醇镁还原法一步制取对氯苯胺的研究

醇镁还原法一步制取对氯苯胺是一种新的方法 ,研究发现最佳反应温度为 80℃～ 85℃ ,反应时间为4h ,对氯硝基苯与镁粉的用量 (物质的量比 )为 1∶3,产率为 80 %。     

纳米级BaAl_2O_4微粉的制备和性质

分别用溶胶 -凝胶法、低温固相反应法 ,制得了纳米级BaAl2 O4微粉 ,用电镜观察了其形貌和粒径的大小 ,用X-射线衍射仪进行了物相分析 ,测定了其纯度与晶型 ,讨论了制备方法与粒度大小的相互影响     

Measurements of single chain form factors by small-angle neutron scattering from polystyrene blends containing high concentrations of labelled molecules

A series of small angle neutron scattering measurements on blends of normal polystyrene (PSH) and labelled (deuterated) polystyrene (PSD) have been made with concentrations of PSD from 5 to 50 mol %. It is shown that the single chain form factor of the polymer in bulk can be obtained from a single concentration measurement for any concentration of labelled molecules, providing the molecular weights of the parent and labelled molecules are the same and the molecular weight distributions are narrow.     

Delay-dependent state estimation for delayed neural networks

In this letter, the delay-dependent state estimation problem for neural networks with time-varying delay is investigated. A delay-dependent criterion is established to estimate the neuron states through available output measurements such that the dynamics of the estimation error is globally exponentially stable. The proposed method is based on the free-weighting matrix approach and is applicable to the case that the derivative of a time-varying delay takes any value. An algorithm is presented to compute the state estimator. Finally, a numerical example is given to demonstrate the effectiveness of this approach and the improvement over existing ones.     

冷媒充填机的PLC控制

介绍了冷媒充填机控制系统的组成和工作原理，着重叙述了西门子S7－200可编程控制器与触摸屏结合的控制方式，使系统的性能得到较大的提高。     

JFC磷酸酯的合成和应用

详述了JFC磷酸酯的合成工艺路线，以及它在织物前处理精练工艺中的应用。与其它磷酸酯类精练剂性能对比，证明它可作为一种性能优良的精练剂中的添加剂。     

End-User Computing in a CASE Environment

Computer-aided software engineering (CASE) tools are currently being used by IS professionals rather than by users. No matter how effective these tools may be, however, they will not be able to assist in the reduction of application backlogs without supporting user-driven applications. This article examines characteristics of a CASE environment from the various perspectives of decision support, identifies the advantages and limitations of end-user computing in this environment, and suggests how IS managers can realize the potentials of CASE for user applications.     

绍兴咸亨快餐店

咸亨酒店随着鲁迅先生的《孔乙己》名闻天下，而凝聚着胆略、智慧和勇气的“咸亨”，经过几十年的延伸和拓展，不仅成了绍兴的一种象征，更是一块响当当的民族品牌。如今咸亨人又反弹琵琶，推出了’咸亨快餐”。 在快餐经营业中，如何使中式快餐走出传统模式，使它更加迎合消费者的口味，以及制作加工省时、省料是快餐店老总们研究的问题。同样，如何在设计过程中使传统的形式，特别是绍兴咸亨这个有一百多年历史文脉的老店走出其现有的模式，向前跨越一步是设计者深入探究的问题。而作为绍兴的一家中式快餐，我们的设计必须把握它的特点：…     

A Built-in Self-Test Scheme with Diagnostics Support for Embedded SRAM

In this paper we propose a novel built-in self-test (BIST) design for embedded SRAM cores. Our contribution includes a compact and efficient BIST circuit with diagnosis support and an automatic diagnostic system. The diagnosis module of our BIST circuit can capture the error syndromes as well as fault locations for the purposes of repair and fault/failure analysis. In addition, our design provides programmability for custom March algorithms with lower hardware cost. The combination of the on-line programming mode and diagnostic system dramatically reduces the effort in design debugging and yield enhancement. We have designed and implemented test chips with our BIST design. Experimental results show that the area overhead of the proposed BIST design is only 2.4% for a 128 KB SRAM, and 0.65% for a 2 MB one.     

中国电子商务思考

网络经济持续走低，但电子商务的发展大方向是不会改变的。在中国，目前的主要问题是宽带网的重复建设、认证机构建设缺乏有效监管、电子商务立法滞后、物流配送系统不完善、标准化问题成为电子商务发展的障碍等，当前应做的主要是：政策的宏观引导、示范推广、加强对宽带网和认证机构建设的监管等。