浅议铵梯炸药质量检验中的三个问题

文章探讨了GB 12437-2000标准规定的产品检验项目中,中包浸水试验的科学性问题和对批产品进行抽样时的样本代表性问题以及使用多段爆速仪测试爆速时应注意的样本量问题.     

台州市"20020913"特大暴雨洪水分析及思考

2002年9月13-14日，台州市受18号强热带风暴“黑格比”减弱后的低压环流的外围影响，台州温岭-路桥-黄岩-杜桥-线普降大到特大暴雨，灾情严重。这场暴雨的特征是历时短、强度高、笼罩面积小，是台州历史上罕见的平原大暴雨。通过对这场暴雨洪水特性和水利工程所发挥作用的分析，揭示暴雨的成因和特性，提出几点思考。     

未增塑聚氯乙烯(PVC-U)异型材配方基础

PVC-U异型材配方十分复杂,常用原料通常在10种以上。根据大连实德集团实际生产情况,这10多种原料通常以7大组分的方式进行配料和生产。文中就该配方中7大组分的分类、特点及应用情况分别进行了详细介绍。     

汽车漆漆膜质量的改进与提高

通过对车身漆膜质量问题的分析,采取专业清洁公司整体承包车间保洁、工艺方面改进、更换生产外材料、供应商加强对汽车漆使用的监控等一系列措施,漆膜质量水平得以提高.     

风管摩擦阻力的直接计算方法

提出用高精度的反映密度、黏度和温度关系的经验公式和Colebrook公式计算风管摩擦阻力系数的方法。分析和算例表明，用该方法计算，计算结果比采用常用工程设计方法更为准确，为应用计算机进行风道设计提供了直接、简便的方法。     

Hydrothermal Reaction Mechanism and Pathway for the Formation of K2Ti6O13 Nanowires

Calculations and detailed first principle and thermodynamic analyses have been performed to understand the formation mechanism of K₂Ti₆O₁₃ nanowires (NWs) by a hydrothermal reaction between bulk Na₂Ti₃O₇ crystals and a KOH solution. It is found that direct ion exchange between K⁺ and Na⁺ plus H⁺ interactions with [TiO₆] octahedra in Na₂Ti₃O₇ promote the formation of an intermediate H₂K₂Ti₆O₁₄ phase. The large lattice mismatch between this intermediate phase and the bulk Na₂Ti₃O₇ structure, and the large energy reduction associated with the formation of this intermediate phase, drive the splitting of the bulk crystal into H₂K₂Ti₆O₁₄ NWs. However, these NWs are not stable because of large [TiO₆] octahedra distortion and are subject to a dehydration process, which results in uniform K₂Ti₆O₁₃ NWs with narrowly distributed diameters of around 10 nm.     

Structural transformation of FePt nanocomposite films during annealing and its effects on magnetic properties

Fe100-xPtx(x=30at.%-60at.% ) nanocomposite films were deposited on natural-oxidized Si(100) substrates by magnetron sputtering. The as-deposited films were annealed between 373 and 1073 K. In situ X-ray diffraction shows that the FePt nanocomposite films undergo a phase transformation from a disordered FCC phase to an ordered L10 phase between 673 and 773 K. The coercivity is 306 kA·m-1 whiles the average grain sizes is about 10 nm in the optimized FePt alloy film sample annealed at 673K. The adjustable coercivity and fine grain size suggest that this FePt nanocomposites system is suitable as recording media at extremely high areal density.     

A Study on NMR and GC/MS Spectra of the Isomers of Linear Hexyl Naphthalene

The GC/MS and NMR analysis of the reaction products of naphthalene with 1-bromohexane were reported. The products obtained were suggested to have six isomers of linear hexylnaphthalene and the structure of each isomer was determined by GC/MS and NMR spectra. For the first time, the unique chemical shift data were obtained. The content of each isomer calculated by ¹H NMR and ¹³C NMR spectra was consistent with that by GC/MS spectra, which confirmed the accuracy of NMR data.