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排序方式: 共有844条查询结果,搜索用时 15 毫秒
91.
溶胀动力学方法测定高分子链结构 总被引:2,自引:0,他引:2
本文成功地用溶胀动力学方法测定了交联、线型及支化高分子的溶胀特征曲线,并认为可由这种溶动力学探针技术判别高分子链的结构类型及特征,是一个很有特色的研究方法。 相似文献
92.
This paper reports both experimental and numerical investigations on delamination mechanisms in [05, 905, 05] carbon fiber(CF)/poly(etheretherketone) (PEEK) laminate subjected to low-velocity impact. It was found that the CF/PEEK composite exhibits the same damage mechanisms as epoxy-based composites, but superior delamination resistance. For the crossply laminate, the impact delamination results from a Mode II interlaminar fracture process, and a close association exists between the interlaminar shear stress field and the delamination growth. The prediction of impact-induced delamination sizes is discussed. 相似文献
93.
D Desaulniers R Poon W Phan K Leingartner WG Foster I Chu 《Canadian Metallurgical Quarterly》1997,13(5):627-638
It has been reported that suramin, an anthelminthic, trypanocidal agent and an inhibitor of P2 receptors, may antagonise N-methyl-D-aspartate (NMDA) subtype of the excitatory amino acid receptors. Both NMDA receptors and P2X subclass of P2 receptors are ligand-gated Ca2+-selective channels and, since the increased influx of Ca2+ into neurons has been linked to neurotoxicity, simultaneous inhibition of P2X and NMDA receptors in vivo by suramin could represent an effective neuroprotective treatment. We have found that suramin inhibited the binding of [3H]CGP 39653 to NMDA receptor binding sites in vitro and reduced the frequency of NMDA channel openings in patch-clamp studies. Suramin (1 mM) had no effect on [3H]kainate binding in vitro. In vivo, intracerebroventricular (I.C.V.) injections of suramin (70 nmol/brain) antagonised convulsive effects of the NMDA agonist (RS)-(tetrazol-5-yl)-glycine (TZG, LY 285265). Suramin, however, did not prevent neurotoxic lesions in the hippocampus caused by I.C.V. administration of TZG. Increasing the dose of suramin resulted in death from severe respiratory depression. 相似文献
94.
In a wireless mobile client-server environment, a mobile user may voluntarily disconnect itself from the Web server to save its battery life and avoid high communication prices. To allow Web pages to be updated while the mobile user is disconnected from the Web server, updates can be staged in the mobile host and propagated back to the Web server upon reconnection. In this paper, we analyze algorithms for supporting disconnected write operations for wireless Web access and develop a performance model to identify the optimal length of the disconnection period under which the cost of update propagation is minimized. The analysis result is particularly applicable to Web applications which allow wireless mobile users to modify Web contents while on the move. We show how the result can be applied to real-time Web applications such that the mobile user can determine the longest disconnection period such that it can still propagate updates to the server before the deadline so that a minimum communication cost is incurred. 相似文献
95.
炭黑添加剂对活性炭纤维中孔率的影响 总被引:8,自引:1,他引:7
纺制含炭黑的聚丙烯腈原丝,经预氧化,炭化,活化制得了中孔含量较高的活性炭纤维,考察了炭黑种类,含量及预氧化,炭化,活化地活性炭纤维孔结构的影响,并对成孔机理进行了探索。 相似文献
96.
Nguyen Thu Nhan Pham Khac Hung Do Minh Nghiep Tran Quoc Thang Hyoung Seop Kim 《Metals and Materials International》2006,12(2):167-172
Microscopic features of liquid and amorphous alumina (Al2O3) were simulated by molecular dynamics calculations. The simulations were performed in an orthorhombic cell with 3000 particles using the Born-Mayer potential at temperatures of 0, 2500, 2700, and 3000 K under constant pressure. It was found that a large cluster of pores contained several thousand spherical pores, which were formed with radii larger than 0.73 Å. The observed variations of Al2O3 structures with atomic arrangements of AlOx (x=3, 4, 5, and 6) are discussed. 相似文献
97.
Ha Tran Nguyen Le-Thu T. Nguyen Trung Thanh Nguyen Anh Tuan Luu Thang Van Le 《Journal of Polymer Research》2014,21(9):1-11
Novel 3-hexylthiophene-based hyperbranched conjugated polymers containing triphenylamine and benzo [c] [1, 2, 5] thiadiazole moieties were synthesized by Suzuki coupling polymerization of tris (4-bromophenyl) amine, 2,2′-(3-hexylthiophene-2,5-diyl) bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane) and 4,7-dibromobenzo [c] [1, 2, 5] thiadiazole. Organic solvent-soluble polymers with number-average molecular weights of 24,000 and 42,000 g/mol were obtained in 54–57 % yields. Their structures, molecular weights and thermal properties were characterized via proton nuclear magnetic resonance (1H NMR) and Fourier transform infrared (FT-IR) spectroscopies, gel permeation chromatography (GPC), thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) and wide-angle powder X-ray diffraction (XRD) measurements. Optical investigation by UV–vis and fluorescence spectroscopies revealed that the incorporation of the benzo [c] [1, 2, 5] thiadiazole moiety in the hyperbranched polymer structure resulted in a red-shift of the maximum absorption wavelength and an increase in the solution-photoluminescence quantum yield, indicating an extension of the conjugation length. The UV–vis, DSC and XRD results demonstrated that the aggregation of conjugated polymer chains could effectively be reduced by the hyperbranched structures and that conjugation length extension via the introduction of benzo [c] [1, 2, 5] thiadiazole units led to the coexistence of both crystalline and amorphous phases in the solid state and in solution upon addition of a non-solvent. 相似文献
98.
Ngoc Kim Pham Do Trung Nguyen Bang Tam Thi Dao Kieu Hanh Thi Ta Vinh Cao Tran Van Hieu Nguyen Sang Sub Kim Shinya Maenosono Thang Bach Phan 《Journal of Electronic Materials》2014,43(7):2747-2753
We have investigated the switching behavior of as-deposited CrO x and post-annealed CrO y films by use of a variety of electrodes (top electrode Ag, Ti; bottom electrode Pt, fluorine tin oxide (FTO)). Resistance switching is highly dependent on electrode material and post-annealing treatment. Among Pt devices, I–V hysteresis was observed for the Ag/CrO x /Pt device only; no resistance switching was observed for Ag/CrO y /Pt, Ti/CrO x /Pt, and Ti/CrO y /Pt devices. Among FTO devices, I–V hysteresis was observed for the Ag/CrO x /FTO device whereas I–V hysteresis with the opposite switching direction was observed for Ag/CrO y /FTO, Ti/CrO x /FTO, and Ti/CrO y /FTO devices. The direction of switching depends not only on electrode material but also on post-annealing treatment, which affects the density of grain boundaries. Thus, the density of grain boundaries determines the type of charge carrier involved in the switching process. For as-deposited CrO x films with a high density of grain boundaries Ag filament paths mediated by electrochemical redox reaction were observed, irrespective of bottom electrode material (Pt or FTO). Post-annealed CrO y films with a low density of grain boundaries suppressed electrochemical redox reaction in the Ag/CrO y /Pt device but promoted short-range movement of O2? ions through the bottom interface, resulting in resistance switching in the Ag/CrO y /FTO device. Electrochemical redox reaction-controlled resistance switching occurred solely in oxides with a high density of grain boundaries or dislocations. 相似文献
99.
100.