聚合物载体－稀土金属络合物的研究 ⅩⅢ．聚［苯乙烯－甲基丙烯酸β（甲基亚硫酰基）乙酯］的结构与其稀土金属络合物催化丁二烯聚合的活性

从测得的竞聚率计算了单体链节在聚［苯乙烯－甲基丙烯酸β（甲基亚硫酰基）乙酯］（ＰＳＭ）中的序列分布。苯乙烯（Ｓ）或甲基丙烯酸β（甲基亚硫酰基）乙酯（Ｍ）的长序列的概率随着ＰＳＭ中相应单体含量的增加而增加。对于Ｓ和Ｍ摩尔分数大致相等的ＰＳＭ，单体链节的长序列分布函数值相接近。用与此结构相近的ＰＳＭ合成的稀土金属络合物，其催化活性不佳。在Ｍ短序列分布和Ｓ长序列分布较高的情况下，络合物的催化活性最好。所得聚丁二烯的微观结构与ＰＳＭ中单体单元的分布无关。     

Variation of the creep limit and structure of a welded joint in PT-3V titanium alloy under the effect of cyclic loading. Report 2

Comparative analysis of the characteristics of amplitude-dependent internal friction (IF) was carried out to explain reasons leading to an increase of the creep limit of the butt welded joint in PT-3V titanium alloy (PT-2V filler material) after cyclic loading. IF was measured by the method of the direct torsional pendulum on cylindrical specimens representing the gage part of the specimens subjected to preliminary cyclic loading. The data were processed using the Granato-Lucke theory. The results show that the reduction of IF after cyclic loading took place as a result of an increase of the number and redistribution of pinning points of the dislocations. Consequently, the density of mobile dislocations decreases by 8% and the length of dislocation segments by 18%. These processes of stabilization of the structure were completed within 5·10 ⁴ cycles of preliminary loading. Stabilization of the dislocation structure of the material of the welded joint increases its creep limit.Translated from Problemy Prochnosti, No. 4, pp. 35–40, April, 1996.     

国外新型干燥设备及其技术

干燥装置是一类重要的化工设备。本文概要介绍国外开发的新型干燥设备及其原理、特点、应用。     

压型钢板组合楼板承载力的有限元分析

压型钢板组合楼板是 2 0世纪发展起来的一种新型结构形式。它具有显著的优势 ,如轻质、高强 ,施工快捷等 ,将在未来的建筑领域中大有作为。组合楼板的承载力主要取决于钢板 -混凝土界面处的抗剪强度。建立了一个二维有限元模型来研究单向组合板的性能。并将计算结果与试验数据进行对比 ,验证了模型的有效性     

COATES GRAPH APPROACH FOR GENERATING SYMBOLIC NETWORK FUNCTION

In this paper, symbolic code matrix ,constant matrix and count matrix are defined .The first twomatrices are used to describe the elemental expression of augmented matrix and the nede admittance equa-tion is thus obtained. The third matrix is used to obtain the incoming degree matrix, and according to thematrix all the 1- factors of the Coates graph are given. By using the data code, the determinant is expandedand the same items in the expansion are merged. Thus the symbolic network function in which no term can-cellation occurs is generated.     

On the construction of the reachability domain in one nonlinear problem

An algorithm for construction of the reachability domain by the given time instant ? for a nonlinear third order system under the condition of preliminary approach to a predefined point is proposed. All possible cases of location of this point in the motion plane of the system for different values of the time instant ? are studied.     

化肥厂合成气及重整氢真空变压吸附制取高纯度氢气

从设计、生产操作和经济效益3个方面阐述了以化肥厂合成气及重氢为原料，通过真空变压吸附（VPSA）装置制取高纯度氢的过程。工业应用结果表明，该制氢工艺是一项操作简便灵活，制氢费用较低的工艺路线。VPSA装置技术和设计上的特点能够保证大的操作弹性、高的产品氢纯度和较高的氢气回收率。在36％－51％的低限负荷下，通过适当调整吸附时间，可获得纯度99％的氢气产品，89％－92％的氢气回收率。     

浅谈如何搞好加油站的风险评价

阐述了加油站实施HSE管理，进行加油站风险评价的必要性，介绍了评价方法及其应用范围，评价组织的建立和工作流程及注意事项，指出：进行加油站风险评价，在选择评估方法时应从加油站的生产实际出发，针对不同的区域，采用适当的，可操作的方法；找出身边存在的危害因素，采取适当的措施来控制和化解风险，提高加油站安全管理水平，才能适应加入WTO后所面临的挑战。     

秸杆材料用作草皮栽培基质的研究

本文介绍了秸杆毡的成型工艺 ,通过植物所需的水、肥料和空气三种因素对秸杆毡的化学和物理性能进行了研究 ,该材料可被用作草皮栽培基质     

分析型全蒸发器在啤酒挥发性成分测定中的应用

综述了分型全蒸发器技术在啤酒发酵过程中的应用状况，并介绍了分析型全蒸发器模型结构及与之配合使用的连续多分支管。