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31.
On structural and high temperature electrochemical properties of ZrO2 thin film coating on Zr metal produced by carbonate melt 总被引:1,自引:0,他引:1
Melt of NaCO3 can favor oxidation of Zr to form ZrO2 thin film on Zr surface, which is used to make Zr/ZrO2 oxidation/reduction electrode of pH sensor for testing elevated temperature aqueous solutions. Using SEM, EPMA, XPS, EXAFS
and HRTEM, we found that ZrO2 film is tightness and solid with 20 μm thickness composed by nanometer-sized monoclinic crystals. Zr/ZrO2 interface is characterized of zoning structure according to topography and chemical composition in five zones: oxygen-rich
ZrO2, ZrO2, oxygen-rich Zr metal, oxygen-bearing Zr and Zr from outmost to center. Melt oxidation process of Zr involved oxidation time,
air and temperature. The air is important effect on structural and electrochemical properties of ZrO2 thin film for making elevate temperature electrochemical sensor. If oxygen air largely presented in carbonate melting process,
ZrO2 thin film is not tightness and not for oxidation/reduction electrode. 相似文献
32.
Daniel X. Gouveia Odair P. Ferreira Antonio G. Souza Filho M. G. da Silva J. A. C. de Paiva Oswaldo L. Alves Josué Mendes Filho 《Journal of Materials Science》2007,42(2):534-538
The thermal decomposition properties of Mg–Fe hydrotalcites were studied through in situ 57Fe Mössbauer spectroscopy and in situ X-ray diffraction. Abrupt changes in the quadrupolar splitting measured in the Mössbauer spectra revealed a phase transition from the starting lamellar structure to a new crystalline arrangement. By analyzing the Mössbauer parameters we show that the material is highly disordered in the 300–400 °C temperature range. This hypothesis is confirmed by the X-ray results whose diffractograms indicated the collapse of the lamellar structure and the formation of a solid solution. 相似文献
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Polyurethane elastomer composites were developed using milled fiberglass and their mechanical properties were studied. In particular, the organically chemical treatment of the milled fiberglass was investigated in detail. It was demonstrated that both strength and toughness of the resulting elastomer composites were improved considerably with the addition content of fiberglass. Furthermore, it was indicated that the optimal properties can be achieved by the proper addition of milled fiberglass that was chemically treated using coupling agent. 相似文献
37.
Oxide films were deposited on different substrates by laser molecular beam epitaxy. Reflection high-energy electron diffraction was performed to in situ investigate the change of growth mode and the lattice relaxation during the growth. An asymmetrical phenomenon was found in the two kinds of strain states, compressive stress and tensile stress of heterostructures with different lattice mismatch. In the case of BaTiO3/SrTiO3 (2.2%), 2D layer-by-layer growth mode without lattice relaxation can be maintained for a longer period for BTO films on STO with compressive stress, comparing to STO films on BTO with tensile stress. When MgO films were deposited on SrTiO3 with a large mismatch of 7.8%, compressive stress leads to rapid lattice relaxation with a very thin wet layer, and 3D strained island were observed. As a comparison, SrTiO3 films on MgO with tensile stress were configured. No RHEED patterns can be observed duo to a large tensile stress. 相似文献
38.
Effect of boron on the low-cycle fatigue behavior and deformation structure of INCONEL 718 at 650 °C
L. Xiao M. C. Chaturvedi D. L. Chen 《Metallurgical and Materials Transactions A》2004,35(11):3477-3487
Symmetrical push-pull low-cycle fatigue (LCF) tests were performed on INCONEL 718 (IN718) containing 12, 29, 60, and 100 ppm
B at 650 °C. The results showed that all the alloys experienced a relatively short period of initial cyclic hardening at low
strain amplitudes, followed by a regime of saturation or slightly continuous cyclic softening. The initial cyclic hardening
phase decreased with increasing strain amplitudes, and disappeared at the high strain amplitudes. A serrated flow was observed
in the plastic regions of cyclic stress-strain hysteresis loops. The saturated cyclic stress amplitude at a given strain amplitude
was highest for the alloy with 60 ppm B, and lowest for the alloy with 12 ppm B. The LCF lifetime increased with increasing
B concentration up to 60 ppm, and then decreased as the B content increased from 60 to 100 ppm. Fractographic analysis suggested
that the fracture mode changed from intergranular to transgranular cracking as the B concentration increased. The characteristic
deformation microstructures produced by LCF tests at 650 °C, examined via transmission electron microscopy, were regularly spaced arrays of planar deformation bands on {111} slip planes in all four
alloys. A ladderlike structure was observed in some local regions in the alloy with 12 ppm B. Heavily deformed planar deformation
bands were observed in the fatigued specimens with 100 ppm B. The mechanism of improvement in the LCF life of IN718 due to
B addition is discussed. 相似文献
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