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11.
Quantitation of Cefaclor in Pharmaceutical Dosage Forms Using High Performance Liquid Chromatography
Mary Mathew V. Das Gupta Charlie Bethea 《Drug development and industrial pharmacy》1993,19(14):1723-1729
A stability-indicating high-performance liquid chromatography for the quantitation of cefaclor in pharmaceutical dosage forms has been developed. The method is accurate and precise with a percent relative standard deviation of 1.2 based on 5 readings. A number of inactive ingredients present in the capsules and suspensions did not interfere with the assay procedure. The extraction procedure from the dosage forms is very simple. The recovery from the synthetic mixtures was quantitative. The capsules which had expired 3 years ago lost only 3% of the potency. The drug appears to be very sensitive to strong acids or bases since a 5 minute boiling caused 100% degradation of drug in both the solutions. 相似文献
12.
Reconstruction of an original continuous curve and the estimation of its parameters from the digitized version of the curve
is a challenging problem, as quantization always causes some loss of information. In this paper, we have developed a scheme
for reconstruction which is applicable to a class of curves having at the most two parameters. The class of curves for which
the scheme works has also been characterized. We have shown that for one-parameter curves the exact domain of values of the
parameter can be obtained. But in the two-parameter case, only the smallest rectangle containing the domain can be realised.
The distinctive feature of our scheme is that it provides a unified approach to solve the reconstruction and the domain-finding
problem for a class of curves. 相似文献
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Sidhartha R. Das Basheer M. Khumawala 《International Journal of Flexible Manufacturing Systems》1991,3(2):121-147
Flexible manufacturing systems (FMSs) are a class of automated systems that can be used to improve productivity in batch manufacturing. Four stages of decision making have been defined for an FMS—the design, planning, scheduling, and control stages. This research focuses on the planning stage, and specifically in the area of scheduling batches of parts through the system.The literature to date on the FMS planning stage has mostly focused on the machine grouping, tool loading, and parttype selection problems. Our research carries the literature a step further by addressing the problem of scheduling batches of parts. Due to the use of serial-access material-handling systems in many FMSs, the batch-scheduling problem is modeled for a flexible flow system (FFS). This model explicitly accounts for setup times between batches that are dependent on their processing sequence.A heuristic procedure is developed for this batch-scheduling problem—the Maximum Savings (MS) heuristic. The MS heuristic is based upon the savings in time associated with a particular sequence and selecting the one with the maximum savings. It uses a two-phase method, with the savings being calculated in phase I, while a branch-and-bound procedure is employed to seek the best heuristic solution in phase II. Extensive computational results are provided for a wide variety of problems. The results show that the MS heuristic provides good-quality solutions. 相似文献
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Ankur Das Rahul Caprihan 《The International Journal of Advanced Manufacturing Technology》2008,38(11-12):1098-1113
Manufacturing flexibility is a difficult to quantify concept that defies universal definition. This paper presents a novel fuzzy-logic approach for measuring manufacturing flexibility that exploits linguistic variables for quantifying pertinent factors affecting commonly utilized flexibility types. Towards this end, we identify and measure the contribution of specified state variables towards the assumed flexibility types in order to compute an overall flexibility index for a generic manufacturing system. The suggested framework provides a convenient end user approach amenable to software implementation that is exemplified through the development of a prototypical software tool called “Flexibility Evaluator”. 相似文献
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A simple method (based on Floquet theory) for obtaining the characteristic equation (and hence stability) of periodic discrete-time systems is presented. Using this method it is shown that 2-periodic controllers can be used to relocate the zeros of SISO plants. Some examples are considered to illustrate the use of 2-periodic controllers for robust control of finite gain margin problems 相似文献
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