液态混合有机标准物质研究

本研究采用重量法配制有机液态混合标样 ,并对配制方法、混合标样的均匀性、稳定性及影响不确定度的因素进行了研究 ,并用气相色谱法进行了比对分析。经稳定性监测 ,稳定度大于等于一年 ,不确定度小于± 2 %。     

炼油污水浮选剂的优化

介绍炼油污水处理中几种浮选剂在实验室、放大试验及污水处理场试用中的处理效果和对比情况,优化选出两种高效的浮选剂XY-Ⅱ和PAFC,这两种高效的浮选剂形成絮凝体的速度快,产渣量少、成本低、除油效果好.     

丙烯压缩机振动偏高原因分析及解决方法

在丙烯腈生产过程中,发现其关键设备丙烯制冷压缩机轴振动值不断上升,针对此种情况对机组进行了分析与探讨,并制定解决方案。结果表明压缩机转子未采用正确的动平衡试验是造成轴振动的主要原因。采取正确的检维修方案是保证机组长周期运行、装置长周期运行的关键。     

La doping effects on intergrowth Bi2WO6–Bi3TiNbO9 ferroelectrics

La doping effects on intergrowth Bi₂WO₆–Bi₃TiNbO₉ ferroelectric ceramics were studied by X-ray diffraction, electron probe microanalysis and dielectric spectroscopy. It was found that the La³⁺ distribution, ferroelectric phase transition and dielectric relaxation behavior are apparently affected by La doping. With increasing La³⁺ content, the site of dopant ion varies, the grain growth of Bi₅TiNbWO₁₅ is restrained, the Curie temperature is reduced and broadened. Furthermore, two dielectric relaxation loss peaks were observed both in temperature and frequency spectra. The calculated relaxation parameters revealed the oxygen vacancy related to the relaxation process.     

品牌换标启示录

近几年国内外许多大品牌纷纷更换自己的标志，从柯达、富士到英特尔，从中国联通到腾讯网，从联想到创维，再到华为等，那么导致品牌换标的原因是什么？标志的再设计在其中起到一个怎样的作用？     

The thermal behavior of mechanically activated galena by thermogravimetry analysis

The thermal decompositions of mechanically activated and nonactivated galenas were studied by thermogravimetry analysis (TGA) at the heating rate of 10 K min⁻¹ in argon. Results indicate that the initial temperature of thermal decomposition (abbreviated as T _di) in the TGA curves for different galenas decreases gradually with increased grinding time. The specific granulometric surface area (S _G), the structural disorder, and the content of elemental sulfur of mechanically activated galenas were analyzed by an X-ray diffraction (XRD) laser particle-size analyzer, XRD analysis, and the gravimetric method, respectively, which shows that the specific granulometric surface area of mechanically activated galenas remains almost constant after a certain grinding time, but the lattice distortions (ε) rise, the crystallite sizes (D) decrease, and the elemental sulfur contents of mechanically activated galenas increase with increased grinding time. The results imply that the decrease of the initial temperature of thermal decomposition in the TGA curves for mechanically activated galenas is mainly caused by the increase of lattice distortions, and the formation of new dangling bonds resulted from the production of elemental sulfur of mechanically activated galenas with increased grinding time. Finally, the differences in the thermal-decomposition reactivity between nonactivated and mechanically activated galenas were also discussed.     

拉伸试验测量不确定度的研究

分析了拉伸试验中抗拉强度Rm的影响因素，对测量不确定度的主要分量进行量化，评定了Rm的相对测量不确定度，作为生产检验中评定测量不确定度的尝试，以便为用户提供钢材性能测量结果的不确定度。     

自蔓延高温合成TiNi多孔体合金

为了开发新型的生体材料，本文对自蔓延高温合成TiNi多孔体合金——人造骨材料进行了研究。以单质钛粉和镍粉作原料，在氩气保护条件下，采用预热点燃模式和热爆模式制得了不同形态的多孔TiNi形状记忆合金。采用SEM和XRD分析了样品的孔洞特征和相组成，测试了其力学性能，并研究了合成条件参数与样品表面形貌和孔隙状态之间的关系。结果表明，用SHS法制备TiNi多孔体合金是可行的。     

阜新市细河改造工程坝基渗漏计算及处理效果分析

阜新市细河改造工程由四座橡胶坝和两岸防洪大堤组成，由于堤(坝)基第四系冲洪积层广泛发育，存在渗漏同题。合理选择施工处理方案，是工程成功的关键。作者根据场区不同的地质条件环境条件采取有针对性的不同处理方案，既解决了防渗问题又缩短了施工工期，降低工程造价，取得了很好的经济效益和社会效益。     

Analysis and Optimization of the Energy Efficiency in the 802.11 DCF

This paper introduces an analytical model to investigate the energy efficiency of the IEEE 802.11 distributed coordinated function (DCF). This model not only accounts for the number of contending nodes, the contention window, but also the packet size, and the channel condition. Based on this model, we identify the tradeoff in choosing optimum parameters to optimize the energy efficiency of DCF in the error-prone environment. The effects of contention window and packet size on the energy efficiency are examined and compared for both DCF basic scheme and DCF with four-way handshaking. The maximum energy efficiency can be obtained by combining both the optimal packet size and optimal contention window. To validate our analysis, we have done extensive simulations in ns-2, and simulation results seem to match well with the presented analytical results. The Ohio Board of Regents Doctoral Enhancements Funds and the National Science Foundation under Grant CCR 0113361 have supported this work. Xiaodong Wang received his B.S. degree in communication engineering from Beijing Information Technical Institute of China in 1995, and his M.S. degree in electric engineering from Beijing University of Aeronautics and Astronautics of China in 1998. He joined China Telecom in 1998 where he worked on communication protocols for telecommunication. From June 2000 to July 2002, he worked on GSM base station software development at Bell-labs China, Beijing, China. Currently he is a Ph.D. student in Computer Engineering at University of Cincinnati. His research activities include wireless MAC protocols, energy saving for wireless sensor networks. He is a student member of the IEEE. Jun Yin received the BS degree in automatic control from Dalian Railway Institute of China in 1997, and the MS degree in flight control from Beijing University of Aeronautics and Astronautics of China in 2001. Since 2001 she has been a Ph.D. student in the OBR Research Center for Distributed and Mobile Computing at the University of Cincinnati. Her research interests include performance evaluation of 802.11 MAC protocol, wireless ad hoc networks and sensor networks. She is a student member of the IEEE. Dharma P.Agrawal IEEE Fellow, 1987; ACM Fellow, 1998; AAAS Fellow, 2003 Dr. Agrawal is the Ohio Board of Regents Distinguished Professor of Computer Science and Computer Engineering in the department of Electrical and Computer Engineering and Computer Science, University of Cincinnati, OH. He has been a faculty member at Wayne State University, (1977–1982) and North Carolina State University (1982–1998). He has been a consultant to the General Dynamics Land Systems Division, Battelle, Inc., and the U. S. Army. He has held visiting appointment at AIRMICS, Atlanta, GA, and the AT&T Advanced Communications Laboratory, Whippany, NJ. He has published a number of papers in the areas of Parallel System Architecture, Multi computer Networks, Routing Techniques, Parallelism Detection and Scheduling Techniques, Reliability of Real-Time Distributed Systems, Modeling of C-MOS Circuits, and Computer Arithmetic. His recent research interest includes energy efficient routing, information retrieval, and secured communication in ad hoc and sensor networks, effective handoff handling and multicasting in integrated wireless networks, interference analysis in piconets and routing in scatternet, use of smart directional antennas (multibeam) for enhanced QoS, Scheduling of periodic real-time applications and automatic load balancing in heterogeneous workstation environment. He has four approved patents and three patent filings in the area of wireless cellular networks.