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11.
Being a new kind of nanomaterials, aromatic polyamide nanofibers (ANF) have been much highlighted in recent studies. We here demonstrate an isopropyl alcohol (IPA) accelerated chemical cleavage on poly (p-phenylene terephthalamide) chopped fibers, which provides an efficient preparation method of ANF. The comprehensive study on the processes accelerated by different alcohols revealed that the preparation time of ANF in the mixed medium of dimethyl sulfoxide (DMSO)-alcohol (20:1 in volume) was shorten to 45 min and 75 min for methanol (ethanol) and isopropanol, respectively. However, the nanofibers prepared in DMSO-IPA exhibited the minimum in axial and radial dimensions, providing the finest and most uniform diameter of 16 nm. The corresponding ANF films through vacuum assisted filtration also showed the highest tensile strength of 150 MPa, in comparison with those of the ANF films prepared using other alcohols, which were about 110 MPa. Furthermore, ANF/silicon hybrid films were prepared by the ionic ring-opening reaction followed by the alkoxysilane condensation and nanoparticle fabrication. By changing the organo functional groups in the alkoxysilane, the surface of the films were adjustable in a wide contact angle range from 56° (hydrophilic) to 150° (superhydrophobic), suggesting the amendable interfacial properties potential applicable to composite fabrication with most of the resin matrix.  相似文献   
12.
胡秋  肖刚 《轻合金加工技术》2002,30(7):23-24,12
对冷轧机工作辊由于摩擦力引起的垂直、横向振动作了定性分析,指出了它们的危害,提出了预防措施。  相似文献   
13.
加强对研究生的挫折教育,已成为新时期研究生教育的一项非常重要而迫切的任务。研究生挫折教育的途径主要有:培养研究生树立良好的挫折观;将远大志向与正确、切实的短期目标有机结合;研究生导师要将挫折教育作为自身工作的重要职责和内容;要创设挫折情境,加强实践体验;在研究生中积极开展抗挫互助活动;帮助研究生学会自我调适、自我超越、自我教育。  相似文献   
14.
随着现代信息的蔓延,学校素质教育的全面推进,学校图书馆的地位在不断提高,作用也会逐渐的凸现出来.图书馆是落实素质教育的一个重要阵地,把图书活动作为一个栽体,充分发挥图书馆现有的物质基础,大力开展全校师生的读书活动,形成爱书,读书的良好风尚,使图书馆成为师生最大、最亲近的学习课堂.由此,大力加强和广泛发展高校图书馆的建设,是一项非常重要而迫切的艰巨任务,也是高校图书馆顺应时代发展的必要,这样就要求正确面对管理,加强对图书馆智能化的探究.  相似文献   
15.
嵌入式系统在电子产品中的应用,加快了电子产品更新换代的速度,要想在技术竞争中立于不败之地,唯有加快应用软件开发进程,缩短产品开发周期.模拟器在嵌入式系统应用软件开发中的使用,大大简化了软件调试过程.本文基于μ C/OS-II嵌入式实时操作系统,研究开发出一款利用模拟器进行应用软件开发的多媒体播放器智能菜单,具有很大的实际应用价值,加快了产品的开发速度,增加了产品的核心竞争力.  相似文献   
16.
Testing the equality of proportions for correlated otolaryngologic data   总被引:1,自引:0,他引:1  
In otolaryngologic (or ophthalmologic) studies, each subject usually contributes information for each of two ears (or eyes), and the values from the two ears (or eyes) are generally highly correlated. Statistical procedures that fail to take into account the correlation between responses from two ears could lead to incorrect results. On the other hand, asymptotic procedures that overlook small sample designs, sparse data structures, or the discrete nature of data could yield unacceptably high type I error rates even when the intraclass correlation is taken into consideration. In this article, we investigate eight procedures for testing the equality of proportions in such correlated data. These test procedures will be implemented via the asymptotic and approximate unconditional methods. Our empirical results show that tests based on the approximate unconditional method usually produce empirical type I error rates closer to the pre-chosen nominal level than their asymptotic tests. Amongst these, the approximate unconditional score test performs satisfactorily in general situations and is hence recommended. A data set from an otolaryngologic study is used to illustrate our proposed methods.  相似文献   
17.
Despite the outstanding power conversion efficiency (PCE) of perovskite solar cells (PSCs) achieved over the years, unsatisfactory stability and lead toxicity remain obstacles that limit their competitiveness and large-scale practical deployment. In this study, in situ polymerizing internal encapsulation (IPIE) is developed as a holistic approach to overcome these challenges. The uniform polymer internal package layer constructed by thermally triggered cross-linkable monomers not only solidifies the ionic perovskite crystalline by strong electron-withdrawing/donating chemical sites, but also acts as a water penetration and ion migration barrier to prolong shelf life under harsh environments. The optimized MAPbI3 and FAPbI3 devices with IPIE treatment yield impressive efficiencies of 22.29% and 24.12%, respectively, accompanied by remarkably enhanced environmental and mechanical stabilities. In addition, toxic water-soluble lead leakage is minimized by the synergetic effect of the physical encapsulation wall and chemical chelation conferred by the IPIE. Hence, this strategy provides a feasible route for preparing efficient, stable, and eco-friendly PSCs.  相似文献   
18.
Li-rich layered oxides (LLOs) have been considered as the most promising cathode materials for achieving high energy density Li-ion batteries. However, they suffer from continuous voltage decay during cycling, which seriously shortens the lifespan of the battery in practical applications. This review comprehensively elaborates and summarizes the state-of-the-art of the research in this field. It is started from the proposed mechanism of voltage decay that refers to the phase transition, microscopic defects, and oxygen redox or release. Furthermore, several strategies to mitigate the voltage decay of LLOs from different scales, such as surface modification, elemental doping, regulation of components, control of defect, and morphology design are summarized. Finally, a systematic outlook on the real root of voltage decay is provided, and more importantly, a potential solution to voltage recovery from electrochemistry. Based on this progress, some effective strategies with multiple scales will be feasible to create the conditions for their commercialization in the future.  相似文献   
19.
Li  Shuang  Li  Wenjing  Wang  Zhehe  An  Dongdong 《Mobile Networks and Applications》2022,27(4):1397-1407
Mobile Networks and Applications - Artificial fish swarm algorithm (AFS) is used in the field of function optimization problems widely. The traditional AFS algorithm has some problems such as long...  相似文献   
20.
Xie  Jun  Zhang  Jianwei  Liu  Shuang  Chen  Guohua 《The Journal of supercomputing》2022,78(3):3500-3516
The Journal of Supercomputing - This study was to evaluate the performance of magnetic resonance imaging (MRI) reconstruction algorithm based on convolutional neural network (CNN) in the diagnosis...  相似文献   
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