The Effect of the Estimation on Goodness‐of‐Fit Tests in Time Series Models

Abstract. We analyze, by simulation, the finite‐sample properties of goodness‐of‐fit tests based on residual autocorrelation coefficients (simple and partial) obtained using different estimators frequently used in the analysis of autoregressive moving‐average time‐series models. The estimators considered are unconditional least squares, maximum likelihood and conditional least squares. The results suggest that although the tests based on these estimators are asymptotically equivalent for particular models and parameter values, their sampling properties for samples of the size commonly found in economic applications can differ substantially, because of differences in both finite‐sample estimation efficiencies and residual regeneration methods.     

Preparation of BaMgAl10O17∶Eu2+ and Its Phase Behavior in Microemulsion System

BaMgAl10O17∶Eu2 (BAM) was prepared in the microemulsion system and its phase behavior was studied. There exists a small region in the reverse microemulsion system where the dispersed particles are of spherical form. In this way, BAM blue phosphor with good dispersion can be synthesized. The microemulsion phase diagrams of the pseudo-ternary system (Triton X-100/cosurfactant-oil-BAM brine) were first established intuitively by the dilution method. The microstructure of microemulsions was determined through eyeballing, conductance technique, and polar optical microscopy. Its phase behavior is affected by various factors, such as temperature (room temperature, 30, 40 ℃), oil, surfactants, and cosurfactants in microemulsions. According to the phase diagrams, the microemulsion system of Triton X-100/1-hexanol-hexane-BAM brine was chosen to prepare the precursor. The BAM phosphor can be obtained via sintering the precursor at a comparatively low temperature. The phosphors were characterized by XRD and vacuum ultraviolet (VUV) spectra.     

基体温度对磁控溅射沉积ZAO薄膜性能的影响

利用中频交流磁控溅射方法 ,采用氧化锌铝陶瓷靶材 [w(ZnO) =98%、w(Al2 O3 ) =2 % ]制备了ZAO(ZnO∶Al)薄膜 ,观察了基体温度对ZAO薄膜的晶体结构、电学和光学性能的影响 ,采用X射线衍射仪对薄膜的结构进行了分析 ,采用光学分度计和电阻测试仪测量了薄膜的光学、电学特性 ,采用霍尔测试仪测量了薄膜的载流子浓度和霍尔迁移率。结果表明 :沉积薄膜时的基体温度对薄膜的结构、结晶状况、可见光透射率以及导电性有较大的影响。当基体温度为 2 5 0℃ ,Ar分压为 0 8Pa时 ,薄膜的最低电阻率为 4 6× 10 -4Ω·cm ,方块电阻为 35Ω时 ,可见光 (λ =5 5 0nm)透射率高达 92 0 %。     

Structural transformation of FePt nanocomposite films during annealing and its effects on magnetic properties

Fe100-xPtx(x=30at.%-60at.% ) nanocomposite films were deposited on natural-oxidized Si(100) substrates by magnetron sputtering. The as-deposited films were annealed between 373 and 1073 K. In situ X-ray diffraction shows that the FePt nanocomposite films undergo a phase transformation from a disordered FCC phase to an ordered L10 phase between 673 and 773 K. The coercivity is 306 kA·m-1 whiles the average grain sizes is about 10 nm in the optimized FePt alloy film sample annealed at 673K. The adjustable coercivity and fine grain size suggest that this FePt nanocomposites system is suitable as recording media at extremely high areal density.     

Space–Time Power Schedule for Distributed MIMO Links Without Instantaneous Channel State Information at the Transmitting Nodes

A space-time optimal power schedule for multiple distributed multiple-input multiple-output (MIMO) links without the knowledge of the instantaneous channel state information (CSI) at the transmitting nodes is proposed. A readily computable expression for the ergodic sum capacity of the MIMO links is derived. Based on this expression, which is a non-convex function of power allocation vectors, a projected gradient algorithm is developed to optimize the power allocation. For a symmetric set of MIMO links with independent identically distributed channels, it is observed that the space-time optimal power schedule reduces to a uniform isotropic power schedule when nominal interference is low, or to an orthogonal isotropic power schedule when nominal interference is high. Furthermore, the transition region between the latter two schedules is seen to be very sharp in terms of nominal interference-to-noise ratio (INR). For MIMO links with correlated channels, the corresponding space-time optimal power schedule is developed based on the knowledge of the channel correlation matrices. It is shown that the channel correlation has a great impact on the ergodic capacity and the optimality of different power scheduling approaches.     

提高自来水水质的策略

一、前言 供水公司分为四类。第三、四类公司供水50×104 m~3/d以下,要求其供水水质符合国家标准GB/5749-85“生活饮用水卫生标准”;供水100×104 m~3/d以下的第二类水司供水水质要达到80年代国际水平;供水100×104m~3/d以上的直辖市、对外开放城市、重点旅游城市要达到     

宏蜂窝模型的传播模型校正研究

详细介绍了 宏蜂窝传播模 型校正的基本操作流程 结果分析及注意事项 对工程 ,人员了解和开展模型校正工作有一定的指导作用 。     

Analysis and synthesis of on-chip spiral inductors

This paper presents a physically based compact model for estimating high-frequency performance of spiral inductors. The model accurately accounts for skin and proximity effects in the metal conductors as well as eddy current losses in the substrate. The model shows excellent agreement with measured data mostly within 10% across a variety of inductor geometries and substrate dopings up to 20 GHz. A web-based spiral inductor synthesis and analysis tool COILS, which makes use of the compact models, is presented. An optimization algorithm using binary searches speeds up the synthesis of inductor designs.     

Ozonation of CI Reactive Black 5 using rotating packed bed and stirred tank reactor

This study investigates the ozonation of CI Reactive Black 5 (RB5) by using the rotating packed bed (RPB) and completely stirred tank reactor (CSTR) as ozone contactors. The RPB, which provides high gravitational force by adjusting the rotational speed, was employed as a novel ozone contactor. The same ozone dosage was separately introduced into either the RPB or the CSTR for the investigation, while the experimental solution was continuously circulated within the apparatus consisting of the RPB and CSTR. The decolorization and mineralization efficiencies of RB5 in the course of ozonation are compared for these two methods. Moreover, the dissolved and off‐gas ozone concentrations were simultaneously monitored for the further analysis. As a result, the ozone mass transfer rate per unit volume of the RPB was significantly higher because of its higher mass transfer coefficient and gas–liquid concentration driving force. Furthermore, ozonation kinetics was found to be independent of the gravitational magnitude of an ozone gas–liquid contactor. Therefore, the results suggest employing RPBs as ozone‐contacting devices with the advantage of volume reduction. The experimental results, which can be used for further modeling of the ozonation process in the RPB, also show the requirement of correct design for the RPB. Consequently, the present study is useful for the understanding of practical application of RPBs. Copyright © 2004 Society of Chemical Industry     

掺钛蓝宝石激光晶体中夹杂物的分析

本文用大视场光学显微镜、电子探针观察和分析了掺钛蓝宝石激光晶体中夹杂物的形状、尺寸大小及元素组成，并提出消除和减少这些夹杂物的方法．