新颖在线痕量钠离子分析仪的研制

作者研制的在线痕量钠离子分析仪,根据能斯特响应的原理,以新颖的化学分析流路系统为核心技术,摒弃了传统技术形成的连续流动和手工标定的工作方式,借助于单片机技术,实现了间歇式静态测量和全自动标定的方式.经现场运行考核证明,该仪器工作可靠,具有自动化程度高、维护量小、运行成本低等特点,具有广阔的应用前景.     

煤基多孔炭材料的制备及其处理焦化废水的研究

以无烟煤为原料制备煤基多孔炭材料。考察了炭化温度及CO2流量对炭材料性能的影响,比较了粉末状和柱状炭材料对焦化废水中COD的去除效果。实验结果表明:当炭化温度为600℃,CO2流量为0.4L/min时,多孔炭材料的比表面积最大,为838.51m2/g。粉末状多孔炭材料处理焦化废水的效果更好,COD的去除率可达到72%。     

PVC抗冲改性剂-MBS树脂的生产技术及市场前景

介绍了目前PVC抗冲改性剂MBS树脂的生产技术、技术进展和国内外MBS树脂的生产、消费现状，分析了我国MBS树脂的发展前景，由于PVC制品的迅速发展、抗冲改性剂产品结构的调整，以及MBS树脂的应用领域不断拓宽，MBS的需求将越来越大，同时对我国MBS树脂生产的发展提出了一些建议。     

锻造镗孔技术在大口径厚壁无缝钢管生产中的应用

随着国内电力需求的迅猛增长,目前国内生产的大口径厚壁无缝钢管远不能满足市场需求,致使Φ159～1 066 mm规格范围的该类管大部分需进口。内蒙古北方重工集团公司特殊钢厂采用锻造镗孔工艺生产出高压锅炉用大口径厚壁无缝钢管。介绍了该产品的生产工艺与设备技术,对所生产的成品钢管各项性能的检测结果表明,产品质量稳定可靠,各项性能指标达到或超过相关标准的要求。     

单轴载荷下6063锻造铝合金的疲劳特性研究

研究了6063锻造铝合金单轴拉压载荷下的疲劳特性。结果表明,该材料的单轴疲劳特性对应力幅值有较大的依赖性。在应力幅值低于165MPa时,材料以弹性变形为主,当应力幅值达到198MPa时,塑性变形明显,同时,材料出现明显的循环硬化特征。     

高分子网络微区沉淀法制备纳米NiO粉体

采用高分子网络微区沉淀法制备了纳米级NiO粉体。该方法是以硝酸镍和尿素为原料，以丙烯酰胺为有机单体、以N，N＇-亚甲基双丙烯酰胺为交联剂，以过硫酸铵为引发剂，在水浴63℃中加热凝胶。采用TG—DTA、XRD、TEM等手段分析的结果表明：在600℃煅烧的粉体颗粒细小均匀，粒径在35-45nm，并且单分散性好。凝胶过程是在高分子网络内形成微区沉淀，且彼此独立，加热煅烧时在未发生团聚前分解，保证烧结粉体的单分散性，从而解决了其它方法普遍存在的团聚问题。     

Preparation of Y2O3：Eu^3＋ phosphor by molten salt assisted method

A kind of fine and quasi-spherical Y2O3：Eu^3＋ phosphor was prepared by firing a preparative precursor at 1 200 ℃ for 2 h with the molten salts of Na2CO3, S and NaCl. The precursor was obtained by homogeneous precipitation of yttrium and europium with oxalic acid when using EDTA, citric acid or starch as complexant. The structure and morphology of the phosphors were characterized by XRD and SEM, respectively. The influence of complexing environment, firing temperature and molten salts on formation of the phosphor Y2O3：Eu^3＋ was discussed. The result show that the prepared Y2O3：Eu^3＋ phosphor is of quasi-spherical structure with size of 2-3 μm. Its luminescent intensity is 30% higher than that of the same phosphor prepared by the same procedure but without molten salts, and is 5% higher than that of commercial Y2O3：Eu^3＋ red phosphor.     

AlSi7MgBe合金半固态挤压成形件的热处理工艺

采用正交设计方法，研究了固溶时效工艺参数对AlSi7MgBe合金半固态挤压成形件热处理性能的影响，通过对抗拉强度的测试，对热处理工艺进行了优化，结果表明：当545℃固溶4h，175℃时效11h，成形件具有最优力学性能σb=318MPa，δs=15．24％，此时析出相弥散地分布在基体上。     

微量Sr对AZ91D的铸态组织和性能的影响

研究了微量Sr对镁合金AZ91D的铸态组织和力学性能的影响。结果表明，添加微量Sr可以改变镁合金中口相（Mg17Al12）的形态，使镁合金的抗拉强度达到185．4MPa，比AZ91D提高11．3％，仲长率提高了139．3％，冲击韧度达到29J／cm^2，比不加Sr提高了12．5％，硬度则随着Sr含量的增加而提高。     

Soldering of Zr-based bulk metallic glass and copper by Au-12Ge eutectic alloy

Zr-based bulk metallic glass and copper with different surface roughness were soldered using low temperature eutectic Au-12 Ge(wt%) solder on a thermomechanical simulator. The cross-sectional microstructures of the brazed joints were analyzed by scanning electron microscopy(SEM) and transmission electron microscope(TEM) in detail, and the compositional distribution along the interface was analyzed by energy-dispersive spectrometer(EDS). Results show that the surface roughness of base metals plays an important role in the quality of the brazed joint because the surface roughness can enlarge the effective contact area, which can improve the brazing surface quality between two materials. A moderate roughness of treated Zr-based metallic glass of 18 μm is shown to be the best for the soldering, while the surface roughness has a weak effect on the soldering behavior of Au-12 Ge solder on copper. After soldering, long-range diffusion of atoms occurs between the base metal and solder, and five distinct regions are formed at the joint region.