基于Web服务的数字化校园统一身份认证系统研究

通过对数字化校园网络应用传统统一身份认证和资源访问控制机制不足之处的分析,提出了一种基于Web服务的统一身份认证系统模型,并采用基于票据的集中式架构,以跨域Cookie共享为核心来完成用户的登录、认证和权限控制。实例证明,此方案可以方便的将分散网络节点加入认证体系,完成网络节点单点登录和资源访问控制问题。     

基于设计决定的逐步求精方法及环境

逐步描述、变换及证明的软件开发过程包含两个转换,一是从非形式的用户需求到形式描述,一是从形式描述到算法实现。开发过程中的关键是如何做出设计决定。为了更好地维护、重用软件以及程序证明,不仅仅要对软件的形式描述及实现做文档记录,也要记下开发过程中所做的每一步决定。我 们用两个例子来说明如上这种逐步求精的方法以及设计决定在其中所起的作用,并且我们实现了一个包括SPEC、OOMM、PROT、VERI几个子系统组成的环境来支持上述过程。     

Rapid growth of angle-confined large-domain graphene bicrystals

In the chemical vapor deposition growth of large-area graphene polycrystalline thin films,the coalescence of randomly oriented graphene domains results in a high density of uncertain grain boundaries (GBs).The structures and properties of various GBs are highly dependent on the misorientation angles between the graphene domains,which can significantly affect the performance of the graphene films and impede their industrial applications.Graphene bicrystals with a specific type of GB can be synthesized via the controllable growth of graphene domains with a predefined lattice orientation.Although the bicrystal has been widely investigated for traditional bulk materials,no successful synthesis strategy has been presented for growing two-dimensional graphene bicrystals.In this study, we demonstrate a simple approach for growing well-aligned large-domain graphene bicrystals with a confined tilt angle of 30° on a facilely recrystallized single-crystal Cu (100) substrate.Control of the density of the GBs with a misorientation angle of 30° was realized via the controllable rapid growth of subcentimeter graphene domains with the assistance of a cooperative catalytic surface-passivation treatment.The large-area production of graphene bicrystals consisting of the sole specific GBs with a tunable density provides a new material platform for fundamental studies and practical applications.     

Fe-C-N合金板条马氏体的组织构成

采用适射电子显微镜对五种Fc—C—N合金的板条马氏体的束内和束界区进行详细的观察和分析。研究发现板条马氏体组织中存在填塞马氏体。板条马氏体组织是由一簇簇平行排列的大小板条,以及填充在马氏体板条间,束界和界隅内的不定外形的填塞马氏体和条间残余奥氏体薄膜或膜片所构成。     

Sn及其氧化物超微粉的制备与测试

本文采用气体蒸发法制备出粒度不到５ｎｍ的Ｓｎ及其氧化物的超微粉。利用热重，差热分析和Ｘ射线衍射谱等测试方法研究了热处理制度对其粒度，成份和气敏特性的影响，发现了ＳｎＯ_２正交相的存在。     

SUPERPLASTIC FORMING WITH DIFFUSION BONDING(SPF/DB)OF ALUMINIUM ALLOYS

铝合金的超塑成形和扩散焊接组合工艺(SPF/DB)在工程制造领域里具有巨大的潜在应用价值,在国际上很受重视。本文简要介绍了SPF/DB 的发展状况、工艺特点和应用前景,着重对这一工艺的难点—铝合金的扩散焊接工艺和理论问题进行了综述评论,提出了一些讨论性意见。     

炼厂气脱硫系统的流程设置

分别介绍了炼厂气脱硫化氢装置的一般流程、多脱硫系统脱硫化氢流程、先进模式的炼油厂脱硫化氢系统,分析了这些流程的特点和适用场合,指出为降低投资,节省操作费用,减小操作难度,在新建或大规模扩建的炼油厂中,应采用先进模式的炼油厂脱硫化氢系统.     

Influence of the copper ion on aging rate of oil-paper insulation in a power transformer

To identify the influence of copper ion on the aging rate of oil-paper insulation, accelerated thermal aging experiments on oil-paper insulation were designed and performed at two significant temperatures. A set of characteristic parameters, including dissolved gases, degree of polymerisation, furfural content, water content and acid number of oil, was tested. The experiments- results reveal that copper ion has a different influence on insulation paper and oil during the aging process of the insulation system. On the one hand, it delays the degradation of insulation paper, reducing the ratio of CO₂/CO by about 11% at 80%C and by more than 50% at 130%C. On the other hand, copper ion promotes the oxidation of oil and thus accelerates the aging rate.     

Ultrasensitive aptamer-based multiplexed electrochemical detection by coupling distinguishable signal tags with catalytic recycling of DNase I

This work reports an aptamer-based, disposable, and multiplexed sensing platform for simultaneous electrochemical determination of small molecules, employing adenosine triphosphate (ATP) and cocaine as the model target analytes. The multiplexed sensing strategy is based on target-induced release of distinguishable redox tag-conjugated aptamers from a magnetic graphene platform. The electronic signal of the aptasensors could be further amplified by coupling DNase I with catalytic recycling of self-produced reactants. The assay was based on the change in the current at the various peak potentials in the presence of the corresponding signal tags. Experimental results revealed that the multiplexed electrochemical aptasensor enabled the simultaneous monitoring of ATP and cocaine in a single run with wide working ranges and low detection limits (LODs: 0.1 pM for ATP and 1.5 pM for cocaine). This concept offers promise for rapid, simple, and cost-effective analysis of biological samples.