Room-temperature electroluminescence of p-ZnxMg（1-x）O：Na/n-ZnO p-n junction light emitting diode

p-ZnxMg1-xO：Na/n-ZnO p-n junction light emitting diode （LED） was produced on n-ZnO （0001） single-crystal substrate using pulsed laser deposition. The realization of band gap engineering was achieved by the incor-poration of Mg in ZnO layers and was confirmed by photoluminescence spectrum. The p-type ZnxMg1-xO：Na film with low resistance was obtained at 500 ℃ and in which, Na has taken effect evidenced by Hall and X-ray photo-electron spectroscopy measurements. The current-voltage curve of LED showed a rectifying behavior and obvious electroluminescence was realized by feeding a direct current up to 40 mA. Furthermore, its structural and electric characters are discussed as well.     

不同品种生鲜驴乳营养成分比较

对不同品种生鲜驴乳中常规营养成分,如脂肪、蛋白质、乳糖、干物质含量、维生素C、氨基酸和矿物质等进行比较分析。结果显示,不同品种鲜驴乳中蛋白质、脂肪、水分、干物质、乳糖、维生素C、滴定酸度和pH值变化范围分别为 1.38 g/100 g～ 1.77 g/100 g、0.75 g/100 g～ 1.08 g/100 g、88.89 g/100 g～ 90.64 g/100 g、9.38 g/100 g～ 12.64 g/100 g、4.32 g/100 g～5.56 g/100 g、2.01 g/100 g～3.12 g/100 g、4.48°T～4.74°T、7.09～7.18。德州黑驴生鲜乳显示出最高的氨基酸总量（1 867.89 mg/kg）,德州黑驴生鲜乳中的必需氨基酸显著高于疆岳驴、新疆驴、果拉驴（P<0.05）。德州黑驴生鲜乳中钙、硒含量较其他品种要高,而果拉驴生鲜乳中磷、锌含量较其他品种要高。     

Experience in pressing standard brick from clays and kaolins in thermoplastic state

Conclusions The pressing of argillaceous raw material reduced to a thermoplastic state by heating produces ultradense refractory of high quality.Standard brick made of 50% Vladimirovka kaolin, 3-1 mm, and 50% Chasov-Yar clay finer than 0.5 mm, pressed to 100 kg/cm² and at about 1380°, containing 40% Al₂O₃, shows a high degree of slag resistance and spalling resistance, and has an apparent porosity of 3% bulk density 2.52 g/cm³.     

Integrated UV-based photo microreactor-distillation technology toward process intensification of continuous ultra-high-purity electronic-grade silicon tetrachloride manufacture

Ultra-high-purity silicon tetrachloride (SiCl₄) is demanded as an electronic-grade chemical to meet the stringent requirements of the rapidly developing semiconductor industry. The high requirement for ultra-high-purity SiCl₄ has created the need for a high-efficient process for reducing energy consumption as well as satisfying product quality. In this paper, a mass of production technology of ultra-high-purity SiCl₄ was successfully developed through chlorination reaction in the ultraviolet (UV)-based photo microreactor coupled with the distillation process. The influences of key operational parameters, including temperature, pressure, UV wavelength and light intensity on the product quality, especially for hydrogen-containing impurities, were quantified by the infrared transmittance of Fourier transform infrared spectroscopy (FT-IR) at 2185 cm^-1 and 2160 cm^-1 indicating that characteristic vibrational modes of Si—H bonds, as well as the operating conditions of distillation were also investigated as key factors for metal impurities removing. The advanced intensification of SiCl₄ manufactured by the integration of photo microreactor and distillation achieves the products with superior specifications higher than the standard commercial products.     

形态滤波方法在抵肩力信号降噪中的应用研究

针对抵肩力实验信号采集过程中引入的噪声污染问题,基于数学形态学理论,提出了一种自适应多尺度形态学降噪方法。该方法采用形态开闭-闭开运算提取含噪信号的正、负冲击成分,根据不同尺度形态运算后的噪声统计分布,对不同尺度下形态运算的结果进行加权平均去噪,解决了细节保持与噪声滤波之间的矛盾。仿真实验以高斯白噪声干扰下的blocks信号为研究对象,信噪比和均方根误差为评定降噪结果的标准,结果表明该方法与传统阈值降噪方法相比具有更好的降噪效果。抵肩力实验结果的应用表明,该方法能够在有效抑制信号噪声的同时较好地保留抵肩力信号特征细节,为抵肩力信号特征的提取提供了一种降噪方法。     

刚性卵形弹丸对半无限厚铝合金靶的穿深方程

基于圆柱形空腔膨胀模型,将靶板变形所做的塑性功等效为刚性弹在整个侵彻过程所消耗的动能,对用于计算刚性卵形弹侵彻半无限厚铝合金靶板的侵深公式进行了推导.利用MTS万能试验机对2A12T4、6061T6、7075T6共3种铝合金材料进行了室温下的静态力学性能实验,得到了它们的真实应力-应变曲线,并将各参数代入侵深方程进行计...     

内膛损伤枪管对内弹道性能和弹头出膛状态的影响研究

为研究大口径机枪内弹道性能和弹头出膛状态受内膛损伤的影响规律,探究内膛损伤导致枪管寿终的关键因素,对某12.7 mm重机枪进行了系统的寿命试验。分析获得了该枪枪管内膛损伤的主要形式及其随射弹数增加在枪管轴向的分布及演化规律,在此基础上建立了精确的不同寿命阶段内膛损伤枪管的弹-枪热力耦合有限元模型。采用Fortran子程序实现了内弹道过程与显式有限元方法的迭代数值求解,获得了12.7 mm弹头内弹道性能及出膛状态等随内膛损伤发展的变化规律,将数值模拟结果与寿命试验数据进行对比验证了弹-枪耦合模型的准确性。仿真结果表明:弹头出膛时的扰动量、转速的下降量以及表面形貌的改变量等随枪管射弹数增加而增加,在身管寿命后期表现尤为明显;弹头出膛状态的改变是导致该枪枪管寿终的主要原因。研究结果对进一步分析内膛损伤引起的弹头外弹道性能退化行为,实现从内到外完整地分析枪管寿终机理具有重要意义。     

利用GPS载波相位的跟踪部位不一致修正方法

为提高外弹道测试中外弹道参数估计的精度,研究了利用非遥测和非弹道程序器数据的跟踪部位不一致的修正方法,阐述了利用GPS载波相位进行跟踪部位不一致修正的基本思想,结合外弹道测量的实际情况建立了以GPS载波相位双差数据为参数的修正模型,设计了相应的数据处理流程.仿真结果表明该模型和流程可行,该方法提高了外测系统数据的自处理和自鉴定能力.     

凝胶渗透色谱—气相色谱/质谱法测定塑料桶装食用油中四种邻苯二甲酸酯

建立用凝胶渗透色谱净化―气相色谱/质谱分析塑料桶装食用油中四种邻苯二甲酸酯类增塑剂方法。样品用环己烷―乙酸乙酯(体积比为1∶1)稀释,稀释液经Bio–Bead S–X3凝胶柱净化后,采用气相色谱―质谱在选择离子检测(SIM)模式下进行定性定量分析;结果表明,四种增塑剂在0.1 mg/L~5 mg/L范围内线性关系良好;在空白油样中添加四种增塑剂(添加水平为0.5 mg/kg、5 mg/kg、10 mg/kg)混合标准溶液,平均回收率为85.7%~108.2%,相对标准偏差为3.8%~9.2%,检出限为0.1 mg/kg~0.2 mg/kg。     

细特棉大麻混纺紧密竹节纱的试制

为试制细特棉大麻混纺紧密竹节纱,选用棉大麻混纺粗纱,在紧密纺改造的细纱机上采用竹节纱装置,试制出了棉/大麻65/35 9.7 tex混纺紧密竹节纱,并对影响成纱质量的捻度和紧密纺负压值两项工艺参数进行了试验优选.结果得出对于节长5 cm,竹粗200%,基纱长度11 cm,平均号数为9.7 tex的棉大麻紧密竹节纱,较优的工艺参数为捻度1 217.9捻/m,负压2 400 Pa.