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91.
Summary Plasma-polymerized membranes for gas separation were prepared from 1-(trimethylsilyl)-1-propyne. The permeation data of He, H2 02, N2, CO2, and CH4 through the membranes showed plasma-polymerized 1-(trimethylsilyl)-1-propyne had high permselectivity but low permeability compared with poly[l-(trimethylsilyl)-1-propyne]. This behavior is considered to be due to the crosslinking structure of the plasma-polymerized membrane. The correlation between plasma polymerization conditions and the membrane performance was studied. The optimum condition at which the deposition rate of the plasma polymer is maximized agreed with the optimum value to yield maximum separation factor of gases through the membrane. 相似文献
92.
Masahiko Shimada Ken'ichi Matsushita Shusei Kuratani Taira Okamoto Mjtsue Koizumi Koji Tsukuma Takaaki Tsukidate 《Journal of the American Ceramic Society》1984,67(2):23-C-
The temperature dependence of Young's modulus and internal friction (Q−1 )in alumina, silicon nitride, and partially stabilized zirconia (Y-PSZ) ceramics was studied. Little change in Q−1 was found for alumina, whereas Q−1 for silicon nitride ceramics increased above 700°C. The Q−1 of Y-PSZ increased markedly with increasing temperature up to a peak at ∼200°C. 相似文献
93.
A novel side-chain-sulfonated aromatic diamine of bis[4-(4-aminophenoxy)-2-(3-sulfobenzoyl)]phenyl sulfone (BAPSBPS) was synthesized. Sulfonated copolyimides were synthesized by random and sequenced block copolymerization of 1,4,5,8-naphthalene tetracarboxylic dianhydride, BAPSBPS and nonsulfonated diamine. They displayed good solubility in common aprotic solvents and high desulfonation temperature of 350 °C, suggesting the high stability of sulfonic acid groups. The reduced viscosity was in the range of 0.4-1.8 dl/g at 0.5 g/dl and 35 °C. Flexible and tough membranes with reasonably high mechanical strength were prepared. They showed anisotropic membrane swelling with larger swelling in thickness than in plane. They displayed reasonably high proton conductivity (σ), taking their lower ion exchanging capacity (IEC) into account. For example, the membrane with IEC of 1.54 mequiv/g showed σ values of 81 and 11 mS/cm in water and 70% RH, respectively, at 60 °C. 相似文献
94.
H. Okamoto 《Journal of Phase Equilibria and Diffusion》2006,27(4):429-429
95.
H Okamoto 《Journal of Phase Equilibria》1991,12(6):698-643
Several thermodynamic models for calculating binary phase diagrams published in the literature have been reevaluated. Problems
in some of these models are already evident in the models themselves and may also be seen in the resulting calculated phase
diagrams. When a calculation is attempted, thermodynamic models with quite different formulations may result in very similar
proposed phase diagrams. In such cases, if experimental data of a binary phase diagram can be represented reasonably well
by several different thermodynamic models, a simpler model often provides the clearest insight into the basic properties of
the system. If a calculated phase diagram results in unusual phase relationships, the adopted thermodynamic model may be inappropriate
or may involve unrealistic parameters. If the thermodynamic model is clearly unrealistic and yet the calculated phase diagram
appears to be normal, errors in calculation or in interpretation may be suspect. Various examples of unlikely combinations
of thermodynamic models and phase diagrams are discussed. 相似文献
96.
Journal of Phase Equilibria - 相似文献
97.
98.
Isamu Yamauchi Takashi Okamoto Hajime Ohata Itsuo Ohnaka 《Journal of Alloys and Compounds》1997,260(1-2):162-171
The effects of Cu addition on the β phase formation rate and the thermoelectric power in various FeSi2 and Fe2Si5 based alloys was examined. The peritectoid reaction (a+→β) in FeSi2 alloys was initially enhanced by the addition of Cu but it became slower for longer annealing times. The retained metallic ε was harmful for the thermoelectric power. The inherent thermoelectric properties of (FeSi2)99−XMn1CuX (X=0–1.O at.%), (FeSi2)99−X Co1CuX (X=0–1.0 at.%) alloys were attained after the elimination of ε. In the case of eutectoid reaction (→β+Si). Differential thermal analysis, X-ray diffraction and microscopic observation clearly confirmed that the eutectoid reaction rate was drastically enhanced by the addition of a small amount of Cu and its rate decreased with decreasing Cu content. The rate also depends on the annealing temperature and reached a maximum at about 1073 K for most alloys. The addition of only 0.1 at.% Cu was still very effective even in Mn or Co doped alloys. The thermoelectric power of these alloys increased very quickly with annealing time. Their final values decreased with Cu content and saturated at 0.2 at.% Cu. The value of the 0.1 at.% Cu added alloy was higher than that of both the conventional p- and a-type FeSi2 based alloys. These results suggest that the Fe2Si5 alloys with a small amount of Cu may be attractive as new thermoelectric materials. 相似文献
99.
100.
Journal of Phase Equilibria - 相似文献