Orientation dependence of dielectric and relaxor behaviour in Aurivillius phase BaBi2Nb2O9 ceramics prepared by spark plasma sintering

Grain-oriented Aurivillius phase BaBi₂Nb₂ O₉ ceramics were fabricated using Spark Plasma Sintering (SPS). Their relaxor behaviour was confirmed by a strong frequency dispersion of the dielectric response. The dielectric behaviour has been fitted using different relaxor models. The relaxor parameters are isotropic, while the dielectric constants are highly anisotropic. The piezoelectric constant d ₃₃ is zero perpendicular and parallel to the hot pressing direction, and the P–E response is dominated by losses. The inability to pole the samples at room temperature is consistent with the T _f temperature (∼ ∼115 K) estimated from fitting the experimental data to the Vogel–Fulcher model. This suggests that it may be possible to observe piezoelectric and ferroelectric properties at very low temperatures.     

Recurrent Radial Basis Function Network-Based Fuzzy Neural Network Control for Permanent-Magnet Linear Synchronous Motor Servo Drive

We propose a recurrent radial basis function network-based (RBFN-based) fuzzy neural network (FNN) to control the position of the mover of a field-oriented control permanent-magnet linear synchronous motor (PMLSM) to track periodic reference trajectories. The proposed recurrent RBFN-based FNN combines the merits of self-constructing fuzzy neural network (SCFNN), recurrent neural network (RNN), and RBFN. Moreover, it performs the structureand parameter-learning phases concurrently. The structure learning is based on the partition of input space, and the parameter learning is based on the supervised gradient descent method, using a delta adaptation law. Furthermore, all the control algorithms are implemented in a TMS320C32 DSP-based control computer. The simulated and experimental results due to periodic reference trajectories show that the dynamic behaviors of the proposed recurrent RBFN-based FNN control system are robust with regard to uncertainties     

The effect of carbon precursor on the pore size distribution of mesoporous carbon during templating synthesis process

The starch and cyclodextrin were selected as the precursors and the mixture of surfactant and tetraethyl orthosilicate (TEOS) as template to prepare mesoporous carbon. The result showed that a bimodal pore size distribution in mesoporous carbon derived from starch appeared; one was around 3.4 nm and the other ranged from 3.8 to 16.2 nm. However, there existed a concentrated pore size distribution from 3.2 to 4.2 nm in mesoporous carbon derived from cyclodextrin. The different molecular structure of starch and cyclodextrin and their polymerization process in the presence of sulfur acid were responsible for the resulted mesoporous carbon structure; the starch could polymerize by head to head or side by side, but the cycleodextrin was only polymerized by head to head.     

Cooling rate effects on the microstructure and phase formation in Zr51Cu20.7Ni12Al16.3 bulk metallic glass

A detailed transmission electron microscope (TEM) study has been conducted to investigate the microstructures of the Zr₅₁Cu_20.7Ni₁₂Al_16.3 metallic glass formed at different cooling rates. It has been found that the most competitive crystalline phase to the amorphous structure is an oxygen-stabilized FCC NiZr₂-type phase, which in turn acts as the leading phase to trigger the formation of other crystalline phases in the slow-cooled alloy.     

Substrate temperature dependent morphology and resistivity of pulsed laser deposited iridium oxide thin films

Iridium oxide (IrO₂) thin films were deposited on Si (100) substrates by means of pulsed laser deposition technique at various substrate (deposition) temperatures ranging from 250 to 500 °C. Effects of substrate temperature on the crystalline nature, morphology and electrical properties of the deposited films were analyzed by using X-ray diffraction, Raman spectroscopy, Scanning electron microscopy and four-point probe method. It was found that the above properties were strongly dependent on the substrate temperature. The as-deposited films at all substrate temperatures were polycrystalline tetragonal IrO₂ and the preferential growth orientation changed with the substrate temperature. IrO₂ films exhibited fairly homogeneous thickness and good adhesion with the substrate, the average feature size increases with the substrate temperature. The room-temperature resistivity of IrO₂ films decreased with the increase of substrate temperature and the minimum resistivity of (42 ± 6) μΩ cm was obtained at 500 °C. The resistivity of IrO₂ films correlated well with the corresponding film morphology changes.     

Hemocompatibility of lanthanum oxide films fabricated by dual plasma deposition

Lanthanum oxide films were fabricated using dual plasma deposition. X-ray photoelectron spectroscopy (XPS) showed that La existed in the + 3 oxidation state. X-ray diffraction (XRD) revealed a (101) oriented hexagonal structure. Blood platelet adhesion tests and endothelial cell cultures were used to evaluate the hemocompatibility of the as-deposited films. Scanning electron microscopy (SEM) and optical microscopy were employed to evaluate the surface morphology of the blood platelets and endothelial cells on the films. The results showed that the number of adhered, aggregated and morphologically changed platelets was reduced compared to that observed on low-temperature isotropic carbon (LTIC). Endothelial cells culture tests indicated good adhesion and proliferation of human umbilical vein endothelial (HUVE) cells in vitro. Our study suggests that lanthanum oxide films are potential blood-contacting biomedical materials.     

Solid-state interfacial reactions and compound morphology of cBN grain and surface Ti coating

In order to research thoroughly the mechanism of the solid-state interfacial reactions and the induced compound morphology of cubic boron nitride (cBN) abrasive grains and the surface Ti-coating layer, annealing experiments of Ti-coated cBN grains were conducted at different temperatures of 550-950 °C for dwell times of 60 min under high-vacuum conditions. The corresponding interfacial characteristics were investigated by differential thermal analysis, X-ray diffraction and scanning electron microscopy. The results show that the relevant interfacial reactions and compound morphology between cBN and Ti are significantly influenced by the heat-treatment temperature. No reaction occurs below 550 °C, and TiN is the sole reaction product during heating from 650-750 °C. Three kinds of compounds, TiN, TiB₂ and TiB, can exist in the interfacial region at 950 °C. Here, the favorable interfacial structures, cBN/TiB₂/TiB/(TiB+TiN)/TiN/Ti, are developed for the excellent mechanical and chemical transition effects between cBN grains and Ti coating. The thermodynamic analysis finally predicts that there is a reasonable probability for the formation of such a special interfacial transition layer.     

澳大利亚插头产品标准及测试的分析

文章介绍了澳大利亚的插头产品的标准、测试要点，主要的标准要求，以及易出现不合格的情况，以期给出使用澳洲插头的有益指引．     

SA213-T91钢焊接工艺理论分析及焊接过程控制

针对国产600 MW亚临界机组锅炉末级过热器采用焊接性能较差的SA213-T91钢材。着重阐述该钢材的焊接工艺性能及施工过程控制,以保证SA213-T91小径管焊接接头获得良好的显微组织及优良的综合性能,提高机组运行可靠性。     

一种基于Nios II的喷涂控制系统设计方案

文中介绍基于NiosII处理器的嵌入式改进喷涂控制系统的实现。该系统通过在SOPC加载Nios软核和相应的外围电路,利用FPGA开发板和NiosII的定制指令来实现。该系统具有开发周期短、成本低、易于实现等优点。