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71.
Girish Barot Michael R. Roner Yoshinobu Naoshima Kazutaka Nagao Kimberly Shahi Charles E. Carraher Jr. 《Journal of Inorganic and Organometallic Polymers and Materials》2009,19(1):12-27
A variety of dibutyltin polyethers have been synthesized employing the interfacial polymerization technique. The products
are polymers with degrees of polymerization ranging from 60 to 390. Infrared spectral and mass spectral results are consistent
with the proposed structure. The products show good inhibition of a variety of cancer cells including those associated with
bone, breast, prostrate, and lung cancers. Some also show good viral inhibition of the HSV-1 (herpes simplex) and Vaccina
(small pox) viruses with those derived from electron rich hydroquinone derivative being most active. Hydroquinone-derived
polymers containing electron withdrawing groups exhibit inhibition of a variety of gram positive and gram negative bacteria. 相似文献
72.
The visual clarity of a lighting environment is significantly affected by changing the general color rendering index (Ra) of its illumination. This effect has been studied by a number of researchers, but the cause of this effect has not been thoroughly studied. In order to clarify this, the mutual relations between visual clarity, lightness perception, and feeling of contrast are analyzed by using object colors under illuminations with various Ra values. the results obtained are as follows. (1) the visual clarity of a lighting environment is different from the lightness perception of the object colors in the environment. (2) the change in visual clarity of a lighting environment is highly correlated to a feeling of contrast between object colors under the illumination. (3) the effect of visual clarity is estimated effectively by assessing the feeling of contrast using a specially selected four-color combination. (4) the illuminance for equal visual clarity for any illumination is predicted by the equality of feeling of contrast under the same illumination specified by the gamut area made by the component colors of the four-color combination in a brightness and colorfulness space. (5) the effect of visual clarity under various illuminations cannot be predicted by using their Ra values. 相似文献
73.
74.
The degree of additivity‐law failure of a mixture color consisting of two component chromatic colors has very complex characteristics depending on the used component colors and their mixing conditions. It is significantly affected by the mixture‐color chromaticity and by the brightness/luminance ratio at the chromaticity. A simple relationship was derived between the following quantities: degree of additivity‐law failure, additivity‐law luminance (luminance of the mixture color derived by postulating additivity law), and brightness/luminance ratio at the chromaticity of the mixture color. This relationship can be applied to any additivity‐law failure experiment and any formula on brightness/luminance ratio. © 2002 Wiley Periodicals, Inc. Col Res Appl, 27, 185–190, 2002; Published online in Wiley Interscience (www.interscience.wiley.com). DOI 10.1002/col.10045 相似文献
75.
In eight separate experiments with laboratory silos, silages were prepared with 50 mmol caproic (nC6), isocaproic (iC6), valeric (nC5) and isovaleric (iC5) acid additions per kg Italian ryegrass or cocksfoot, and stored at 25°C for 70 days. In the nC6 and iC6 treatments, fermentation was consistently inhibited, and also the contents of water-soluble carbohydrates (WSC) were considerably higher in the silages than in the grasses. This increase in WSC was partly explained by the increase in glucose but the difference between WSC and “glucose + fructose” was clearly larger in the silages than in the grasses. In the nC5 and iC5 treatments, various results were obtained; in some cases, presumably due to high dry matter content, fermentation was inhibited and WSC increased, while, in one case, fermentation was improved with higher lactic acid and lower butyric acid production than in the control silage. According to the results of five experiments with bag silos, although the inhibition of fermentation was observed by the treatment with nC6, little or no increase in WSC during ensilage was found. 相似文献
76.
77.
High-performance genetic analysis on microfabricated capillary array electrophoresis plastic chips fabricated by injection molding 总被引:1,自引:0,他引:1
Dang F Tabata O Kurokawa M Ewis AA Zhang L Yamaoka Y Shinohara S Shinohara Y Ishikawa M Baba Y 《Analytical chemistry》2005,77(7):2140-2146
We have developed a novel technique for mass production of microfabricated capillary array electrophoresis (mu-CAE) plastic chips for high-speed, high-throughput genetic analysis. The mu-CAE chips, containing 10 individual separation channels of 50-microm width, 50-microm depth, and a 100-microm lane-to-lane spacing at the detection region and a sacrificial channel network, were fabricated on a poly(methyl methacrylate) substrate by injection molding and then bonded manually using a pressure-sensitive sealing tape within several seconds at room temperature. The conditions for injection molding and bonding were carefully characterized to yield mu-CAE chips with well-defined channel and injection structures. A CCD camera equipped with an image intensifier was used to monitor simultaneously the separation in a 10-channel array with laser-induced fluorescence detection. High-performance electrophoretic separations of phiX174 HaeIII DNA restriction fragments and PCR products related to the human beta-globin gene and SP-B gene (the surfactant protein B) have been demonstrated on mu-CAE plastic chips using a methylcellulose sieving matrix in individual channels. The current work demonstrated greatly simplified the fabrication process as well as a detection scheme for mu-CAE chips and will bring the low-cost mass production and application of mu-CAE plastic chips for genetic analysis. 相似文献
78.
Murayama Y Constantinou CE Omata S 《IEEE transactions on ultrasonics, ferroelectrics, and frequency control》2005,52(3):439-444
An ultrasound-based remote sensing method to evaluate the mechanical properties of materials is presented. This method consists of a disk-shaped, piezoelectric transducer, operating at its resonance frequency, and a phase-shifted, feedback circuit. Mechanical parameters are derived by analyzing the signal contained in the phase-shifted values of the reflected signal. It is concluded that, using this novel transducer system and signal processing, remote mechanical measurements can be made. Such measurements obviate the need to apply the force-deformation approach and may be used to enable stiffness imaging. 相似文献
79.
Bakalova R Zhelev Z Jose R Nagase T Ohba H Ishikawa M Baba Y 《Journal of nanoscience and nanotechnology》2005,5(6):887-894
The present study describes an enhancement of the photoluminescence of CdSe quantum dots under long-term ultraviolet irradiation in organic solvents. The photoenhancement effect followed multiexponential kinetics and was found to depend on several factors: intensity of ultraviolet light, polarity of the solvent, presence of capping agents on the nanocrystal surface, and presence of free Cd and Se ions in the solution. High intensity ultraviolet irradiation provoked a rapid enhancement of the photoluminescence of CdSe nanocrystals, reaching the maximum with subsequent photoluminescence decay. Low-intensity ultraviolet irradiation provoked a comparatively slow enhancement of the photoluminescence of CdSe nanocrystals, reaching saturation after 5-6 hours of irradiation in organic solvents (butanol and chloroform). The photoenhancement effect was reversible or irreversible depending on the additional ingredients. The role of free Cd and Se in these processes was clarified. The results are discussed in the context of ultraviolet induced liberation of free Cd and Se ions from the nanocrystal surface and their hypothetical reversible deposition with trapping of the surface holes and influencing the efficiency of radiative versus nonradiative exciton decay during the enhancement of photoluminescence. 相似文献
80.
Yoshinobu Nakamura Hiroaki Honda Atsushi Harada Syuji Fujii Kazuya Nagata 《应用聚合物科学杂志》2009,113(3):1507-1514
The surface treatment of spherical silica particles with a silane coupling agent with mercapto groups was carried out. The treated silica particles were incorporated within polyisoprene and then vulcanized. The effects of the loading amount and alkoxy group number of silane on the stress–strain curve of the filled composite were investigated. For this purpose, silanes with dialkoxy and trialkoxy structures were used. The loading amount of silane on the silica surface was varied from 1 to 8 times the amount required for monolayer coverage. The stress at the same strain increased with the silane treatment, and it was higher in the dialkoxy structure than in the trialkoxy structure above 300% strain. There was no significant influence of the loading amount on the stress for the trialkoxy silane structure. However, the stress was influenced by the loading amount, and the maximum stress was observed at 4 times the silane amount required for monolayer coverage for the dialkoxy structure. The stress had a good relationship with the crosslinking density of silica‐filled polyisoprene rubber (measured with a swelling test). The reinforcement effect by the silane treatment of silica was found to be affected strongly both by the entanglement of the silane chain and polyisoprene rubber matrix and by the crosslinking reaction between the mercapto group of silane and polyisoprene rubber in the interfacial region. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2009 相似文献