劣化环丁砜再生技术的工业应用

为解决国内外环丁砜抽提芳烃工艺中环丁砜的劣化问题，在不添加单乙醇胺的前提下，采用阴离子交换树脂处理劣化的环丁砜，可使系统的pH值从3．4升到5．5左右，离子交换树脂需30d左右再生一次，降低了设备的腐蚀，减少了装置的堵塞，使系统运行稳定，取得了可观的社会效益和经济效益。     

Influence of Shaping Condition on Etherification Performance of Hβ Zeolite

Etherification reaction of FCC light gasoline over Hβ zeolite was investigated to decrease the light olefins in motor gasoline while enhancing octane. Etherification activity of several molecular sieve catalysts for FCC light gasoline was studied in a fixed-bed reactor. The influence of pore-enlarging agent (PEG) with different molecular weight, binder (γ-Al₂O₃), and peptizing agent (HNO₃) in the shaping process on etherification activity of Hβ zeolite was studied. The impregnating ways of precursor of oxides and the order of extruding and impregnating were also investigated. The results show that the activity of extruded Hβ zeolite before impregnating precursor of oxides is higher than the reverse order. The best shaping condition obtained was PEG-4000 10%, γ-Al₂O₃ 20%, and HNO₃ 10%. At the optimal reaction condition, the conversion of tert-olefins reached the peak. 62.93%, the yield of TAME, is also high and the technology can be applied to industry as well.     

New approach to enhance adhesions between carbon nanotube emitters and substrate by the combination of electrophoresis and successive electroplating

Complementary electroplating combined with electrophoresis enhanced the field emission characteristics of emitters by improving the adhesions between CNT emitters and substrate. The emitting current of the CNT emitters prepared by our combined method increased nine times higher than that of CNT emitters prepared by electrophoresis only, since electroplating improved the adhesion of CNT emitters. During the life-time measurement for 10 h, the emitting current of CNT emitters fabricated by electrophoresis only was drastically decreased to 13% of the initial current, while that prepared by the combination of electrophoresis and successive electroplating decreased to 64% of the initial current. We suggest that our method is a promising approach for the efficient fabrication of reliable CNT emitters.     

湿法成形薄型陶瓷砖的干燥

分析了湿法成形薄型陶瓷砖干燥的特点．具体讨论了微波干燥和少空气干燥方式在湿法薄形陶瓷砖干燥上中应用及干燥过程中坯体传动方式的选择。     

两相管流工艺计算软件的研制

利用流体力学理论 ,结合目前国内外最新的两相流理论和实验研究成果 ,在描述气液两相流水力计算、热力计算和流型判断的数学物理模型基础上 ,研制出适用于海洋、沙漠、丘陵地区原油与伴生气、凝析天然气与凝液输送工艺的一套新的计算模拟软件TFTCS。介绍TFTCS软件的结构、功能、适用范围。用该软件对锦州 2 0 - 2海底湿天然气管道进行模拟计算 ,并与管线生产数据进行对比 ,用国外同类软件PIPEPHASE进行验算。实例计算分析表明 ,该软件功能完善 ,操作方便 ,计算结果可靠 ,能满足油气混输管道的设计计算和生产管理的需要     

浅谈城市道路立交的概念性方案设计

通过南昌市某快速路的设计实例，认识到搞好快速路沿线各交叉口的方案设计是快速路规划设计的关键内容。道路交叉口设计应注重交通功能分析，满足路口交通需求，同时也不能忽视立交的景观要求。     

Porosity distribution in highly compressible cake: Experimental and theoretical verification of the dense skin

The rate of filtration and the water content of cake are influenced by the existence of a dense skin in a highly compressible cake. The phenomenon of the dense skin has been rarely studied, and its existence has not been verified experimentally. In this study, the porosity variation in a very compressible cake is measured by using a new experimental apparatus, and with this the existence of dense skin has been established experimentally. ‘Unified theory on solid-liquid separation’, a recently developed theory, is utilized for calculating the porosity variation in a very compressible cake.     

碘量法标定二氧化硫和甲醛标准贮备溶液的改进

在国家标准测定方法的基础上,对碘量法标定二氧化硫和甲醛标准贮备液进行了改进.改进后的实验方法由分步标定变为一步标定,减少了试剂消耗,提高了实验效率.试验表明,改进后的标定方法与原国家标准方法有可比性,准确性有保证,可以广泛应用.     

Performance of GaAs-AlGaAs V-grooved inner stripe quantum-well wirelasers with different current blocking configurations

GaAs-AlGaAs V-grooved inner stripe (VIS) quantum-well wire (QWW) lasers grown by metalorganic chemical vapor deposition with different current blocking configurations, n-blocking on p-substrate (VIPS), p-n-p-n blocking on n-substrate (VI(PN)_nS) and p-blocking on n-substrate (VINS) have been fabricated and characterized. The VIPS QWW lasers show the most stable characteristics with effective current confinement: one of the lasers shows fundamental transverse mode, lasing up to 5 mW/facet, typical threshold current of 39.9 mA at 818.5 mm, an external differential quantum efficiency of 24%/facet, and characteristic temperature of 92 K. The current tuning rate was almost linear at 0.031 mm/mA, and the temperature tuning rate was measured to be 0.14 nm/°C. Comparison of the light output versus current characteristics of the lasers with different current blocking configurations is presented here