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11.
Antibacterial poly{(4‐vinyl phenylboronic acid)‐co‐[2‐(dimethylamino)ethyl methacrylate]} copolymers and their application in water‐based paints 下载免费PDF全文
Hüseyin Cicek Gökhan Kocak Özgür Ceylan Emir Ahmet Kutluca Zeynep Dikmen Vural Bütün 《应用聚合物科学杂志》2018,135(22)
Herein, we report the synthesis of poly(4‐vinylphenylboronic acid) (PVPBA) and poly[2‐(dimethylamino)ethyl methacrylate] (PDMAEMA) homopolymers, copolymers, and their methyl, pentyl, and octyl quaternized forms as dopant in water‐based permanent antibacterial paints. Both quaternized and nonquaternized forms of P(VPBA‐co‐DMAEMA) copolymers have reflected higher MIC values relative to PDMAEMA homopolymers. High molecular weight copolymers were more active against Escherichia coli ATCC 25922, contrarily, lower molecular weight copolymers showed higher antibacterial activity against Staphylococcus aureus ATCC 25923. The paint films prepared with quaternized PDMAEMA homopolymers with a weight of 10% showed better antibacterial activity in water and airborne tests than the copolymers. However, it has been shown that the inadequate anti‐biofilm properties of homopolymer‐containing paint films are overcome with the VPBA content of the copolymer structure and the most effective antibacterial and anti‐biofilm properties have been obtained with paint films containing P(VPBA‐co‐5QDMAEMA) copolymers. These paint films, which can maintain antibacterial and anti‐biofilm properties for at least 1 year, have the potential to be an alternative to Ag/Cl based solid surfaces which require the active substance to be regenerated. © 2018 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2018 , 135, 46245. 相似文献
12.
Zeynep Karahaliloğlu Murat Demirbilek Mesut Şam Melike Erol‐Demirbilek Necdet Sağlam Emir Baki Denkbaş 《应用聚合物科学杂志》2013,128(3):1904-1912
The design and the development of novel scaffold materials for tissue engineering have attracted much interest in recent years. Especially, the prepared nanofibrillar scaffold materials from biocompatible and biodegradable polymers by electrospinning are promising materials to be used in biomedical applications. In this study, we propose to produce low‐cost and cell‐friendly bacterial electrospun PHB polymeric scaffolds by using Alcaligenes eutrophus DSM 545 strain to PHB production. The produced PHB was characterized by Nuclear Magnetic Resonance (NMR) and Fourier Transform Infrared Spectroscopy (FTIR). Nanofibrous scaffolds were fabricated via electrospinning method that has a fiber diameter approximately 700–800 nm. To investigate cell attachment, cell growth, and antioxidant enzyme activity on positively and negatively charged PHB scaffold, PHB surface was modified by plasma polymerization technique using polyethylene glycol (PEG) and ethylenediamine (EDA). According to the results of superoxide dismutase (SOD) activity study, PEG‐modified nanofibrillar scaffolds indicated more cellular resistance against oxidative stress compared to the EDA modification. As can be seen in cell proliferation results, EDA modification enhanced the cell proliferation more than PEG modification, while PEG modification is better as compared with nonmodified scaffolds. In general, through plasma polymerization technique, surface modified nanofibrillar structures are effective substrates for cell attachment and outgrowth. © 2012 Wiley Periodicals, Inc. J. Appl. Polym. Sci., 2013 相似文献
13.
The phase behavior and volumetric properties of polyethylene (PE) in solutions of n‐pentane and n‐pentane/CO2 were studied in a temperature (T) range of 370–440 K at pressures up to 60 MPa. Measurements were conducted with a variable‐volume view‐cell system equipped with optical sensors to monitor the changes in the transmitted light intensity as the P or the T of the system was changed. Lower‐critical‐solution‐temperature‐type behavior was observed for all of the liquid–liquid (L–L) phase boundaries, which shifted to higher pressures in solutions containing CO2. The solid–fluid (S–F) phase boundaries were investigated over a P range of 8–54 MPa and took place in a narrow T range, from 374 to 378 K in this P interval. The S–F phase boundary showed a unique feature in that the demixing temperatures showed both increasing and decreasing trends with P depending on the P range. This was observed in both the PE/n‐pentane and PE/n‐pentane/CO2 mixtures. The density of these solutions were measured as a function of P at selected temperatures or as a function of T at selected pressures that corresponded to the paths followed in approaching the phase boundaries (S–F or L–L) starting from a homogeneous one‐phase condition. The data showed a smooth variation of the overall mixture density along these paths. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 89: 2201–2209, 2003 相似文献
14.
Ayse Altin Burcin Akgun Ozlem Buyukgumus Zeynep Sarayli Bilgici Sesil Agopcan Didar Asik Havva Yagci Acar Duygu Avci 《Reactive and Functional Polymers》2013,73(9):1319-1326
An urea methacrylate (1) and two phosphonated methacrylates (2–3) were synthesized from 2-isocyanatoethyl methacrylate (IEM) and benzyl amine (1), diethyl aminomethylphosphonate (2) and diethyl amino(phenyl)methylphosphonate (3). Their photopolymerization rates are notably higher than commercial monomers, despite the presence of only one double bond. Their polymerization rates follow the order 1 ~ 2 > 3 ~ triethylene glycol dimethacrylate (TEGDMA) > 2-hydroxyethyl methacrylate (HEMA). A tendency toward high crosslinking density during thermal bulk polymerizations, low oxygen sensitivity and high conversions with benzophenone during photopolymerization indicated the importance of hydrogen abstraction/chain transfer reactions. It was found that the addition of the monomers to HEMA significantly increased its polymerization rate, proving their utility as replacements for TEGDMA as reactive diluents for 2,2-bis[4-(2-hydroxy-3-methacryloyloxy propyloxy) phenyl] propane (Bis-GMA). Copolymer systems containing 2 and 3 showed improved Tg values compared to Bis-GMA/TEGDMA systems. 相似文献
15.
Amanda M. Levy Paulino Gomez-Puertas Zeynep Tümer 《International journal of molecular sciences》2022,23(8)
The postsynaptic density (PSD) is a massive protein complex, critical for synaptic strength and plasticity in excitatory neurons. Here, the scaffolding protein PSD-95 plays a crucial role as it organizes key PSD components essential for synaptic signaling, development, and survival. Recently, variants in DLG4 encoding PSD-95 were found to cause a neurodevelopmental disorder with a variety of clinical features including intellectual disability, developmental delay, and epilepsy. Genetic variants in several of the interaction partners of PSD-95 are associated with similar phenotypes, suggesting that deficient PSD-95 may affect the interaction partners, explaining the overlapping symptoms. Here, we review the transmembrane interaction partners of PSD-95 and their association with neurodevelopmental disorders. We assess how the structural changes induced by DLG4 missense variants may disrupt or alter such protein–protein interactions, and we argue that the pathological effect of DLG4 variants is, at least partly, exerted indirectly through interaction partners of PSD-95. This review presents a direction for functional studies to elucidate the pathogenic mechanism of deficient PSD-95, providing clues for therapeutic strategies. 相似文献
16.
Zeynep Duymus Yesil Serpil Karaoglanoglu M. Samil Akyıl Nilgün Seven 《International Journal of Adhesion and Adhesives》2009,29(1):32-35
This study was carried out with the purpose of testing the bond strength of different bonding agents bonded to different substrates.Substrates consisted of cylindrical specimens of three different materials: porcelain, metal, and a porcelain–metal combination. Specimens were all 10 mm in diameter and 4 mm thick. Surfaces to be bonded were air-abraded with Al2O3 and cleaned ultrasonically in distilled water for 10 min. After the preparation of the surface was complete, three different bonding agents were applied to the central region of the substrates. Composite resin of a 3.5 mm diameter and 2 mm thick was applied. All specimens were thermocycled between 5 and 55 °C for 200 cycles with a 30-s dwell time. After thermocycling, specimens were stored at 37 °C in distilled water for an additional 7 days before being subjected to a shear load. Shear testing was conducted Hounsfield test machine.The univariate analysis of variance and the Duncan multiple comparison test were used for statistical assessment. It was found that both type of bonding agents and of substrate led to statistically significant differences in bond strength (p<0.01).It was found that the highest bond strength was produced by Clearfil and on pure alloy substrate (33.36 MPa) and the lowest bond strength in Single Bond and porcelain–alloy substrate (4.25 MPa). 相似文献
17.
Cem Sensogut Murat Ozalp Huseyin Yesil 《International Journal of Adhesion and Adhesives》2009,29(5):589-592
In this study, the effects of borax pentahydrate addition to urea formaldehyde (UF) on the bonding characteristics and free formaldehyde content have been studied. Experiments related to the bending strength, withdrawal shear strength and free formaldehyde content have been conducted on the three-layered beech and poplar plywood which are prepared by the addition of borax pentahydrate into their adhesive mixtures in certain amounts. Addition of borax pentahydrate into the adhesive mixture did not statistically affect the bending strength and withdrawal shear strength of the plywood but did reduce the free formaldehyde content. 相似文献
18.
Mohammed Saleh Zeynep Bilici Merve Kaya Mutlu Yalvac Hudaverdi Arslan H. Cengiz Yatmaz Nadir Dizge 《Advanced Powder Technology》2021,32(4):1264-1275
The use of naturally present heterogeneous catalysts has recently been an essential issue in the Fenton and photo-Fenton processes. In this study, the uses of basalt as a catalyst for the Fenton and photo-Fenton reactions for methylene Blue (MB) and Basic Red 18 (BR18) degradations were investigated. Basalt was selected because of the presence of the iron (III) oxide in the structure. Basalt was characterized by X-Ray Fluorescence (XRF) and X-Ray Diffraction (XRD) analysis to obtain the chemical composition and the crystalline phase. The surface charge and the surface area were obtained by zeta potential and Brunauer Emmett-Teller (BET) analysis. Fourier Transform Infrared Spectroscopy (FTIR) and scanning electron microscope (SEM) were utilized to explore the functional group and the surface morphology. Fenton and photo-Fenton processes were applied to explore the best degradation method. Adsorption was also tested and the adsorption process had minimum removal efficiency (12% for MB and 17% for BR18). The removal efficiencies for MB and BR18 by the Fenton process were 87% and 28%, respectively. The photo-Fenton process had maximum removal efficiency with 100% for MB and 70% for BR18. The optimum conditions were 70 mg/L dye concentration, 5 mM H2O2, 1.0 g/L basalt loading and pH 2. Basalt has shown reuse capability as a catalyst for three consecutive cycles. 相似文献
19.
Zeynep Atamer Jochen Dietrich Horst Neve Knut J. Heller Jörg Hinrichs 《International Dairy Journal》2010,20(6):408-414
The thermal resistances of the Lactococcus lactis phages P008 (a heat-sensitive wide-spread phage) and P680 (a heat-resistant phage) suspended in milk and in solutions supplemented with milk components were studied to elucidate the protective role of milk on phage inactivation. For both phages a decrease of inactivation was observed in casein solution. Furthermore, the inactivation kinetics of the phages in whey, in whey cream (3.5%, 20%, 30% fat) and in whey protein concentrate (0.7%, 5%, 10% protein) were tested. The inactivation experiments in whey cream and in whey protein concentrate having different concentrations of fat and protein revealed that fat had no influence on the inactivation, while, in contrast, the presence of protein had a protective effect. 相似文献
20.
Abdullah Yesil Shahram Minaei 《International Journal of Circuit Theory and Applications》2020,48(11):2023-2038
In this paper, two new complementary metal oxide semiconductor (CMOS) realizations for second-generation voltage conveyor (VCII) are presented. The first proposed VCII has a very simple structure employing only six transistors. The second proposed VCII employs 11 transistors, and none of the transistors at both proposed circuits suffer from the body effect. Small-signal analysis, parasitic elements, and input-referred noise of the proposed VCIIs are given. Moreover, a new active element called voltage controlled second-generation voltage conveyor (VC-VCII) is proposed as dual element of current controlled second-generation current conveyor (CCCII) active element. Its parasitic resistance at the Y terminal can be controlled electronically. Two presented CMOS structures of VCII are worked as VC-VCII with slight modification. Proposed circuits are simulated in Cadence Analog environment using TSMC 0.18-μm process parameters with ±0.9-V supply voltages. Both CMOS structures occupy a small chip area of 276.8 and 271 μm2, respectively. The bandwidth of the current follower stage of the proposed VCIIs is found as 794 MHz, whereas the bandwidth of the voltage follower stage for the first and second proposed VCIIs is found as 2.57 and 1.92 GHz, respectively. As an application example, voltage-mode first-order low-pass filter has been given with its tunable gain by using VC-VCII. 相似文献