Recent Japanese research activities on probabilistic fracture mechanics for pressure vessel and piping of nuclear power plant

This paper describes a review of recent Japanese activities on probabilistic fracture mechanics (PFM) analyses. Japan Atomic Energy Agency (JAEA: previously JAERI) had sponsored research committees on PFM organized by Japan Society of Mechanical Engineers (JSME) and Japan Welding Engineering Society (JWES) for more than a decade. This work still continues with the same members in JWES. The purpose of the continuous activity is to provide probabilistic approaches in several fields of integrity problems of nuclear power plant. This paper shows some of the newest results of the JWES research committee. First topic is evaluation of the new JSME code case with rules of Fitness-For-Service from the view of PFM, including reactor pressure vessel subject to pressurized thermal shock loading, piping with a crack of the allowable size and effect of sizing accuracy for piping integrity. The next one is development of new PFM techniques including reliability assessment of piping with domestic (Japanese) SCC data and maintenance optimization of LWRs based on risk and economic models. The last topic is the international round robin program just starting from 2008.     

Recycle for Sludge Scrap of Nd-Fe-B Sintered Magnet as Isotropic Bonded Magnet

The reduction diffusion method was performed for the sludge scrap of Nd-Fe-B sintered magnets with adding Ca metal to recover the oxidized Nd-Fe-B phase. After washing the resultant powders to remove Ca metal component, the powders obtained were recycled as an isotropic magnetic powder by the melt spinning method. The magnetic properties of powders as recycled were inferior, especially for the coercivity value, due to the deletion of rare earth metals during the washing process. The adjustment of metal composition, i.e., the addition of Nd metal, at the melt spinning process improved the magnetic properties to be Br=～0.75 T, Hcj=～0.93 mA·m-1, and(BH)max=～91 kJ·m-3. The magnetic properties of the bonded magnets prepared from the composition-adjusted powders were Br=～0.66 T, Hcj=～0.92 mA·m-1, and(BH)max=～70 kJ·m-3, which are approximately comparable to the commercially available MQPB boned one(Br=～0.73 T, Hcj=～0.79 mA·m-1, and(BH)max=～86 kJ·m-3).     

BioCell print utilizing patterning with electrostatically injected droplet (PELID) method

The objective of this study is to fabricate three-dimensional cell structures utilizing patterning with electrostatically injected droplet (PELID) method, because it is preferable to perform laboratory experiments with 3D cell structures in tissue engineering and artificial organ. However, it is difficult to fabricate 3D cell structures, because own weight of the cell is above the bonding force between cells. In this paper, we printed Madin?CDarby canine kidney cells and collagen as scaffolds utilizing the PELID method. We investigated growth of printed cells. Number of printed cells was increased day by day. We investigated the fundamental characteristics on patterning collagen. The printed collagen was thick when the time to print was increased. These results indicated that it is possible to fabricate 3D cell structure.     

Protective Effects of Voluntary Exercise on Hepatic Fat Accumulation Induced by Dietary Restriction in Zucker Fatty Rats

Weight control based on dietary restriction (DR) alone can cause lipid metabolic failure and progression to fatty liver. This study aimed to investigate the effect of exercise on preventing DR-induced hepatic fat accumulation in Zucker fatty (ZF) rats by focusing on the relationship between adipose tissue lipolysis and hepatic fat uptake. Six-week-old male ZF rats were randomly assigned to obese, DR, or DR with exercise (DR + Ex) groups. The DR and DR + Ex groups were fed a restricted diet, with the latter also undergoing voluntary exercise. After 6 weeks, hepatic fat accumulation was observed in the DR group, whereas intrahepatic fat was markedly reduced in the DR + Ex group. Compared with the obese (Ob) group, the DR group exhibited 2.09-fold expression of hepatic fatty acid translocase (FAT)/CD36 proteins (p < 0.01) and 0.14-fold expression of hepatic fatty acid-binding protein (FABP)1 (p < 0.01). There were no significant differences between the DR + Ex group and the Ob group. FAT/CD36 and hepatic triglyceride (TG) expression levels were strongly positively correlated (r = 0.81, p < 0.001), whereas there was a strong negative correlation between FABP1 and hepatic TG expression levels (r = −0.65, p < 0.001). Our results suggest that hepatic fat accumulation induced by DR in ZF rats might be prevented through exercise-induced modifications in FAT/CD36 and FABP1 expression.     

Electronic state and magnetism of the rare-earth carbide GdCx (x 0.33)

The electronic state and the magnetism of GdC_x (x = 0.33) were investigated by the discrete variational (DV)-Xα calculation method together with those of Gd metal. Magnetic moments on the gadolinium atoms located at the center of the Gd₁₇ and Gd₄C₂ clusters extracted from Gd metal and Gd_tC were calculated to be 8.38 and 9.70 μ_B, in qualitative agreement with the experimental values (7.96 and 8.28 μ_B respectively). The exchange splitting of the Gd 4f band in Gd₃C was found to increase from that of Gd metal and accounts for the higher Curie temperature of GdC₁ compounds observed in experiments. The calculated results show that the carbon atoms are charge acceptors in these compounds. The higher Curie temperature values (T_c = 350 K) observed in the GdC_x (x 0.33) compounds compared with Gd metal (T_c = 293 K) are discussed on the basis of the spin-fluctuation theory.     

Congener-specific analysis of Pcbs in food samples by using GC/MS

A GC/MS method for congener-specific analysis of polychlorinated biphenyls (PCBs) in food samples was evaluated. There was good agreement between total concentration of PCBs in fish samples (n = 16) measured by using the GC/MS method and the conventional GC-ECD method. The total diet study samples (fishery food, meat, egg, milk, and their products) collected from Osaka in 1982-2001 were analyzed by using the GC/MS method to estimate the temporal trend of daily intake of PCBs from food. The estimated daily intake of total PCBs (sum of tri- to heptaCBs) was in the range of 0.7-4.4 microg/person/day, far below the Japanese provisional acceptable daily intake (250 microg/50 kg-person/day). The dominant congener was 2,2',4,4',5,5'-hexachlorobiphenyl (#153), which accounted for 9-15% of total PCB. The ratio of lower chlorinated congeners decreased from the 1980's to post-2000. The results indicate that the PCB congener profile in foods has gradually changed.     

Competitive oxidation of formaldehyde and formate on amorphous copper-palladium-zirconium alloy electrodes in alkaline media

Raney-type Cu–Pd alloy electrodes were prepared from amorphous Cu–Pd–Zr ternary alloys by treatment with aq. HF, and competitive anodic oxidation reactions of HCHO and HCOO^– were studied on these electrodes in alkaline media. The initial HCHO oxidation product was HCOO^– even on Pd or Pd-rich alloy electrodes which should be more active to the HCOO^– oxidation than to HCHO. The product HCOO^– was oxidized only after a large decrease of the HCHO concentration in the electrolyte. The oxidation rate of HCOO^– was considerably lowered by the existence of even a small amount of HCHO, as well as by the introduction of CO. These results suggest that the HCHO electro-oxidation is accompanied by production of a surface contaminant such as adsorbed CO. The optimum nominal Pd atomic fraction in the Cu–Pd alloy electrodes suitable for the steady simultaneous oxidation of HCHO and HCOO^– in mixed solution was shown to be 0.25 and 0.4 in 1.0 M NaOH (M=moldm^–3) and 0.5 M K₂CO₃, respectively.     

Wavelength demultiplexer using GaInAs-InP MQW-based variable refractive-index arrayed waveguides fabricated by selective MOVPE

A GaInAs-InP multiple quantum well (MQW)-based wavelength demultiplexer composed of an arrayed waveguide in which the refractive index varies across the array was fabricated. Since optical path length differences between waveguides in the array are achieved through refractive-index differences that are controlled by SiO/sub 2/ mask design in selective metal-organic vapor phase epitaxy (MOVPE), straight waveguide gratings having reduced optical propagation losses can be achieved. Furthermore, by employing MQW waveguides, variations in the refractive index may be induced through an applied electric field, allowing the device to manipulate wavelengths dynamically. A straight arrayed waveguide device having a 1.4% difference in refractive index was fabricated using an asymmetric side mask via a single selective MOVPE growth. The achievement of a diffraction angle difference of 4.40/spl deg/ between wavelengths of 1520 and 1580 nm was confirmed experimentally. In addition, a preliminary wavelength demultiplexer with a wavelength separation of approximately 25 nm and a free spectral range (FSR) of approximately 100 nm was also fabricated.     

Application of eddy current inversion technique to the sizing of defects in Inconel welds with rough surfaces

This paper evaluates the applicability of eddy current inversion techniques to the sizing of defects in Inconel welds with rough surfaces. For this purpose, a plate Inconel weld specimen, which models the welding of a stub tube in a boiling water nuclear reactor is fabricated, and artificial notches machined into the specimen. Eddy current inspections using six different eddy current probes are conducted and efficiencies were evaluated for the six probes for weld inspection. It is revealed that if suitable probes are applied, an Inconel weld does not cause large noise levels during eddy current inspections even though the surface of the weld is rough. Finally, reconstruction of the notches is performed using eddy current signals measured using the uniform eddy current probe that showed the best results among the six probes in this study. A simplified configuration is proposed in order to consider the complicated configuration of the welded specimen in numerical simulations. While reconstructed profiles of the notches are slightly larger than the true profiles, quite good agreements are obtained in spite of the simple approximation of the configuration, which reveals that eddy current testing would be an efficient non-destructive testing method for the sizing of defects in Inconel welds.