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排序方式: 共有578条查询结果,搜索用时 15 毫秒
101.
Noriyuki Hara Shuichi Nakamura Yasuhiro Funahashi Norio Shibata 《Advanced Synthesis \u0026amp; Catalysis》2011,353(16):2976-2980
The organocatalytic enantioselective decarboxylative addition of malonic acids half thioesters to isatins using a squaramide catalyst afforded the products with high enantioselectivity. These products are key intermediates in the synthesis of 3‐substituted 3‐hydroxy‐2‐oxindole derivatives. The first enantioselective synthesis of (−)‐flustraminol B has been accomplished. 相似文献
102.
Simultaneous B-M-mode scanning method for real-time full-range Fourier domain optical coherence tomography 总被引:1,自引:0,他引:1
High-speed complex full-range Fourier domain optical coherence tomography (FD-OCT) is demonstrated. In this FD-OCT, the phase modulation of a reference beam (M scan) and transversal scanning (B scan) are simultaneously performed. The Fourier transform method is applied along the direction of the B scan to reconstruct complex spectra, and the complex spectra comprise a full-range OCT image. Because of this simultaneous B-M-mode scan, the FD-OCT requires only a single A scan for each single transversal position to obtain a full-range FD-OCT image. A simple but slow version of the FD-OCT visualizes the cross section of a plastic plate. A modified fast version of this FD-OCT investigates a sweat duct in a finger pad in vivo and visualizes it with an acquisition time of 27 ms. 相似文献
103.
Yazan Al-ZainYosuke Sato Hee Young Kim Hideki HosodaTae Hyun Nam Shuichi Miyazaki 《Acta Materialia》2012,60(5):2437-2447
The effect of room temperature (RT) aging on the superelasticity of Ti-Nb-Mo-based superelastic alloys is investigated. The results show that annealing at relatively low temperatures such as 973 K after severe cold rolling results in poor resistance to the effect of RT aging. The transformation stress increases considerably due to the formation of an isothermal ω phase at RT. Addition of Sn is partially effective in suppressing the RT aging effect in the specimens annealed at 973 K. The RT aging effect is suppressed by increasing the annealing temperature, due to the annihilation of lattice defects or non-equilibrium vacancies introduced during cold rolling, which are responsible for accelerating the diffusion process, however, superelasticity is reduced by annealing at higher temperatures, due to a decrease in the critical stress for slip deformation (σCSS). The specimen annealed at 1173 K followed by aging at 773 K exhibits stable superelasticity with a high resistance to the effect of RT aging. Annealing at 1173 K causes the annihilation of lattice defects or non-equilibrium vacancies, while aging at 773 K induces precipitation of the α phase, which in turn causes an increase in σCSS, and further enhances the resistance to the RT aging effect by enriching the matrix with β-stabilizing elements. 相似文献
104.
Sung‐Jin Kim David Lai Joong Yull Park Ryuji Yokokawa Shuichi Takayama 《Small (Weinheim an der Bergstrasse, Germany)》2012,8(19):2925-2934
This paper gives an overview of elastomeric valve‐ and droplet‐based microfluidic systems designed to minimize the need of external pressure to control fluid flow. This Concept article introduces the working principle of representative components in these devices along with relevant biochemical applications. This is followed by providing a perspective on the roles of different microfluidic valves and systems through comparison of their similarities and differences with transistors (valves) and systems in microelectronics. Despite some physical limitation of drawing analogies from electronic circuits, automated microfluidic circuit design can gain insights from electronic circuits to minimize external control units, while implementing high‐complexity and high‐throughput analysis. 相似文献
105.
Taigo Onodera Shuichi SuzukiTakaaki Mizukami Hisao Kanzaki 《Journal of power sources》2011,196(19):7994-7999
An improved synthesis scheme of non-precious metal N-doped carbon catalysts for oxygen reduction reaction is reported. The non-precious metal N-doped carbon catalysts were prepared by pyrolysis of the mixture (phenol resin, Ketjen black carbon support and cobalt phenanthroline complex). The drastic improvement of distribution state of Ketjen black supported non-precious metal N-doped carbon catalysts was observed by means of transmission electron microscopy (TEM). In addition, the non-precious metal N-doped carbon catalyst synthesized with Ketjen black carbon support showed much higher oxygen reduction reaction (ORR) activity relative to unsupported non-precious metal N-doped carbon catalyst in O2-saturated 0.5 mol l−1 H2SO4 at 35 °C. Moreover, the highest ORR activity was obtained with addition of optimum amount of Ketjen black carbon support was thirtyfold compared to unsupported non-precious metal N-doped carbon catalyst at 0.7 V. Similarly, the performance of a polymer electrolyte fuel cell (PEFC) using the non-precious metal N-doped carbon catalyst as the cathode electrode catalyst was obviously better than that of the non-precious metal N-doped carbon catalyst before optimization. Microstructure, specific surface area and surface composition of the non-precious metal N-doped carbon catalysts were analyzed by XRD, XPS and BET measurement with nitrogen physisorption, respectively. 相似文献
106.
A field survey on energy consumption by hot water supply and cooking was conducted in two cities in China, Nanjing, and Hefei. In each city, 5 housing complexes were selected, and approximately 100 or 200 residential units were selected from each of them. The following items were surveyed: (1) fundamental information, such as number of family members, data on residents, etc., (2) bathing style, and (3) frequency of cooking and cooking time. Most of the residents take showers seven times a week in the summer, but less frequently in the winter. In contrast, the frequency of taking baths increases to several times a week during the winter, compared with 0 or 1 times a week in the summer. These results differ slightly depending on the heating and cooling systems used in the houses. The frequency with which people cook in their own houses ranges from 4 to 7 times a week, which means that “eating out” is relatively frequent, although the result differs significantly among the housing complexes. Distribution of the cooking time has usually two peaks at 20 to 30 min and 50 to 60 min (or 30 to 40 min and longer than 60 min) for lunch and dinner, respectively. The high energy consumption for cooking might be due to the long cooking time. 相似文献
107.
Shin Kajita Naoaki Yoshida Reiko Yoshihara Noriyasu Ohno Takanori Yokochi Masayuki Tokitani Shuichi Takamura 《Journal of Nuclear Materials》2012,421(1-3):22-27
Helium plasma irradiation and electron heating experiments were conducted using tungsten in the divertor simulator NAGDIS-II. Helium plasma irradiation to tungsten led to the formation of nanostructures on the surface, while the nanostructures were annihilated after the potential of the specimen was changed to positive for several 10 min so that electrons irradiated the sample without ion irradiation. The specimens were analyzed in detail by transmission electron microscope with the help of focused ion beam technique. It is revealed that the helium nano-bubbles still remained even after the nanostructures were disappeared from the surface. Porosity of the nanostructured tungsten was measured from the TEM images. 相似文献
108.
The performance of a conventional parallel application is often degraded by load‐imbalance on heterogeneous clusters. Although it is simple to invoke multiple processes on fast processing elements to alleviate load‐imbalance, the optimal process allocation is not obvious. Kishimoto and Ichikawa presented performance models for high‐performance Linpack (HPL), with which the sub‐optimal configurations of heterogeneous clusters were actually estimated. Their results on HPL are encouraging, whereas their approach is not yet verified with other applications. This study presents some enhancements of Kishimoto's scheme, which are evaluated with four typical scientific applications: computational fluid dynamics (CFD), finite‐element method (FEM), HPL (linear algebraic system), and fast Fourier transform (FFT). According to our experiments, our new models (NP‐T models) are superior to Kishimoto's models, particularly when the non‐negative least squares method is used for parameter extraction. The average errors of the derived models were 0.2% for the CFD benchmark, 2% for the FEM benchmark, 1% for HPL, and 28% for the FFT benchmark. This study also emphasizes the importance of predictability in clusters, listing practical examples derived from our study. Copyright © 2008 John Wiley & Sons, Ltd. 相似文献
109.
Abstract A numerical study is performed to investigate heat transfer and fluid flow in the entrance and fully developed regions of an annulus, consisting of a rotating, insulated inner cylinder and a stationary, heated outer cylinder. Several different k-ε turbulence models are employed to determine the turbulent kinetic energy, its dissipation rate, and the heat transfer performance. The governing boundary layer equations are discretized by means of a control volume finite difference technique and numerically solved using the marching procedure. In the entrance region the axial rotation of the inner cylinder induces a thermal development and causes an increase in both the Nusselt number and the turbulent kinetic energy in the inner cylinder wall region. In the fully developed region, an increase in the Taylor number causes an amplification of the turbulent kinetic energy over the whole cross section, resulting in a substantial enhancement in the Nusselt number. These transport phenomena are also affected by the radius ratio and Reynolds number. 相似文献
110.