal treatment of γ-AlO(OH) in a magnesium nitrate aqueous solution at 400°C. The platelets are 100–200 nm in width and 25 nm in thickness. The influence of temperature, the anions of the magnesium salt, the amount of magnesium salt, and precursor pH on the formation of such structure was investigated. The experimental results indicated that the anions of the magnesium salt and precursor pH could have a significant influence on the growth of MgAl₂O₄. MgAl₂O₄ formation followed the in situ transformation mechanism, which was the reason why the MgAl₂O₄ crystallites had a platelet morphology.     

漫谈钛合金在舰船上的应用

钛合金优良的耐海水腐蚀性能、高的比强度、无磁性等特点,使其在船用领域大有潜力可为,我国的船用钛合金经过近40年的研究开发,基本能满足舰艇不同强度级别的需求,在舰船上应用具有明显的社会效益和经济效益,值得进一步应用推广。本文介绍了国内外舰船用钛合金的开发及应用情况。对钛合金在鱼雷发射水缸、高压气瓶、一回路危急冷却器、声扫雷具、二回路泵、阀及管系、声纳导流罩、螺旋桨等方面的应用作了重点介绍。     

完善管理机制提高校长队伍整体水平

校长是一所学校的指挥者,一名好的校长,可以带出一批训练有素的教师队伍,可以推进学校教育改革的不断发展.抓好校长队伍建设是贯彻党的教育方针,全面推进素质教育,办好学校的头等大事.那么,如何加强校长队伍建设就显得尤为重要了.     

继续奏响振荡向上主旋律——2002年白银市场回顾及其2003年展望

本文对2002年国际国内白银市场做了全面分析,对2003年白银市场走势进行了分析预测。白银作为一种贵金属,同时又具有工业金属的特性,世界经济形势,世界政治局势的变化,都对白银价格走势产生影响。鉴于该金属的双重特性,本文就从白银的供应、需求、消费及世界经济的发展等方面论述白银市场前进趋势。     

Facile synthesis of ordered nanocrystalline alumina thin films with tunable mesopore structures

Mesoporous alumina layers have attracted attention for their potential use in ultrafiltration of salts, as a heterogeneous catalyst support, an adsorbent in environmental cleanup, and in petroleum refinement. The ability to control the fast hydrolysis rate of the inorganic precursors using simple and inexpensive routes is important for that potential to be realized. Herein, we introduce a novel and facile route to synthesize mesoporous alumina thin films from the combination of inexpensive and commercially available copolymer with aluminum chloride or nitrate (salts) in an EtOH–surfactant–NH₃ · H₂O–salts (EsNs) system through the evaporation-induced self-assembly (EISA) method. Mesoporous alumina layers obtained utilizing the EsNs system have ordered and tunable pore structures. The ability to easily control the mesophases of the alumina layers within a short time provides distinct advantages over previously reported synthesis procedures. Most importantly, we demonstrate that the binding of surfactant and NH₃ · H₂O for the formation of hydrogen bond between them in the EsNs system controls the fast hydrolysis rate of the inorganic species. This allows for the synthesis of nanocrystalline alumina layers via the aluminum oxo-clusters’ assembly with the surfactant. Such simple route may be applied in the synthesis of other non-silica mesostructured oxides.     

A novel in situ synthesis of dicalcium phosphate dehydrate nanocrystals in biodegradable polymer matrix

In the paper, we found a novel method to synthesize dicalcium phosphate dehydrate (DCPD) nanocrystals by in situ reaction in biodegradable PDLLA matrix. Calcium hydrid was selected as calcium source of DCPD, which is different from general methods. The method is not only simple and effective to synthesize Ca–P particles, but also can avoid the aggregation of inorganic nanoparticles in the course of their being dispersed into polymer matrix.     

激光束偏转法检测金属表面层的缺陷

本文编程计算了由激光光热应产业的金属表面的温度分布和泵浦光的调制频率、金属层厚度等的关系，预言检测浓度缺陷的能力。用激光光束偏转法检测到表面下不同深处的缺陷，并把面扫描幅值信号以三维象和灰度象显示。     

长链烯烃-苯烷基化反应的分子筛催化剂再生性能的研究

通过热重分析和活性稳定性评定考察催化剂的再生性能。研究结果表明,进行氯气吹扫以及苯抽提后进行氮气吹扫两种预处理,导致失活催化剂的起燃点和烧焦反应活化能均有所提高,有利于控制烧焦反应速度。按苯抽提、氮气吹扫、烧焦的顺序,分三个阶段进行催化剂再生,再生催化剂的活性稳定性得到更充分的恢复。     

Effects of capsules on attachment of human periodontal ligament fibroblasts to root surface

The stability of cimetidine (Tagamet) was investigated in total parenteral nutrition (TPN) mixtures containing different amino acid sources. TPN mixtures were stored at 5 degrees C in ethylvinyl acetate bags for 28 days and analysed by stability-indicating high-pressure liquid chromatography. Results indicated that cimetidine was physically compatible and chemically stable (less than 5% degradation) for at least 28 days in TPN mixtures containing either Freamine III, Vamin 14 or Aminoplex 12 as the amino acid source.