Model of cold crystallization of uniaxially oriented poly(ethylene terephthalate) fibers

The differential scanning calorimeter heating curves of uniaxially oriented poly(ethylene terephthalate) (PET) fibers with three peaks were analyzed by using a newly proposed equation. The diffusion-controlled crystallization theory is suitable for describing cold crystallization of uniaxially oriented PET fibers. A crystallization model was proposed based on the kinetic parameters obtained. The model embraces the three sub-processes of crystallization corresponding to different growth geometries. The first sub-process corresponds to the nucleation of ordered molecular segments or the radial growth of preformed nucleus, resulting in the shorter bundle-like entities. The second sub-process corresponds to further growth of the bundle-like crystallites along chain direction, resulting in the longer bundle-like entities. The third sub-process corresponds to the three-dimensional growth of crystallites relating to the random segments, resulting in the spherical entities.     

Characterization of konjac glucomannan–quaternized poly(4‐vinyl‐N‐butyl) pyridine blend films and their preservation effect

Novel polymer blends were prepared from a mixture of 2 wt % konjac glucomannan and 4 wt % quaternized poly(4‐vinyl‐N‐butyl) pyridine (QPVP) in aqueous solution and dried at room temperature for 72 h. Their structure and properties were studied by infrared, wide‐angle X‐ray diffraction, scanning electron microscopy, thermogravimetric analysis, and differential scanning calorimetry. Thermal stability in the dry state was reduced with increasing content of QPVP. Compared with QPVP film, the tensile strength of the films was improved in the dry state. The maximum value of 12.74% tensile break elongation was reached when the content of QPVP was 30%. Structural analysis indicated that clear phase separation was observed when the content of QPVP was only 50%. Results from the filmcoating preservation experiments with lychee showed that this blend film had water‐holding ability. The fruit weight loss rate and rot rate both decreased in various degrees. The potential uses of these novel polymer films could be as preservative films. © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 93: 1868–1875, 2004     

全媒体时代新闻学专业实践教学模式的研究

全媒体时代,需要全媒体型新闻传播人才。新闻学专业教育者,要顺应时代要求,转变教育、教学观念,不断探索教学模式,加大实践教学内容比重,使课堂理论知识和实践教学环节相融合。营造多层次的实践平台,注重单项实践与综合实训相结合,增加"双师型"的教师比例,提高实践教学质量。     

基于MSP430单片机的灾害性天气预警管理系统设计

设计了基于MSP430单片机的灾害性天气预警管理系统,针对常见的雨量、风速及温度自然因素实现实时的监测,并对数据进行分析和处理,设置出相应的警报等级,并能根据警报的等级控制相应的三路设备。     

导磁体在汽车零件感应加热中的应用技术

本文简单介绍了导磁体工作的基本原理，并给出在汽车零件大规模生产中所积累的导磁体应用的一些经验，以阐明如何更有效地使用导磁体。     

EL-CID电磁铁心故障检测试验的应用研究

为了检验发电机定子铁心质量,在制造过程中和安装现场,对发电机定子铁心进行试验是必不可少的.目前国内针对定子铁心更多地是采用常规试验方法,但是常规铁损试验所需的设备容量大、试验线路复杂,而且经济性较差、效率低下.而采用电磁定子铁芯故障探测仪(EL-CID)铁心试验只需提供约4％的额定磁通量,即可完成对铁心故障的诊断,其所需的励磁电源容量较小且容易配备和携带.为了更好地利用EL-CID检测方式进行铁心质量的判定,本文通过模拟多种故障状况下的试验,论证了EL-CID的使用条件和影响因素,为实际工作中EL-CID的应用提供更好的参考依据.     

研究合金定向凝固组织的脉冲磁场设备的研制

介绍了脉冲电磁场发生设备的工作原理 ,设计等。并介绍了其如何与合金的定向凝固设备结合 ,以实现对合金的定向凝固组织在脉冲电磁场作用下的研究。     

Temperature stability and fracture toughness of Nd-Fe-B magnets

Temperature stability and toughness of magnets are very important properties especially for application in motor. In this paper, it is found that temperature stability and toughness of magnets are improved when Fe is substituted with Co andheavy rare earth is substituted for Nd in part and suitable rich B grain-boundary phase is added. In addition, heavy rare earth substitution decreases the remanence temperature coefficient greatly, but has a little effect on Curie temperature of the magnets, which is beneficial to Nd-Fe-B magnets for the application in motor.     

Sr对高铁Al-Si合金组织和性能的影响

研究了Sr元素（加入量分别为0．03％、0．06％、0．09％、0．12％和0．18％）对含Fe量为1．2％的ZL102合金的组织和性能的影响。研究发现，随着Sr元素的加入，合金中粗大的针状Fe相开始出现断裂分叉现象，同时针状Fe相的长度也随Sr元素加入量的增加而减小，但Sr对Fe相的针状形貌没有明显改变。随着Sr元素加入量逐渐增加，合金的抗拉强度和伸长率均呈现出先增后减的变化趋势。当Sr元素加入量达到0．12％时，合金材料的综合力学性能最佳。     

Performance of positive and negative electrodes in amorphous manganese oxide supercapacitor

Using potassium permanganate and acetic manganese as the reactants, amorphous manganese oxide was prepared with mechanochemical method. XRD was used for microstructure characterization, while cyclic voltammetry and constant current charge-discharge were used for electrochemical performance testing. The positive electrode （PE） and negative electrode （NE） were investigated respectively in amorphous manganese oxide supercapacitor, aiming to find their different performances in charging-discharging. The results show that the crystalline structure is destroyed in both the PE and NE material during charge-discharge process. Thereinto, the NE suffers a bit more seriously. When cycling, the PE potential scope diminishes while the NE potential scope enlarges. The increased inner resistance makes the NE curves almost bended to be a right angle, but not the PE curves. The cell＇s equivalent series resistance （ESR） is more dependent on the NE, and the capacitance is mainly determined by the rapid descent of the NE potential range. The capacitances of the NE are highly rate-dependent, decreasing from 121.3 to 53.1 F/g, by 56.2%, over the range of 5-25 mV/s. However, the PE appears to be weakly dependent and its capacitance is only dropped by 22.1%.