Al-Cu-Fe系初生准晶相凝固过程的电子显微分析

采用包括金相（OM），粉末X射线衍射（XRD），扫描电子显微镜（SEM）观察和透射电子显微（TEM）分析等方法，研究了铸态Al592.Cu36.8Fe3.0Si1.0合金（700℃保温2．5h后水淬）的显微组织及相组成。发现铸锭中存在4种相：准晶I相，τ3相（或φ相），θ－Al2Cu相和η－AlCu相，凝固过程可描述为：初生晶是准晶Ⅰ相；在保温过程中发生包晶或共晶反应（L＋i→τ3(或φ）或L→τ3（或φ）＋i)形成的τ3相（或φ相），呈微畴结构；而剩余液体水淬形成θ－Al2Cu相和η－AlCu 相。     

近非临界相位匹配温度调谐MgO：LiNbO3OPO

通过对MgO:LiNbO3参量过程温度相位匹配及走离角，允许参量等运转参数的理论计算与分析，确定了晶体的切割角度θ=82℃，以近非临界相位匹配（NCPM）取代NCPM，将温度调节范围控制在较低的温度上，研制了532nm泵浦的MgO:LiNbO3温度调谐脉冲光学参数振荡器（OPO），在800～1700nm波段实现连续调谐输出。参量泵浦功率密度阈值为57.3MW/cm^2，泵浦能量约2倍阈值处，单谐振（SRO）参量转换效率为11%以上。     

关于非线性浅水波理论中的孤立波解

本文在[1]的基础上,详尽地得到了Boussinesq方程和KdV方程的孤立波解,并对波高和波形进行了细致的分析。为了更好地比较,本文还给出了高阶摄动的孤立波解。     

Prediction of residual colour in reactive dyeing effluent

In this study, the absorbance of the three-dye mixture effluent from reactive dyeing has been used to predict the residual colour value of the dyeing effluent. The colour values of the dyeing effluent have been predicted in terms of ADMI colour values. The prediction accuracy was found to be satisfactory when some mathematical approaches, such as linear and non-linear regression, were used.     

钻井液用降滤失润滑剂的研制与应用

以沥青磺化为基础,辅以表面活性剂和降滤失剂等材料,通过化学处理加工研制出了ZR-1钻井液用降滤失润滑剂.由于大多数润滑剂在使用过程中容易出现起泡现象,因此在研制ZR-1的过程中对乳化剂进行了优选,通过调整HLB值,达到了不起泡的效果.该产品不仅能显著改善钻井液的润滑性,而且降滤失的效果好,能使泥饼黏滞系数降低50%以上,高温高压滤失量降低20%以上;该产品无毒无害,不污染环境,储存、运输和使用均方便安全.对ZR-1的性能进行了室内试验评价,介绍了该处理剂在川渝地区的应用.     

G104-5P42分支水平井钻井液工艺技术

G104-5P42井是在高尚堡G104-5区块构造较高部位部署的一口重点开发井，也是冀东油田第一口鱼骨型水平分支井，钻探目的是开发高浅北区Ng12油层，挖掘高浅北区井间剩余油潜力。该井主井眼斜深为2388m，水平位移为736．42m，水平段长243m，第一分支斜深为2342m，水平段长120．25m，水平位移为682．14m，第二分支斜深为2421m，水平段长117m，水平位移为761．73m。三开选用无固相甲酸盐聚合醇钻井液，在钻进油气层前加入GN-YBJ-I保护剂。应用结果表明，无固相甲酸盐聚合醇钻井液具有好的防塌能力和润滑减阻效果，性能稳定、黏度、切力较低，有利于减少环空压力损耗；在油气层段密度控制在1．08g／cm^3以内，为近年来同区块密度使用最低井，减小了有害固相及滤液对储层的伤害密度，经测试该井获高产油流；该井全井平均机械钻速为15．09m／h，钻井周期比原设计提前15d。该体系的配制及维护成本较高，适宜在目的层井段使用，但可回收再利用。     

K0.9Li0.1（Ta0.5Nb0.5）O3晶体压电应变系数的测量

用准静态ｄ＿（３３）测量仪和干涉法相结合。测量了Ｋ＿（０．９）Ｌｉ＿（０．１）（Ｔａ＿（０．５）Ｎｂ＿（０．５）Ｎｂ＿（０．５））Ｏ＿３晶体的压电应变系数。结果为：ｄ＿（３３）＝８６．０，ｄ＿（３３）＝一２９．５，ｄ＿（１５）＝１１２．９×１０￣（－１２）Ｃ／Ｎ．     

npn AlGaN/GaN HBT模型与特性分析

基于实验数据对GaN材料的少子寿命和碰撞电离率进行了建模,应用漂移-扩散传输模型开展了npnAlGaN/GaN异质结双极晶体管的特性研究,给出了器件导通电压、偏移电压和饱和电压的解析式.结果表明:实际器件导通电压、偏移电压及饱和电压较大的原因主要是高基区电阻和基区接触的非欧姆特性,为器件的工艺制造提供了理论指导.     

Preparation and characterization of polyurethane microcapsules containing n‐octadecane with styrene‐maleic anhydride as a surfactant by interfacial polycondensation

A series of polyurethane microcapsules containing a phase change material (PCM) of n‐octadecane was successfully synthesized by an interfacial polymerization in aqueous styrene‐maleic anhydride (SMA) dispersion with diethylene triamine (DETA) as a chain extender reacting with toluene‐2,4‐diisocyanate (TDI). The average diameter of microPCMs is in the range of 5–10 μm under the stirring speed of 3000–4000 rpm. Optical and SEM morphologies of microPCMs had ensured that the shell was regularly fabricated with the influence of SMA. FTIR results confirmed that the shell material was polyurethane and the SMA chains associated on core material reacted with TDI forming a part of shell material. The shell thickness was decreasing in the range of 0.31–0.55 μm with the molar ratio of DETA/TDI from 0.84 to 1.35 and the weight of core material increasing from 40 to 80% (wt %). By controlling the weight ratio of PCM as 40, 50, 60, 70, and 80% in microPCMs, it was found using DSC that the T_m and T_c of microPCMs were in the range of 29.8–31.0^oC and 21.1–22.0°C and an obvious phase change had been achieved nearly the same temperature range of that of PCM. The results from release curves of microPCM samples prepared by 1.4, 1.7, and 2.0 g of SMA indicated the release properties were affected by the amount of the dispersant, which attributed to the emulsion effect and shell polymerization structure. The above results suggest that the shell structure of microPCMs can be controlled and the properties of microPCMs determined by shell will perform proper practical usage. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 4996–5006, 2006     

方波扫描路径确定声源声功率误差特性分析

改进了矩形测量面方波扫描路径测量声功率的误差模型 ,以单极子、偶极子及四极子声源为例 ,给出了扫描方向、测量面离声源的距离及扫描线的密度的选取对理论误差的分布图形。分析结果表明 :对选定的测量面 ,在扫描线密度小的情况下 ,通过调整声源离测量面的距离 ,可以在声源近处找到一个最优点或较优点 ,使理论误差为零或很小 ;在绝大多数情况下 ,沿测量面长边扫描误差比沿短边扫描小。