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Vilma Sanhueza Leopoldo Lpez‐Escobar Ursula Kelm Ruby Cid 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2006,81(4):614-617
Mesoporous materials were obtained from two natural silica sources, diatomite and pumicite, under hydrothermal conditions, autogenic pressure and in presence of the surfactant cetyltrimethylammonium bromide (CTAB) as the template. Using diatomite, a temperature of 383 K and the following molar ratios in the initial reaction gel: SiO2/Al2O3 = 8.86; CTAB/SiO2 = 0.1; Na2O/SiO2 = 0.10–0.25 and H2O/Na2O = 250–300, the mesoporous material MCM‐41 was obtained in a reaction time of 48 h. When pumicite was used, a mesoporous material was obtained in a reaction time of 96 h, a reaction temperature of 423 K and an initial reaction gel with the following molar ratios: SiO2/Al2O3 = 8.86; CTAB/SiO2 = 0.1; Na2O/SiO2 = 0.25 and H2O/Na2O = 330. Copyright © 2006 Society of Chemical Industry 相似文献
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A Monge A López de Ceráin O Ezpeleta H Cerecetto E Dias R Di Maio M González S Onetto G Seoane L Suescun R Mariezcurrena 《Canadian Metallurgical Quarterly》1998,53(11):758-764
A role of psychic stress in precipitating hyperthyroid Graves' disease has been suggested, but the evidence in support of this pathogenetic mechanism is conflicting. In this study we investigated the possible occurrence of Graves' disease in patients with panic disorder, a psychiatric condition characterized by recurrent endogenous stress. The study group included 87 consecutive patients suffering from panic disorder since 1 to 30 years: 17 males (mean age 31.3, range 26-43 years) and 70 females (mean age 37.6, range 15-73 years). Two hundred and sixty-two normal subjects with no present or past history of psychiatric disorder served as controls. Patients were submitted to a full evaluation of the thyroid that included physical examination, assays for free thyroid hormones, TSH, thyroglobulin (TgAb), thyroperoxidase (TPOAb) and TSH receptor (TRAb) antibodies, and thyroid echography. The prevalence of circulating TgAb and/or TPOAb in patients with panic disorder did not differ from that in the control group. Twelve patients with panic disorder (13.7%) had circulating TgAb and/or TPOAb, but none had TRAb. Three out of 12 patients with thyroid antibodies, indicating a genetic susceptibility to autoimmune thyroid disease, had a family history of clinical thyroid autoimmunity, and 4 of them had a hypoechogenic pattern of the thyroid at ultrasound suggesting autoimmune thyroiditis. None of the patients with panic disorder had a previous history of hyperthyroidism. On examination, clinical hyperthyroidism or endocrine ophthalmopathy were not found in any of them. A small goiter was appreciated by palpation in 16 patients (18.3%). Free thyroid hormones and TSH were within the normal range in all patients but one: a 55-year old lady with normal serum free thyroid hormones and undetectable TSH. During an 18-month follow-up she did not develop hyperthyroidism and her TSH spontaneously returned in the normal range. Considering the individual duration of panic disorder, evidence for previous or present Graves' hyperthyroidism was not found for a total of 478 patient-years of exposure to recurrent endogenous stress in the whole study group, and for a total of 39 patient-years in patients with a genetic susceptibility to autoimmune thyroid disease. In conclusion, we found that recurrent endogenous stress did not precipitate Graves' hyperthyroidism in a series of 87 patients with panic disorder, encompassing a total of 478 patient-years of exposure to stress. Failure to activate the hypothalamic-pituitary-adrenal axis by endogenous stress due to panic disorder as opposed to exogenous stress due to life-events might explain why panic disorder does not precipitate Graves' hyperthyroidism. 相似文献
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Nieke Michael Sampaio Gabriela Thm Thomas Seidl Christoph Teixeira Leopoldo Schaefer Ina 《Software and Systems Modeling》2022,21(1):225-247
Software and Systems Modeling - A product line is an approach for systematically managing configuration options of customizable systems, usually by means of features. Products are generated for... 相似文献
26.
Francesco dell’Isola Massimo Cuomo Leopoldo Greco Alessandro Della Corte 《Journal of Engineering Mathematics》2017,103(1):127-157
We consider a bi-dimensional sheet consisting of two orthogonal families of inextensible fibres. Using the representation due to Rivlin and Pipkin for admissible placements, i.e. placements preserving the lengths of the inextensible fibres, we numerically simulate a standard bias extension test on the sheet, solving a non-linear constrained optimization problem. Several first and second gradient deformation energy models are considered, depending on the shear angle between the fibres and on its gradient, and the results obtained are compared. The proposed numerical simulations will be helpful in designing a systematic experimental campaign aimed at characterizing the internal energy for physical realizations of the ideal pantographic structure presented in this paper. 相似文献
27.
Spline Based Pseudo‐Inversion of Sampled Data Non‐Minimum Phase Systems for an Almost Exact Output Tracking 下载免费PDF全文
This paper considers the problem of achieving a very accurate tracking of a pre‐specified desired output trajectory , for linear, multiple input multiple output, non‐minimum phase and/or non hyperbolic, sampled data, and closed loop control systems. The proposed approach is situated in the general framework of model stable inversion and introduces significant novelties with the purpose of reducing some theoretical and numerical limitations inherent in the methods usually proposed. In particular, the new method does not require either a preactuation or null initial conditions of the system. The desired and the corresponding sought input are partitioned in a transient component ( and ut(k), respectively) and steady‐state ( and us(k), respectively). The desired transient component is freely assigned without requiring it to be null over an initial time interval. This drastically reduces the total settling time. The structure of ut(k) is a priori assumed to be given by a sampled smoothing spline function. The spline coefficients are determined as the least‐squares solution of the over‐determined system of linear equations obtained imposing that the sampled spline function assumed as reference input yield the desired output over a properly defined transient interval. The steady‐state input us(k) is directly analytically computed exploiting the steady‐state output response expressions for inputs belonging to the same set of . 相似文献
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Control of Switching Modes and Conductance Quantization in Oxygen Engineered HfOx based Memristive Devices 下载免费PDF全文
Sankaramangalam Ulhas Sharath Stefan Vogel Leopoldo Molina‐Luna Erwin Hildebrandt Christian Wenger Jose Kurian Michael Duerrschnabel Tore Niermann Gang Niu Pauline Calka Michael Lehmann Hans‐Joachim Kleebe Thomas Schroeder Lambert Alff 《Advanced functional materials》2017,27(32)
Hafnium oxide (HfOx)‐based memristive devices have tremendous potential as nonvolatile resistive random access memory (RRAM) and in neuromorphic electronics. Despite its seemingly simple two‐terminal structure, a myriad of RRAM devices reported in the rapidly growing literature exhibit rather complex resistive switching behaviors. Using Pt/HfOx/TiN‐based metal–insulator–metal structures as model systems, it is shown that a well‐controlled oxygen stoichiometry governs the filament formation and the occurrence of multiple switching modes. The oxygen vacancy concentration is found to be the key factor in manipulating the balance between electric field and Joule heating during formation, rupture (reset), and reformation (set) of the conductive filaments in the dielectric. In addition, the engineering of oxygen vacancies stabilizes atomic size filament constrictions exhibiting integer and half‐integer conductance quantization at room temperature during set and reset. Identifying the materials conditions of different switching modes and conductance quantization contributes to a unified switching model correlating structural and functional properties of RRAM materials. The possibility to engineer the oxygen stoichiometry in HfOx will allow creating quantum point contacts with multiple conductance quanta as a first step toward multilevel memristive quantum devices. 相似文献
30.
Multilayer lead‐free piezoceramic composites: Influence of co‐firing on microstructure and electromechanical behavior 下载免费PDF全文
Azatuhi Ayrikyan Florian Weyland Sebastian Steiner Michael Duerrschnabel Leopoldo Molina‐Luna Jurij Koruza Kyle G. Webber 《Journal of the American Ceramic Society》2017,100(8):3673-3683
In this study lead‐free 2‐2 and 0‐3 ceramic/ceramic composites comprised of the non‐ergodic relaxor 0.93(Bi1/2Na1/2)TiO3–0.07BaTiO3 and ergodic relaxor 0.94Bi0.5(Na0.75K0.25)0.5TiO3–0.06BiAlO3 were investigated. The macroscopic electromechanical behavior was characterized as a function of continuent content, revealing an enhancement in the unipolar strain from the multilayer composite structure. Systematic evaluation of the effects of co‐sintering on microstructural properties, such as grain size and porosity, revealed potential mechanisms by which the increase in unipolar strain was achieved. In addition, interdiffusion between the constituents was observed, providing evidence for the formation of a functionally graded ceramic by co‐sintering. These data are contrasted with high‐resolution energy dispersive X‐ray microanalysis for measurement of chemical composition across the interface of 2‐2 ceramics. These findings provide insight into how synthesis routes can be optimized for tailoring the enhancement of electromechanical properties of lead‐free electroceramic composite systems. 相似文献