Egyptian Mango Juice. Experiment on Storage Experience

In this study processed mango juice was packed in four types of containers and stored at different temperatures for 16 weeks through which furfural level determination and organoleptic assessment were conducted. The experiment revealed an evident relationship to exist among furfural level, storage temperature and type of packing material. Furfural level failed to closely parallel flavour difference; therefore it could be regarded as one of the features concomitant juice aging rather than accepted as a satisfactory criterion of off flavour. The study relates flavour deterioration to the changes in the lipid fraction of the juice.     

Influence of some compounds on gentamicin formation by Micromonospora purpurea

Production of gentamicin antibiotics by Micromonospora purpurea was carried out successfully on a synthetic medium which contained the following ingredients (g/litre): glucose 10.0, NaNO₃ 2.0, KH₂PO₄ 1.0, and CaCO₃ 1.0. The initial pH value of the fermentation medium was adjusted to 7.2. Effects of certain amino acids, organic acids, vitamins, purine and pyrimidine bases on the fermentative production of gentamicins were revealed. The ingredients which increased the antibiotic yields were phenylalanine, isoleucine, lysine, methionine, leucine, arginine, glycine, β′-alanine, cystine, tryptophan, malic acid, maleic acid, cobalamin, folic acid, riboflavin, vitamin B₁, vitamin B₆, biotin, nicotinamide, uracil, adenine, guanine and adenosine. Trace elements (Co, Mo, Fe, Cu, Zn and Mn) exhibited their important role on the biosynthesis and formation of gentamicins by Micromonospora purpurea.     

Optimal Design of Concrete Canal Section for Minimizing Costs of Water Loss,Lining and Earthworks

Canal section design with minimum cost, which can be considered as an objective function, involves minimization of total costs per unit length of the canal, including direct costs of per cubic meter earthworks and per meter canal lining and indirect costs of water losses through canal seepage and evaporation. Since the costs (both direct and indirect) are associated with the canal geometry and dimensions, it is possible to lower them by optimization of the mentioned objective function. For this purpose, some constraints were subjected and considered to solve the problem. Flow discharge, as the main constraint, was considered in addition to the minimum permissible velocity and Froude’s number, as subsidiary constraints. MATLAB programming software was used to demonstrate and run the optimization algorithm. The results finally were illustrated in forms of dimensionless graphs, which simplify the optimum design of canal dimensions with minimum cost per meter length. Comparing the results with other similar studies, however show the importance and role of earthworks and lining costs, as well as including the subsidiary constraints in the optimization process.     

Unsaturated polyesters. II. Structure and properties of polyester resins based on cinnamylsuccinic acid

Unsaturated Polyester resins were prepared by the reaction of cinnamylsuccinic acid with saturated diols, namely, ethylene, diethylene, propylene, dipropylene, tetramethylene, and hexamethylene glycols, and the unsaturated diols, namely, 1,4-butene- and 1,4-butynediols. All the polyester resins obtained have been characterized and were found to cure with styrene, with relatively low conversions. The properties of the cured polyesters in the form of films were determined. IR and ¹H-NMR spectroscopy were used for both qualitative and quantitative analyses of the polyesters and their hydrolyzate products, after curing with styrene.     

Application of myrrh extract as an eco-friendly dye and antimicrobial agent on wool and silk fabrics part 2: antimicrobial activity and fastness property

ABSTRACT

We investigate the dyeing and antimicrobial properties of myrrh (Commiphora molmol) extracts on wool and silk fabrics, the use of eco-friendly materials such as sumac (Rhus coriaria), manjakani (Quercus infectoria), alum, and ferrous sulfate as mordants. The mordanting methods were optimized.

The best conditions of dyeing process were discussed in the first part of this study. Dyed fabrics were assessed for color strength (K/S), color fastness, and antimicrobial activity. Non-mordanted dyed wool and silk showed color fastness of grade 4–5. Dyed fabrics showed good antimicrobial activity, which was enhanced by mordanting.     

Aflatoxin B1, ochratoxin A and zearalenone in sorghum grains marketed in Tunisia

A total of 64 samples of sorghum (37 Tunisian sorghum samples and 27 Egyptian sorghum samples) were collected during 2011–2012 from markets in Tunisia. Samples were analysed for contamination with aflatoxin B1, ochratoxin A and zearalenone by High-Performance Liquid Chromatography Coupled with Fluorescence Detection (HPLC-FLD). Aflatoxin B1 was found in 38 samples in the range 0.03–31.7 µg kg^?1. Ochratoxin A was detected in 24 samples with concentrations ranging from 1.04 to 27.8 µg kg^?1. Zearalenone was detected in 21 samples and the concentration varied between 3.7 and 64.5 µg kg^?1. ANOVA analysis of the influence of the country of origin on the incidence and concentration of mycotoxins in the samples studied showed no significant difference (P > 0.05) between the two batches of samples for each of the three mycotoxins studied. The studied mycotoxins contaminate sorghum and may also co-exist because of the diversity of the mycobiota in this cereal.     

Edge-Localized Modes (ELM) Modification with Transport Barrier Control in Tokamak by Analytical Strategies

High confinement mode (H-mode) in tokamaks is characterized by the formation of a transport barrier at the edge of the plasma. The H-mode increases the plasma energy confinement time by around a factor of two compared to the Low confinement mode (L-mode). This result made a great step towards achieving the higher temperatures and pressures needed to create ignition conditions. The Grad–Shafranov Equation describes the magnetic flux distribution of plasma in an axisymmetric system like a tokamak. In this paper, we have calculated the magnetic flux surfaces in IR-T1 tokamak by two methods. An analytical solution of magnetic surfaces approximated by equilibrium calculation of GS equation based on first three (and then four) terms of expansion in flux function. Results of two methods are in good agreement with each other.     

Silver(I) Polymer of Tripodal Amine: Synthesis,Structure and Photoluminescence

Starting from tripodal ligand tris-(methyl-imidazole) amine (1) the colourless complex tris-(methyl-imidazole)aminesilver(I)perchlorate (2) has been synthesized, characterized by IR, UV/Vis and ¹HNMR spectroscopic studies and finally solid state structure has been established by single crystal X-ray diffraction studies. A single crystal X-ray structure determination revealed the formation of coordination polymer. The crystal structure possesses weak d¹⁰–d¹⁰ ‘argentophilic’ interactions with Ag–Ag separation (3.348 Å). The weak luminance at 375 nm may be this Ag–Ag weak interaction. The molecule possesses weak H-bonding with C2 and C4H of imidazole with oxygen of ClO₄.     

Highly basic CaO nanoparticles in mesoporous carbon materials and their excellent catalytic activity

Highly basic CaO nanoparticles immobilized mesoporous carbon materials (CaO-CMK-3) with different pore diameters have been successfully prepared by using wet-impregnation method. The prepared materials were subjected to extensive characterization studies using sophisticated techniques such as XRD, nitrogen adsorption, HRSEM-EDX, HRTEM and temperature programmed desorption of CO2 (TPD of CO2). The physico-chemical characterization results revealed that these materials possess highly dispersed CaO nanoparticles, excellent nanopores with well-ordered structure, high specific surface area, large specific pore volume, pore diameter and very high basicity. We have also demonstrated that the basicity of the CaO-CMK-3 samples can be controlled by simply varying the amount of CaO loading and pore diameter of the carbon support. The basic catalytic performance of the samples was investigated in the base-catalyzed transesterification of ethylacetoacetate by aryl, aliphatic and cyclic primary alcohols. CMK-3 catalyst with higher CaO loading and larger pore diameter was found to be highly active with higher conversion within a very short reaction time. The activity of 30% CaO-CMK3-150 catalyst for transesterification of ethylacetoacetate using different alcohols increases in the following order: octanol > butanol > cyclohexanol > benzyl alcohol > furfuryl alcohol.