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91.
92.
Nucleation effects of 2,2′‐methylene‐bis (4,6‐di‐tert‐butylphenyl) phosphate metal salts as a nucleating agent for isotactic polypropylene (iPP) were investigated with differential scanning calorimeter and polarized optical microscope, and their effects on mechanical, optical, and heat resistance properties of iPP were also studied. The results showed that monovalent metal salts of substituted aromatic heterocyclic phosphate such as sodium salt, lithium salt, and potassium salt had a good performance. With 0.2 wt % of sodium salt, lithium salt, or potassium salt incorporated into iPP, the crystallization peak temperature of iPP could be increased by 13.5, 13.6, and 15.0°C, respectively; the mass fraction of crystallinity of iPP could be increased by about 5%; and crystallization rate was enhanced increasingly. Meanwhile the tensile strength and flexural modulus of iPP could be increased by about 10 and 30%, respectively, and the clarity and heat distortion temperature of iPP could also be improved significantly. But bivalent and trivalent metal salts of substituted aromatic heterocyclic phosphate had little effect on properties of iPP. Meanwhile the morphology study showed that the addition of monovalent sodium salt could decrease the spherulite size of iPP significantly. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 4868–4874, 2006 相似文献
93.
高校基本建设项目的投资成本发生在项目建设的各个过程之中。项目建设的全过程都应该控制投资成本。在可行性研究和设计等前期,应该执行限额设计的目标管理制度。在施工期间应该严格执行合同,对工程签证、工期等实行严格控制。付款方式也是投资成本控制的有效手段。 相似文献
94.
Preparation of carbon
nanotubes/hydrogenated nitrile rubber composite by ultrasonic technique 总被引:1,自引:0,他引:1
将低相对分子质量的液体氢化丁腈橡胶(HNBR)溶于丙酮溶剂中,加入碳纳米管,用超声波技术制备了液体HNBR与碳纳米管的复合母料,然后再与HNBR混炼、硫化,获得碳纳米管/HNBR复合材料.结果表明,碳纳米管在HNBR中分散性好,对HNBR有较好的增强性,但在后期机械加工中产生了断裂. 相似文献
95.
化工项目环境影响评价工程分析的思考 总被引:1,自引:0,他引:1
本文通过实例分析,对化工项目环境影响评价工程分析的内容、方法等进行探讨.根据化工项目的特点,提出化工项目环境影响评价工程分析必须增加的内容和重点,以及在工程分析方法上要注意的问题. 相似文献
97.
98.
The pH mediated intra-molecular association and inter-molecular aggregation of a range of amphiphilic poly(l-lysine iso-phthalamide) polymers have been investigated in aqueous solution over a range of pH values and concentrations. The desired functionality of these novel bioresponsive amphiphilic polymers was achieved by incorporating pendant hydrophilic carboxyl groups along the polymer backbone, via the l-lysine moiety, balanced by a degree of hydrophobicity introduced via the iso-phthaloyl moiety. Incorporation of low levels of bis-functional Cy3 (poly-Cy3) and/or Cy5 dye (poly-Cy3/5 or poly-Cy5) co-monomers in the responsive polymer backbone allowed detailed probing of the pH mediated hydrophobic association using a combination of optical spectroscopic techniques. Both steady-state fluorescence spectroscopy and fluorescence lifetime measurements of poly-Cy3 revealed a conformational transition at pH 4.5. Thus, below a critical pH the polymer collapsed into a compact globular structure (hypercoil) bringing the fluorophore molecules into close proximity with one another. This resulted in a dramatic reduction in fluorescence intensity and fluorescent lifetime in the single fluorophore systems (poly-Cy3) accompanied by a red shift in the maximum emission wavelength. Observed redshifts in the emission maxima and enhancements of fluorescent lifetimes with increasing polymer concentration suggested the formation of polymer aggregates. Fluorescence resonance energy transfer (FRET) was measured in mixtures of single fluorophore containing poly-Cy3 (donor) and poly-Cy5 (acceptor) and dual fluorophore containing poly-Cy3 (donor)/Cy5 (acceptor) in an effort to distinguish between intra-molecular versus inter-molecular association. The relevance of the results with respect to potential in vivo applications (drug delivery and biodiagnostics) is discussed. 相似文献
99.
使用毛细管电泳分离并定量分析了对苯二酚——— 1种黑白显影液中的显影剂和它的衰退反应产物对苯二酚单磺酸盐。优化了的毛细管电泳分离。 相似文献
100.
Chengyun Yue J. Milton Harris Per-Erik Hellberg Karin Bergstrom 《Journal of the American Oil Chemists' Society》1996,73(7):841-845
A series of noncyclic acetal-linked cleavable surfactants were simply prepared by condensation of aldehydes with poly(ethylene
glycol) monomethyl ethers. All of the products were characterized by1H nuclear magnetic resonance. Their hydrophile-lipophile balance, surface tension, cloud point, critical micelle concentration,
and foam height were determined. Hydrolysis kinetic studies, followed by gas chromatography, showed that they had higher hydrolytic
reactivity in acidic solution than cyclic acetal-linked cleavable surfactants. 相似文献