High-temperature oxidation of aluminum electroplated Fe-Mn alloys

Austenitic Mn-Al alloys (20–32 W/O Mn, 7–10 Al, 2–3 Si, 1C) were found to have satisfactory oxidation resistance up to 950°C under isothermal conditions in air. Surface enrichment of aluminum is a necessary condition for obtaining an almost pure alumina scale for uses at higher temperatures. Four different Mn-steels were Al-coated by the Capuano electroplating process. In all the steels there was an increase in the hot-oxidation resistance. The best results were obtained with steels containing both Al and Si, and this for temperatures up to 1100°C. No spalling was noticed during rapid cooling of the test pieces. Silicon was found to act as a diffusion barrier to outward iron diffusion. It appears that there is formation of a pure, thin film of alumina from the matrix which interacts with the aluminum diffusing from the superimposed, coating for the formation of good bonds.     

大丝束聚丙烯腈基预氧丝炭化研究

采用正交实验法研究了炭化温度、炭化时间、升温速率等因素对两种聚丙烯腈基预氧丝炭化产物结构和性能的影响.结果表明,进口东邦48 K大丝束聚丙烯腈基预氧丝环化程度优于国产吉林6 K小丝束聚丙烯腈基预氧丝,在炭化温度950℃,升温速率4℃/min,保温时间10 min条件下,炭化可取得最佳性能,炭化产物纤维拉伸强度达2.96 GPa,而国产吉林6 K小丝束在炭化温度1 100℃,升温速率4℃/min,保温时间5 min条件下炭化产物性能最佳,产物炭纤维拉伸强度近3.80 GPa.伴随两种预氧丝炭化过程,纤维颜色加深,表面缺陷减少,拉伸断裂模式均由假塑性向脆性过渡,为复合材料低成本开发中预氧丝坯体制备与炭化工艺提供了参考依据.     

水煤浆在燃油热水锅炉内的燃烧试验

主要介绍了７ＭＷ燃油热水锅炉改烧水煤浆的改造设计，水煤浆炉前系统的调试，锅炉改造后的调试和水煤浆燃烧试验的结果。     

Morphologies and microstructures of tree-like carbon produced at different reaction conditions in a CVD process

Centimeter-size multi-branched tree-like carbon structures have been generated by the catalytic chemical vapor deposition of toluene using ferrocene as the catalyst precursor and investigated by means of SEM, TEM, and EDX. It is found that a temperature of 1000-1200 °C and a carrier gas flow rate of 1000-2500 ml/min are necessary for the generation of the carbon trees. Their morphologies and microstructures change greatly with the changing reaction conditions. The fractal dimensions of the trees are calculated to quantitatively investigate the influence of different reaction temperatures on the morphologies.     

试析冷战后中日关系中安全困境的成因

安全困境是现实主义解释国际政治的一个基本概念。从安全困境在国际政治学中的一般定义着手,结合中日地缘政治利益、实力对比、历史积怨及美国的介入等问题分析了中日安全困境的成因。     

In vitro hydrolysis of natural and synthetic γ-linolenic acid-containing triacylglycerols by pancreatic lipase

The present study compared thein vitro hydrolysis of two 18:3n-6-rich oils—evening primrose oil (EPO) and borage oil (BO)—and different synthetic 18:3n-6-containing triacylglycerols (TG). Incubation of EPO and BO with pancreatic lipase lipolyzed 18:3n-6 from the TG species. The rate of lipolysis of TG species containing two or three molecules of 18:3n-6, which comprised 36% of total 18:3n-6 in BO and only 7% in EPO, was significantly slower than those containing only one molecule of 18:3n-6. This was found especially in those with two molecules of linoleic acid, which constituted 20% of total 18:3n-6 in BO, whereas over 80% were present in EPO. In a separate study, various synthetic 18:3n-6-containing TG were also subjected toin vitro hydrolysis by pancreatic lipase. Results showed that release of 18:3n-6 from thesn-1/sn-3 positions was significantly slower when two other stereospecific positions in the same TG molecule were occupied by either palmitic acid (16:0) or monounsaturated (18:1 and 20:1) fatty acids than when occupied by 18:2n-6. The rate of hydrolysis ofsn-2-γ-linolenyl-sn-1(3)-diacylglycerol to formsn-2-mono-γ-linolenyl glycerol was also significantly slower when both thesn-1 andsn-3 positions in TG molecules were occupied by either saturated fatty acids (16:0 and 18:0) or long-chain monounsaturated fatty acids than when occupied by 18:2n-6. These findings suggest that the stereospecific position of 18:3n-6 in TG molecules and the constituent of its neighboring fatty acids modulated availability of 18:3n-6 from 18:3n-6-containing TG or 18:3n-6-rich oils.     

压缩感知算法在阵列测向中的相干信号分辨

现有算法在进行信号重建时,需要原始信号的稀疏信息来控制初始原子集的大小和算法迭代的最大次数,这削弱了重建精度,增加了计算复杂度,限制了其实际应用能力。为了克服这个问题,提出了基于正交匹配追踪算法的改进算法。该算法将阵元个数作为假设稀疏度,在稀疏度未知的初始阶段扩展初始原子集。最后通过对测量信号的幅度进行阈值过滤以实现信号的分辨和信源数的估计。为解决测向人员面对监测软件所指示的多个信号示向度中,无法分辨哪些指示方向是同一个信号源所产生的折反射信号的问题,首次提出了基于压缩感知算法的相干关系分析和相干信号分辨的模型。实测数据结果表明,该算法在不同环境下可以清晰分辨相干信号,并且能够适应多种实验平台。     

“EM”水玻璃自硬砂的应用

本文介绍了一种可用于大型铸铜件的“EM”水玻璃自硬砂.通过实验及实际生产验证,该砂在满足强度要求的同时还可明显减少水玻璃的加入量,且该砂的溃散性很好,各方面均优于传统的水玻璃砂.     

基于ZYNQ飞艇囊体应变在线监测系统设计

针对当前高空飞艇囊体的应变实时测量装置无法同时具备体积小和实时测量的工作属性,创新性地用光学器件和感光元件配合,对工作中飞艇囊体两个固定点的相对位移量进行测量,提出了一种能够在线监测飞艇囊体应变的测量装置,能够实现应变在线测量且测量精度高;采用TCD1500C电荷耦合器件作为数据来源;主芯片采用ZYNQ处理器,ZYNQ能够具备FPGA的并行处理能力和Cortex的数据调度能力,能够处理CCD高速数据;通过自定义IP核,使用PS端与PL端互联AXI协议,实现了高速、大量数据传输;为了得到应变信号,采用了将应变信号转化为位移信号进行采集的方法,之后将位移信号采集存储至SD卡中并周期性显示到上位机上,实现地面对飞艇囊体应变的实时监控;实现了飞艇囊体应变的实时测量并把测量精度提高至0.1％.