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排序方式: 共有990条查询结果,搜索用时 31 毫秒
11.
Summary Glow discharge polymerizations of allyltrimethylsilane (ATMS) and trimethylvinyloxysilane (TMVOS) were investigated by elemental analysis and infrared spectroscopy. The formed polymers were far different in elemental composition from the starting materials, and possessed high carbon and hydrogen contents. There was less difference in an infrared-spectral sense between the two polymers from ATMS and TMVOS. A polymer-forming process in a discharge state is discussed. 相似文献
12.
For the purpose of synthesizing standards to be used in the quantification of TAG hydroperoxides, three TAG (1,2-dioleoyl-3-palmitoylglycerol,
1-oleoyl-2-linoleoyl-3-palmitoylglycerol, and triolein) monohydroperoxides were chemically synthesized as authentic specimens.
TAG were prepared by using a simple condensation in pyridine of glycerol and the corresponding acid chlorides. These TAG were
then converted into monohydroperoxides by a photosensitized peroxidation. The synthesized monohydroperoxides were analyzed
by normal-phase and RP-HPLC. The results of normal-phase HPLC analysis showed that monohydroperoxides from a corresponding
TAG were a mixture of regioisomers. In RP-HPLC, however, the regioisomers of monohydroperoxides were not separated and gave
a single peak, which may improve the sensitivity for the detection of TAG monohydroperoxides. In this study TAG monohydroperoxide
standards were synthesized; these will be useful for the study of yet unknown biological and pathological roles of TAG hydroperoxides. 相似文献
13.
Akio Makishima Hajime Kubo Takajjro Shimohira 《Journal of the American Ceramic Society》1986,69(6):130-C
Formation of yttrium aluminosilicate glasses containing calcium oxide from batches melted at 1550°C was investigated. Densities and thermal expansion coeflcients were measured for some glasses. In a specific compositional region, crystals with a needlelike habit were observed in the glass matrix. A crystal in the form of a tubular hexagonal prism was identified as Ca4 Y6 0(Si04 )6 . 相似文献
14.
Tsuyoshi Asakawa Hidefumi Takeda Shigeyoshi Miyagishi Morie Nishida 《Journal of the American Oil Chemists' Society》1986,63(11):1479-1482
The qualitative and quantitative determination of anionic surfactants (sodium and lithium alkylsulfate, sodium dodecylbenzenesulfonate,
sodium di-2-ethylhexyl sulfosuccinate, sodium and lithium perfluoroalkylcarboxylate, and lithium perfluorooctanesulfonate)
were investigated by a capillary tube isotachophoresis using a potential gradient detector. The leading electrolyte solution
was the mixture of acetonitrile and aqueous solution of histidine buffer containing calcium chloride. The terminating electrolyte
solution was the aqueous solution of sodium octanoate. These electrolytes were effective for the analysis of the mixtures
of strongly acidic surfactants. 相似文献
15.
Tsuyoshi Hagio Kazuo Kobayashi Hisayoshi Yoshida Hiroaki Yasunaga Hiroshi Nishikawa 《Journal of the American Ceramic Society》1989,72(8):1482-1484
Pressureless sintering of hexagonal boron nitride (BN) was performed using a powder activated by mechano-chemical treatments. Physical properties of the sintered BN bodies depend on the type of starting powder and the conditions of the treatments. The BN body, which was obtained at 2000°C using an appropriate activated powder, was 99 wt% pure and was excellent in mechanical and physical properties, in spite of its low density (1.64 g/cm3 ). 相似文献
16.
The effect of pressure on the melting, solid-solid transition, and crystallization of poly(trans-1,4-butadiene) (PTBD) was investigated using the pressure range of 1–3000 kg/cm2. D.t.a. measurements showed that, the melting and transition temperatures increase with increasing pressure, whose pressure coefficients are 38°C per 1000 kg/cm2 and 22°C per 1000 kg/cm2, respectively. These values were in fairly close agreement with those calculated from the Clausius-Clapeyron equation. Morphological studies using electron microscope and small-angle X-ray scattering method revealed that, the samples crystallized with relatively small supercoolings under normal or high pressure, are formed of distinct lamellae 400–800 Å thick. The lamellar thickness was inappreciably dependent on crystallization pressure. The significant effect of pressure on crystallization was recognized in a tendency of the crystallinity to increase, with increasing crystallization pressure. This pressure effect was explained by the mechanism that, the increased pressure might make the packing of molecular chains in liquid, more dense and that the secondary crystallization might be accelerated, to increase the lateral dimensions of lamellae. 相似文献
17.
Tadayoshi Matsumori Tsuguo Kondoh Atsushi Kawamoto Tsuyoshi Nomura 《Structural and Multidisciplinary Optimization》2013,47(4):571-581
This paper deals with density-based topology optimization considering fluid and thermal interactions, in which the Navier–Stokes and heat transport equations are coupled. We particularly focus on designing heat exchangers. In the engineering context, heat exchangers are designed while considering a certain amount of input power. Therefore it is important to maximize the performance of a heat exchanger under a constant input power. In this paper we propose a way to control the input power by introducing an extra integral equation. To be more precise, in the fluid analysis, the inlet pressure is determined by solving the extra integral equation together with the Navier–Stokes equation. By doing this we can keep the inlet power constant even when the flow channels are changed in the optimization process. Consequently, the system of equations of the fluid field takes an integrodifferential form. On the other hand, in the heat transport analysis, a single governing equation is defined for simultaneously modeling both the solid and fluid parts. The design variable is a fluid fraction whose distribution represents the topology of the solid and fluid domains. When designing heat exchangers, two different heat conditions are considered in the formulation of the optimization problems, namely temperature-dependent and temperature-independent heat sources. Through the numerical examples for designing flow channels in a heat exchanger, it is shown that distinct topologies can be obtained according to the input power and the heat source conditions. 相似文献
18.
Question-Answering Bulletin Boards (QABB), such as Yahoo! Answers and Windows Live QnA, are gaining popularity recently. Questions
are submitted on QABB and let somebody in the internet answer them. Communications on QABB connect users, and the overall
connections can be regarded as a social network. If the evolution of social networks can be predicted, it is quite useful
for encouraging communications among users. Link prediction on QABB can be used for recommendation to potential answerers.
Previous approaches for link prediction based on structural properties do not take weights of links into account. This paper
describes an improved method for predicting links based on weighted proximity measures of social networks. The method is based
on an assumption that proximities between nodes can be estimated better by using both graph proximity measures and the weights
of existing links in a social network. In order to show the effectiveness of our method, the data of Yahoo! Chiebukuro (Japanese
Yahoo! Answers) are used for our experiments. The results show that our method outperforms previous approaches, especially
when target social networks are sufficiently dense.
相似文献
Tsuyoshi MurataEmail: |
19.
20.
Detecting Communities in <Emphasis Type="Italic">K</Emphasis>-Partite <Emphasis Type="Italic">K</Emphasis>-Uniform (Hyper)Networks 下载免费PDF全文
In social tagging systems such as Delicious and Flickr,users collaboratively manage tags to annotate resources.Naturally,a social tagging system can be modeled as a (user,tag,resource) hypernetwork,where there are three different types of nodes,namely users,resources and tags,and each hyperedge has three end nodes,connecting a user,a resource and a tag that the user employs to annotate the resource.Then how can we automatically cluster related users,resources and tags,respectively? This is a problem of community detection in a 3-partite,3-uniform hypernetwork.More generally,given a K-partite K-uniform (hyper)network,where each (hyper)edge is a K-tuple composed of nodes of K different types,how can we automatically detect communities for nodes of different types? In this paper,by turning this problem into a problem of finding an efficient compression of the (hyper)network’s structure,we propose a quality function for measuring the goodness of partitions of a K-partite K-uniform (hyper)network into communities,and develop a fast community detection method based on optimization.Our method overcomes the limitations of state of the art techniques and has several desired properties such as comprehensive,parameter-free,and scalable.We compare our method with existing methods in both synthetic and real-world datasets. 相似文献