有滞后环节的系统的闭环鲁棒辨识方法

提出一种新的针对带滞后环节的任意阶系统的闭环辨识方法。通过“三步法”，实现在闭环条件下的被控制对象的传递函数参数的辨识，所提出方法具有很强的鲁棒性。仿真例子表明该方法的有效性。     

B113－2型低汽／气比CO高温变换催化剂的研制

介绍了Ｂ１１３－２Ｍ低汽／气比ＣＯ高温变换催化剂的研制方法及其特点．实验室测试表明，Ｂ１１３－２型催化剂具有堆密度低、运行强度高、选择性好、抗沸水性能优、本体含硫低及低温活性好等优点．     

Preparation of fluoroacrylate nanocopolymer by miniemulsion polymerization used in textile finishing

Latex based on fluoroacrylate (TAN) and other comonomers was prepared via miniemulsion polymerization in the presence of stearyl trimethyl ammonium chloride (STAC) and 2, 2′‐azobis (2‐amidinopropane) dihydrochloride (ABAP) as a water soluble initiator. Light transmittance studies demonstrated that the light transmittance of prepared emulsions increases with the amount of TAN, STAC, cosolvent DPM, and hydrophobe DM. Given suitable reaction temperature and quantities of TAN, STAC, DPM, and DM, a copolymer emulsion of fluoroacylate with a particle size of 50 nm was produced. The water repellency tested on polyester fabrics displayed greater effectiveness than that of commercial products with higher fluorine content. © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 94: 1466–1472, 2004     

Synthesis of Dimethyl Carbonate from Methanol and Carbon dioxide using Potassium Methoxide as Catalyst under Mild Conditions

Pd-supported on WO₃–ZrO₂ (W/Zr atomic ratio=0.2) calcined at 1073 K was found to be highly active and selective for gas-phase oxidation of ethylene to acetic acid in the presence of water at 423 K and 0.6 MPa. Contact time dependence demonstrated that acetic acid is formed via acetaldehyde formed by a Wacker-type reaction, not through ethanol by hydration of ethylene.     

和田菟丝子在不同寄主中有效成分含量的测定研究

采用高效液相色谱法(HPLC)对和田菟丝子中槲皮素和山萘酚进行了定量测定。测定寄主为胡麻植物的菟丝子中槲皮素含量为0 239 mg·g-1,山萘酚的含量为0 347 mg·g-1 ;寄主为苜蓿的菟丝子中槲皮素含量为0 103 mg·g-1,山萘酚的含量为0 068 mg·g-1。和田菟丝子寄主不同,其槲皮素和山萘酚的含量不同,应结合寄主植物研究其有效成分。     

2,6-二氯-3-甲基苯胺合成新工艺

通过n-乙酰化保护氨基，氯磺酸与氨水反应在氨基对位形成磺酰胺阻塞基团，再经脱乙酰基，氯化，水解脱阻塞基团，合成2，6-二氯-3-甲基苯胺得到目标产物。与经典文献方法相比，用盐酸代替氢氧化钠脱除乙酰基，用氯酸钠和浓盐酸代替双氧水和浓盐酸或氯气的氯化方法，合成过程中省略了中间产物的分离步骤，以间甲苯胺计总摩尔收率从20％提高到了60．8％，产品纯度大于99．5％。     

地表水质监测模型中的几种人工智能方法

重点对地表水质预测模型的几种人工智能方法进行了评述,具体说明了BP神经网络水质预测模型、地表水COD灰色预测模型、时间数列预测方法及WASP5模型系统等方法的原理和特点.并提出地表水质预测模型WASP5与GIS系统集成的趋势,建立水质自动监测系统是我国水质现状和社会发展的需要,并分析了发展水质自动检测系统的方法及可行性.     

固定床催化合成N,N-二甲基丙胺的研究

以正丙醇和二甲胺为主要原料,采用浸渍法制备负载活性金属的Al2O3催化剂,在固定床反应器中考察了催化剂载体预处理及反应条件对合成N,N-二甲基丙胺的影响.结果表明:一次磷酸处理的A12O3上负载入活性组分(Cu10%,Cr12%)的催化剂具较满意的选择性和活性.较合适的反应工艺条件为压力0.8Mpa,反应温度220℃,空间速度为0.3h-1,进料比为二甲胺:丙醇=3:1,此时产品的收率达到90%以上.     

A new LCL-lens array with electrodes of interlaced structure to be applied for auto-stereoscopic 3D displays

A new design of the liquid crystal lenticular (LCL) lens array with interlaced electrodes is proposed to realize an auto-stereoscopic 3D display. The structure of interlaced electrodes aims to generate a desired non-uniform electric filed to improve the focusing ability of the LCL-lens array with lower voltage drives. This paper is organized as first to describe the design criteria of a lenticular lens sheet for wide extended graphics array LCD panel. Based on the designed lenticular lens array, an LCL-lens array with proposed interlaced electrodes is next designed. The fabrication and the detailed structure are given. A series of experiments are then conducted and successfully verify the focusing capability and desired 3D display functions, that is, to separate two images to right and left eyes. Also, the developed auto-stereoscopic 3D display is able to adapt to varied viewer locations with favorable imaging quality.     

Design and realization of a high resolution (640 × 480) SWIR image acquisition system

A new image acquisition system module for extracting signals of high-resolution short wave infrared (SWIR) from a focal plane array (FPA) is presented in this study. The short wave infrared (SWIR—with wavelength about 900–1,700 nm) images have been proven its unique values in many applications such as military, semiconductor inspection and aviation security. The designs for the SWIR data acquisition system module consists of digitization and acquisition of FPA signals, design of synchronous dynamic random access memory controller and real-time image signal transformation and display. Three major steps involved towards a successful SWIR module—(1) Selection of hardware ICs according to specification for the FPA; (2) Design of a timing generator for the image acquisition system to control FPA and other ICs by Verilog HDL programming; (3) Integrate the individual modules on a PCB. The SWIR image output signals are successfully generated in the format of National Television System Committee (NSTC), which can be displayed on a common NTSC monitor, flat panel displays with an AV input terminal or a CRT display in a favorable speed of frame rate at 30 per second.