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81.
The formation process of Ba2La8(SiO4)6O2 was clarified using thermogravimetry–differential thermal analysis (TG-DTA) and a high-temperature powder X-ray diffraction (HT-XRD) method. Phase changes identified from the HT-XRD data surprisingly corresponded to the weight loss and/or endothermic peaks observed in the TG-DTA curves. Raw material with the composition Ba2La8(SiO4)6O2 was completely reacted at 1400°C and produced only an apatite-type compound without a secondary phase. Moreover, the synthesis of Ba2+ x La8− x (SiO4)6O2−δ crystals with x = 0–2 was attempted using a solid-state reaction.  相似文献   
82.
The cyclic performance of a composite SiO and carbon nanofiber (CNF) anode was examined for lithium-ion batteries. SiO powder of several micrometers was pulverized using high energy mechanical milling. The SiO was ball-milled for 12 h with CNF to produce a composite electrode material that exhibited excellent cycling performance. A reversible capacity of approximately 700 mAh g−1 was observed after 200 cycles. The excellent cyclic performance was discussed with respect to the change of the valence state of Si by ball-milling. A large irreversible capacity at the first cycle for the SiO/CNF composite electrode was reduced to 2% by chemically pre-charging with a lithium film attached to the rim of the electrode.  相似文献   
83.
The thermal behaviors and the flame‐retardancy of styrene–ethylene–butadiene–styrene–block copolymer containing various additives were studied. The combustion was measured by the Underwriter laboratory (UL) test and cone calorimeter test and thermogravimetric analysis and program‐mass spectroscopy were applied to analyze the thermal behaviors. The blend with halogen additives showed the best result in the UL test. However, the blend with red‐phosphorous was the best in the cone calorimeter test. As the styrene sequence in the copolymer tended to degradate at a lower temperature, the major scission products spouted out from the polymer surface originated from polystyrene. The shorter the ignition times of the blends with red‐phosphorous were, the lower the peak heat release rates were. It was an interesting phenomenon because it suggested that the chemical structure of the residue changed to more stable polymers. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 104: 156–161, 2007  相似文献   
84.
Concentrations and depth distributions of the surface hydrogen and the surface deuterium in vacuum evaporated nickel layers and beryllium plates have been investigated by the ERDA method. It is shown that if the evaporation vacuum pressure is kept better than 10−6 Torr, the hydrogen adsorption from the residual gas during the evaporation is negligible and the hydrogen from residual or atmospheric gases after the evaporation is the main source of the surface hydrogen. Commercial beryllium plates are found to have surface hydrogen of about 1016 atoms cm2. Deuterium treated samples, either in D2 gas or heavy water, do not show more than possibly a partial replacement of hydrogen. The influence of substrates is small if the thickness of the evaporated nickel layer is more than 2000 Å. The measurements are in good agreement with previously published results.  相似文献   
85.
The steeping conditions for kernels affected the physicochemical properties of corn starch. Steeping in an alkaline solution minimized the nitrogen and phosphorus contents, while that in water and a sulfite solution gave high contents. The alkaline-steeping appeared to slightly reduce the crystallinity of starch granules, as judged on X-ray diffraction. Steeping at a low temperature produced the starch showing the lowest pasting temperature, on amylography, but it showed a similar gelatinization temperature, on photopastegraphy. to those of the other starches. The starches with low nitrogen and lipid contents swelled largely and were extensively solubilized on heating. The actual amylose contents were 20–21%, which were considerably lower than the apparent contents.  相似文献   
86.
The purpose of this research is to characterize the cryogenic delamination growth behavior in woven glass fiber reinforced polymer (GFRP) composite laminates subjected to Mode II fatigue loading. Mode II fatigue delamination tests were performed at room temperature, liquid nitrogen temperature (77 K) and liquid helium temperature (4 K) using the four-point bend end-notched flexure (4ENF) test method, and the delamination growth rate data for the woven GFRP laminates were obtained. The energy release rate range was determined by the finite element method. Microscopic examinations of the specimen sections and fracture surfaces were also carried out. The present results are discussed to obtain an understanding of the fatigue delamination growth mechanisms in the woven GFRP laminates under Mode II loading at cryogenic temperatures.  相似文献   
87.
Growth rate has a direct impact on the productivity of nitride LED production.Atmospheric pressure growth of GaN with a growth rate as high as 10μm/h and also Al0.1Ga0.9N growth of 1μm/h by using 4 inch by 11 production scale MOVPE are described.XRD of(002) and(102) direction was 200 arcsec and 250 arcsec, respectively.Impact of the growth rate on productivity is discussed.  相似文献   
88.
The transitional behaviors of myoblasts toward differentiation were investigated in the cultures at the low and high seeding densities (respectively, X0 = 1.0 × 103 and 2.0 × 105 cells/cm2). In the culture at the low seeding density, an increase in confluence degree accompanied a decrease in growth potential (Rp), being Rp = 0.85 and 0.11 at t = 48 and 672 h, respectively. Myoblasts seeded at the high density resulted in the immediate cessation of growth with keeping the low range of Rp = 0.02–0.09 throughout the culture. The reduction of Rp led to the generation of three subpopulations of cells in proliferative, quiescent and differentiated states. Close cell contacts in the confluent state of high seeding culture induced cell quiescence to a higher extent with suppressing differentiation.  相似文献   
89.
Recently, remote monitoring camera systems have been widely used for security. In such systems, one important function is that the system automatically detects any change in the scenes from the monitoring cameras. In wireless remote monitoring camera systems, the images of the scenes are generally transmitted as compressed data (e.g., JPEG file), because of the capacity of the wireless channel. This article shows the automated detection of the change point in time-series data of compressed JPEG file quantity (Kbytes) from the monitoring camera by applying the sequential probabilistic ratio test (SPRT) and the Chow test, which is well known as a standard method for detecting structural change in time-series data.  相似文献   
90.
The role of BGP inside an AS is to disseminate the routes learned from external peers to all routers of the AS. A straightforward, but not scalable, solution, is to resort to a full-mesh of iBGP sessions between the routers of the domain. Achieving scalability in the number of iBGP sessions is possible by using Route Reflectors (RR). Relying on a sparse iBGP graph using RRs however has a negative impact on routers’ ability to quickly switch to an alternate route in case of a failure. This stems from the fact that routers do not often know routes towards distinct next-hops, for any given prefix.In this paper, we propose a solution to build sparse iBGP topologies, where each BGP router learns two routes with distinct next-hops (NH) for each prefix. We qualify such iBGP topologies as NH-diverse. We propose to leverage the “best-external” option available on routers. By activating this option, and adding a limited number of iBGP sessions to the existing iBGP topology, we obtain NH-diverse iBGP topologies that scale, both in number of sessions and routing table sizes. We show that NH diversity enables to achieve sub-second switch-over time upon the failure of an ASBR or interdomain link. The scalability of our approach is confirmed by an evaluation on a research and a Service Provider network.  相似文献   
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