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31.
Huiping Hu Qiyuan Chen Zhoulan Yin Pingmin Zhang Lusheng Ye 《Metallurgical and Materials Transactions A》2003,34(13):793-797
The thermal decompositions of mechanically activated and nonactivated galenas were studied by thermogravimetry analysis (TGA)
at the heating rate of 10 K min−1 in argon. Results indicate that the initial temperature of thermal decomposition (abbreviated as T
di) in the TGA curves for different galenas decreases gradually with increased grinding time. The specific granulometric surface
area (S
G), the structural disorder, and the content of elemental sulfur of mechanically activated galenas were analyzed by an X-ray
diffraction (XRD) laser particle-size analyzer, XRD analysis, and the gravimetric method, respectively, which shows that the
specific granulometric surface area of mechanically activated galenas remains almost constant after a certain grinding time,
but the lattice distortions (ε) rise, the crystallite sizes (D) decrease, and the elemental sulfur contents of mechanically activated galenas increase with increased grinding time. The
results imply that the decrease of the initial temperature of thermal decomposition in the TGA curves for mechanically activated
galenas is mainly caused by the increase of lattice distortions, and the formation of new dangling bonds resulted from the
production of elemental sulfur of mechanically activated galenas with increased grinding time. Finally, the differences in
the thermal-decomposition reactivity between nonactivated and mechanically activated galenas were also discussed. 相似文献
32.
33.
水性涂料VOC测定偏差对计算结果的影响 总被引:2,自引:0,他引:2
阐述水性涂料VOC的三项测定偏差对计算VOC结果的影响 ,指出国内现有标准的检测方法与国际标准方法存在的差距 相似文献
34.
H级干式变压器的现状及其发展前景 总被引:9,自引:1,他引:8
介绍了H级干式变压器的分类、NOMEX^R纸的技术性能、各类H级干式变压器的结构特点与技术性能,将H级干式变压器与环氧浇注式干式变压器进行了比较,并展望了H级干式变压器未来在我国的发展前景。 相似文献
35.
Chia‐Yin Chen Yu‐Chi Cheng Shau‐Wei Tsai 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2002,77(6):699-705
A lipase‐catalyzed enantioselective hydrolysis process under in situ racemization of the remaining (R)‐thioetser substrate with trioctylamine as the catalyst was developed for the production of (S)‐fenoprofen from (R,S)‐fenoprofen 2,2,2‐trifluoroethyl thioester in isooctane. Detailed investigations of trioctylamine concentration on the enzyme activation and the kinetic behavior of the thioester in racemization and enzymatic reactions were conducted, in which good agreement between the experimental data and theoretical results was observed. © 2002 Society of Chemical Industry 相似文献
36.
37.
Weitang Li Zhenghui Li Shifu Zhu Shujun Yin Beijun Zhao Guanxiong Chen 《Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment》1996,370(2-3):435-437
Instead of the temperature oscillation method (TOM), a modified vapor growth method was applied in this paper to grow large HgI2 crystals with fewer lattice defects by providing a relatively stable temperature field during growth. And a new processing technique of HgI2 crystals was developed for detector fabrication by merging solution string-sawing and hand-cleaving. The lattice deformations caused during cleaving were reduced greatly by eliminating passivated layers on the sawed crystal platelets before cleaving. 相似文献
38.
39.
A theoretical model is presented to describe the effect of ion beam bombardment rate on the formation of tetrahedral amorphous carbon (ta-C) films. The critical ion energy, Ec, corresponding to a 50% sp3 content in the films, is found to be dependent on both the effective thermal resistance and the ion beam bombardment rate. In the model, the ‘window’ width in the ion energy scale for the formation of ta-C material increases with decreasing deposition rate and with a reduction in the effective thermal resistance, until limited by lower and upper boundary thresholds. Experimental data are reproduced by the model. The plasmon energy, which correlates with sp3 fraction, is found experimentally of be higher for lower deposition rate and smaller effective thermal resistance. Data points for high sp3 content ta-C films deposited on silicon substrates at room temperature occupy a region in the ion energy-deposition rate (E-r) diagram similar to that predicated from the theory. 相似文献
40.
本文研究了经济分析基本方法之一最优等效替代法的实质,系统地导出了被评价方案的绝对经济指标与相对经济指标的关系,并结合典型案例分析指出了该方法的应用条件,对正确进行建设项目的经济评价具有现实意义。 相似文献