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41.
Toshinori Okura Giichi Sudoh Hiroyuki Inoue Takafumi Kanazawa 《Journal of Materials Science》1995,30(4):1033-1036
The SiKΒ X-ray emission spectra for several silicates and silico-phosphates were measured using a high-resolution X-ray fluorescence spectrometer with two InSb(III) analyser crystals. Molecular orbital calculation analysis for the obtained spectra was performed by a SCC-DV-Xα method and the energy positions and relative intensities of the spectral fine structures were calculated with Slater's transition-state method. The calculated results interpreted the spectral profiles successfully. The energy shifts of the SiKΒ main peak were also discussed in terms of the electronegativity of the second-nearest-neighbour atoms. These shifts were attributed to the changes in the stability of the Si-O bonds due to the existence of second-nearest-neighbour P atoms. 相似文献
42.
From the point of view of waste recycling, hydroxyapatite (HAp) can be synthesized using the waste sludge from semiconductor process. The possibility of using HAp as an anticorrosive pigment was investigated. The water absorption of coating pigmented with anticorrosive pigment, HAp, red lead (RL) and zinc potassium chromate (ZPC), and the corrosion at interface between coating and substrate were monitored using AC impedance technique. The amount of absorbed water decreased in the order of ZPC- > HAp- > RL-pigmented > unpigmented film. However, the water absorbed into HAp- or ZPC-pigmented film seems to be beneficial to anticorrosive function. The anticorrosive performance of HAp is superior or at least comparable to those of ZPC and RL, which have been known as representative anticorrosive pigments. It seems that the anticorrosive properties of HAp is mainly achieved by passivating the substrate, namely the soluble component of HAp reacts with Fe to form iron phosphate in the presence of water. 相似文献
43.
Toshinori Taishi Hideaki IseYu Murao Takayuki OhsawaYuki Tokumoto Yutaka OhnoIchiro Yonenaga 《Microelectronic Engineering》2011,88(4):496-498
Local vibrations of oxygen in Ge crystals grown from a melt fully covered by B2O3 were evaluated by Fourier-transform infrared spectroscopy. Ge single crystals containing oxygen were grown by the Czochralski method under various growth conditions. Oxygen concentrations in the crystals were determined to be in the range between 8.5 × 1015 and 5.5 × 1017 cm−3 from the infrared absorption at 855 cm−1 originating in local vibration of Ge-Oi-Ge quasi-molecules. Absorption peaks relating to GeOx, SiOx and Si-Oi-Si were not detected in the as-grown crystals. The calibration coefficient for determining oxygen concentration in Ge crystals from the absorption peak intensity at 1264 cm−1 was estimated to be 1.15 × 1019 cm−2. 相似文献
44.
We have developed a spectroscopic transmission-type four detector polarimeter (T-FDP). It consists of a detector head and a multichannel spectrometer equipped with a two-dimensional CCD detector. Inside the T-FDP, three cubic beam splitters are aligned in a straight line and they are rotated relative to each other. From the responses of the spectroscopic T-FDP to five inputs with known polarization states it is possible to determine the characteristic matrices of the T-FDP at various wavelengths. The trajectories of the experimentally measured polarization states on the Poincaré sphere agree well with theoretical predictions. These results demonstrate the feasibility of using the T-FDP for spectroscopic ellipsometry. 相似文献
45.
46.
Yosuke Abe Tomohito Tsuru Shi Shi Naoko Oono Shigeharu Ukai 《Journal of Nuclear Science and Technology》2016,53(10):1528-1534
Various types of nanometric defects such as voids and helium (He) bubbles produced by high-energy neutron irradiations are known to degrade the mechanical properties of irradiated materials. In this study, we have evaluated the obstacle strength of He bubbles to the mobility of an edge dislocation in α-iron for 2 and 4 nm bubbles with He-to-vacancy (He/V) ratios ranging from 0 to 1 at 300 and 500 K, by molecular dynamics simulation. Results showed that as the He/V ratio increases, the obstacle strength needed for the release of a dislocation from the bubble becomes stronger up to a moderate He/V ratio (0.6 and 0.4 for 2 and 4 nm bubbles, respectively, at both temperatures), and a further increase in the He/V ratio leads to weakening of the obstacle strength. For He/V = 1, the obstacle strengths are 10–30% weaker than those at moderate He/V ratios depending on the bubble size and temperature. The extent of obstacle strength was found to be correlated with the dilation caused by He bubbles depending on the bubble size, He/V ratio, and temperature. 相似文献
47.
Tai Cheng Chuanjiang Qin Satoru Watanabe Toshinori Matsushima Chihaya Adachi 《Advanced functional materials》2020,30(24)
Quasi‐2D metal halide perovskite films are promising for efficient light‐emitting diodes (LEDs), because of their efficient radiative recombination and suppressed trap‐assisted quenching compared with pure 3D perovskites. However, because of the multidomain polycrystalline nature of solution‐processed quasi‐2D perovskite films, the composition engineering always impacts the emitting properties with complicated mechanisms. Here, defect passivation and domain distribution of quasi‐2D perovskite films prepared with various precursor compositions are systematically studied. As a result, in perovskite films prepared from stoichiometric quasi‐2D precursor compositions, large organic ammonium cations function well as passivators. In comparison, precursor compositions of simply adding large organic halide salt into a 3D perovskite precursor ensure not only the defect passivation but also the effective formation of quasi‐2D perovskite domains, avoiding unfavorable appearance of low‐order domains. Quasi‐2D perovskite films fabricated with a well‐designed precursor composition achieve a high photoluminescence quantum yield of 95.3% and an external quantum efficiency of 14.7% in LEDs. 相似文献
48.
49.
Norihiro Moriyama Yuta Kawano Qing Wang Ryota Inoue Meng Guo Makoto Yokoji Hiroki Nagasawa Masakoto Kanezashi Toshinori Tsuru 《American Institute of Chemical Engineers》2021,67(7):e17223
Pervaporation (PV) is a membrane technology that holds great promise for industrial applications. To better understand the PV mechanism, PV dehydrations of various types of organic solvents (methanol, ethanol, iso-propanol, tert-butanol, and acetone) were performed on five types of organosilica and two types of silicon carbide-based membranes, all with different pore sizes. Water permeance was dependent on the types of organic aqueous solutions, which suggested that organic solvents penetrated the pores and hindered the permeation of water. In addition, water permeance of various types of membranes in PV was well correlated with hydrogen permeance in single-gas permeation. Furthermore, a clear correlation was obtained between the permeance ratio in PV and that in single-gas permeation, which was confirmed via the modified-gas translation model. These correlations make it possible to use single-gas permeation properties to predict PV performance. 相似文献
50.
Development of high performance,waterborne coatings. Part II: Factors affecting adhesion performance
A new manufacturing process for high performance, waterborne coatings for can coating application was developed, which includes emulsification of an epoxy resin with or without a hardener by incorporation of an acrylic resin. It is possible by this new process to emulsify a variety of resins with minimum effects of the surfactant. (acrylic resin). The effects of surfactant and neutralizer on adhesion performance were studied. It was found that the effects of the acrylic resin amount were relatively small, and that the effects of the neutralizer were significant. It was confirmed that the usage of ammonia or amines with a branched alkyl group is required to achieve balanced dry and wet adhesion. 相似文献