液态混合有机标准物质研究

本研究采用重量法配制有机液态混合标样 ,并对配制方法、混合标样的均匀性、稳定性及影响不确定度的因素进行了研究 ,并用气相色谱法进行了比对分析。经稳定性监测 ,稳定度大于等于一年 ,不确定度小于± 2 %。     

Isothermal Gas Forming of Mg Alloy AZ31 Sheet

There have been reports on sheet forming of Mg alloy in industry via the punch and die method;this paper is probably the first formal one for studying the sheet formability of AZ31 employing pressurized gas to press the sheet into a female die cavity at various elevated temperatures.The results indicate it is feasible to form a rectangular box via pressurized gas from extruded sheets of 0.5 and 1.7 mm thick.The formed box has 1:2 depth over width ratio,which should be large enough when dealing with realistic industrial sheet forming parts.Presently,forming a sheet of 0.5 mm thick is considered a technical challenge by industry,and it is conquered as demonstrated in this paper.Gas forming technique applied to Mg alloy is unprecedented and shows potential for industrial utilization.     

骆马湖水环境变化趋势及对策研究

随着经济发展、城市化率的提高，加之滨湖开发，骆马湖的水质呈现一定的恶化趋势，生态系统遭受破坏，水体富营养化发展有越来越严重的趋势。通过对骆马湖营养化程度和污染原因的分析，提出了一些对策措施和解决办法，以期实现湖泊的生态、环境与经济的协调发展。     

拉西瓦水电站工程反拱水垫塘优化设计

在大型高水头水电站中,拉西瓦水电站是我国第一座采用反拱形水垫塘作为特高拱坝坝后消能建筑物的工程,也是我国现有特高拱坝水垫塘中长度最短、宽度最小的工程,其单位水体消能率接近国际经验控制的最高标准。在无规范明确规定和缺少工程资料的情况下,经一系列科研试验和数值计算,优化了反拱水垫塘结构和排水、抽水系统设计等。其经验丰富了我国坝后消能建筑物的设计内容,对我国规范中反拱水垫塘设计规定以及对其他大型高水头水电站坝后消能防冲建筑物的设计具有重要参考价值。     

煤直接液化中SO2-4 /ZrO2固体酸的催化作用

以二苯甲烷、苯乙醚为煤的模型化合物,以四氢萘(THN)为溶剂,进行中高压加氢液化实验,结合产物的气相色谱和质谱分析,考察了SO2-4/ZrO2固体酸对煤直接液化的催化作用及加氢液化机理.实验结果表明,SO2-4/ZrO2固体酸对模型化合物的转化具有良好的催化活性,与非催化液化相比,400 ℃、H2初压5 MPa、30 min时二苯甲烷的转化率由8.96%提高到61.75%,且模型化合物的存在促进了溶剂THN的转化,上述条件下THN的转化率也达到10.92%;模型化合物及THN的转化主要包括氢解、异构、氢转移及烷基化等反应;SO2-4/ZrO2固体酸的催化作用主要为酸催化的离子反应机理,增强催化剂的酸性有利于煤的催化液化.     

Structural Description of Polyaromatic Nucleus in Residue

The proton nuclear magnetic resonance spectroscopy （1H-NMR）, the synchronous fluorescence spectrometry （SFS） and the ruthenium ions catalyzed oxidation （RICO） method were used to determine the chemical structure of polyaromatic nucleus in Oman residue fractions. The results of 1H-NMR analyses showed that the average numbers of aromatic rings in the aromatics, resins and asphaltenes units were 3.2, 5.6 and 8.2, respectively. SFS was used to investigate the distribution of aromatic rings in residue fractions, the main distribution range of aromatic rings in aromatics, resins and asphaltenes were 3 4 rings, 3--5 rings and more than 5 rings, respectively. The aromatic network in residue fractions was oxidized to produce numerous carboxylic acids. The types and content of benzenepolycarboxylic acids, such as phthalic acid, benzenetricarboxylic acids, benzenetetracarboxylic acids, benzenepentacarboxylic acid and benzenehexacarboxylic acid disclosed the condensed types of aromatic nuclei in the core. The biphenyl fraction （BIPH）, the cata-condensed fraction （CATA）, the peri-condensed fraction （PERI） and the condensed index （BCI） were calculated based on the benzenepolycarboxylic acids formed. The results implied that there was less biphenyl type structures in all residue fractions. The aromatics fraction was almost composed of the cata-condensed type system, and the asphaltenes fraction was wholly composed of the peri-condensed type system, while in the resins fraction co-existed the two types, herein the peri-con- densed type was predominant over the cata-condensed type. Based on the analytical results obtained in the study, the components --aromatics, resins and asphaltenes -- were given the likely structural models.     

Modeling Power Supply Noise in Delay Testing

Excessive power supply noise during test can cause overkill. This article discusses two models for supply noise in delay testing and their application to test compaction. The proposed noise models avoid complicated power network analysis, making them much faster than existing power noise analysis tools. can cause performance degradation and     

An analytical model for I-V and small-signalcharacteristics of planar-doped HEMTs

An analytical current-voltage (I-V) model for planar-doped HEMTs is developed. This compact model covers the complete range of I-V characteristics, including the current saturation region and parasitic conduction in the electron-supplying layer. Analytical expressions for the small-signal parameters and current-gain cutoff frequency are derived from the I-V model. Modeling results for a 0.1-μm-gate planar-doped AlInAs-GaInAs HEMT show excellent agreement with measured characteristics. Threshold voltages and parasitic conduction in planar-doped and uniformly doped HEMTs are also compared and discussed     

Seya-Nanioka系统真空紫外单色仪的分辨能力及波长读数精度

本文分析了Seya-Namioka系统光学参数与离焦量的关系,为选取最佳光学参数提供了依据。同时,简要说明了影响谱线质量及波长读数精度的因素,并讨论了补偿波长读数误差的方法。