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31.
This paper further illustrates the applicability of multiple internal reflectance infrared spectroscopy to the analysis of near-surface photooxidation. The results are compared with transmission infrared spectra to evaluate compositional gradients resulting from photooxidation and the influence of oxygen diffusion. The sample was a solvent-cast film of atactic, narrow distribution polystyrene, Mw of 100,000, that had been drawn to a ratio of 3.0 at 110°C by solid state coextrusion. Irradiation of these thin films, ~25μm thickness, was performed on exposure to air at 35°C for periods of up to 6 h using a mercury source emitting at 254 nm. On photooxidation, a board peak appears at 3200–3500 cm?1, attributable to hydroperoxide formation. The most dramatic increase in the infrared spectra is found for a carbonyl band at 1730 cm?1. It appears to result from an aromatic acid group since it is shifted to 1660 cm?1 on immersion of the oxidized polystyrene films in aqueous ammonium hydroxide. It is confirmed that the photooxidation of polystyrene occurs preferentially at the surface and that this reaction rate is greatly reduced in the drawn polystyrene film. 相似文献
32.
Poly(p-tert-butoxycarbonyloxystyrene): a convenient precursor to p-hydroxystyrene resins 总被引:1,自引:0,他引:1
An efficient synthetic route to pure, high molecular weight poly(p-hydroxystyrene) is reported. The route involves synthesis of a new monomer, p-tert-butoxycarbonyloxystyrene, polymerization by radical initiation or by cationic initiation in liquid SO2, followed by thermolysis or acidolysis of the tert-butoxycarbonyl protecting group. Porous, crosslinked resin beads containing the nucleophilic, phenol pendant group have been prepared in a similar fashion from the precursor terpolymer of p-tert-butoxycarbonyloxystyrene, styrene and divinylbenzene. The utility of this resin for solid-phase synthesis has been demonstrated. 相似文献
33.
This study was undertaken to elucidate the state of a polymer in the amorphous state through a change of motion of the molecular chain caused by heat treatment below the glass transition temperature. From dielectric measurements of amorphous poly(ethylene terephthalate) heat-treated below Tg, it was found that the average relaxation time, the distribution of relaxation time and the dielectric strength increase with increase of heat treatment. From these results, it was concluded that the amorphous state becomes more random by heat treatment. 相似文献
34.
Taisuke Ito 《Polymer》1982,23(10):1412-1434
Results for the compressibilities of a wide range of polymer crystals along the fibre- and the transverse crystal axes are presented. Good agreement is found between the theoretical and the experimental results of different authors. 相似文献
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38.
Set-based particle swarm optimization (S-PSO) operates on discrete space. S-PSO can solve combinatorial optimization problem with high quality and is successful to apply to the large-scale problem. In S-PSO, a velocity is a set with possibility and a position is a candidate solution. In this paper, we present a novel algorithm of set-based particle swarm optimization with status memory (S-PSOSM) to decide the position based on the previous position for solving knapsack problem. Some operators are redefined for S-PSOSM. S-PSOSM is a simple algorithm because the state of probability reduces. In addition, the weight of S-PSOSM is discussed. S-PSOSM shows high qualities in experimental results. 相似文献
39.
Yasuhiro Jimbo Yuki Tamatsukuri Minato Ito Kohei Yokoyama Yoshiharu Hirakata Shunpei Yamazaki 《Journal of the Society for Information Display》2015,23(7):313-318
To improve the reliability and mechanical durability of a flexible organic light‐emitting diode display, the entire flexible display is coated with an aluminum oxide film by atomic layer deposition (ALD). Because the step coverage of ALD is excellent, the AlOx film was deposited not only on the front and back surfaces but also on the side surfaces of the display. A high‐temperature and high‐humidity preservation test, repetitive bending tests, and a pencil hardness test were conducted on the flexible display with ALD‐AlOx coating. The display survived 500 h of a 65°C, 95% preservation test, endured a 100,000‐time repetitive bending test with a curvature radius of 4 mm, and was found to have a pencil hardness of 4H. 相似文献
40.
Recently, various robots with many degrees of freedom, such as rescue robots and domestic robots, have been developed and
used in practical applications. It is difficult to control such robots autonomously in real environments, because in order
to control the many degrees of freedom, we have to observe many states, calculate huge amounts of information, and operate
many actuators. In this study, we consider a flexible robot without sensors or controllers that can determine the inclination
of a slope and climb up the slope. In order to demonstrate the effectiveness of the proposed framework, we have developed
a prototype robot and conducted experiments. The result indicates that the robot could determine the inclination and climb
up a gentle slope autonomously. Thus, we have realized an autonomous robot that has no explicit sensors or controllers. 相似文献