Low-Temperature Superplastic Deformation of Cold-Rolled Fe–5.6Mn–1.1Al–0.2C Steel

Metallurgical and Materials Transactions A - A cold-rolled low Al-added medium Mn steel was employed to investigate the low-temperature superplastic deformation at a relatively high initial strain...     

Effect of Heat Treatment on Microstructure and Mechanical Properties of Extruded PM Ti–6Al–4V Alloy With Deformation Flowlines

Metallurgical and Materials Transactions A - Two heat treatments, namely 955°C/2h/AC (AC = air cooling) and 955°C/4h/FC (FC = furnace cooling), were carried out on...     

Characterization of ultrafine La x Sr1−x MnO3 powder prepared by spray pyrolysis

The characterization of La _x Sr_1−x MnO₃ powders produced by spray pyrolysis using scanning electron microscopy (SEM) and transmission electron microscopy (TEM) observation, specific surface area (Brunauer-Emett-Teller), and particle size distribution measurements shows that the resultant large particles are loose agglomerates consisting of many small particles. However, the sintered tiny particles can form hard agglomerates, and the particle size increases remarkably. The structures of the powders before and after sintering were identified by x-ray diffraction (XRD). The study of the electrical property of the powder shows that the powder is a metallic conductor. In a reducing atmosphere, the powder can be decomposed. When the powder is cofired with yttria-stabilized zirconia 5% (YSZ) powder at 1200 °C for 5 h, no new phase is produced, and the powder remains a single provskite hexagonal-rhombohedral structure.     

含硫氰酸盐、硫化物固体废物中总氰化合物测定方法

实验建立了含硫氰酸盐、硫化物固体废物中总氰化合物的测定方法,采用硝酸银滴定法、异烟酸-吡唑啉酮分光光度法分别测定总氰化合物含量高、低的样品。通过条件实验优化了前处理方式、称样量和干扰去除方法。该方法测定结果的相对标准偏差为0.43%～1.33%,加入标准物质回收率为91.5%～101.5%,精密度和准确度良好,符合测定要求。     

含砷氰化尾矿回填利用污染控制技术试验研究

针对某黄金生产企业含砷氰化尾矿污染特征,开展了搅拌洗涤法、臭氧氧化法、酸化溶砷法、铁盐固砷法等多种无害化方法联合处理试验研究,旨在将该含砷氰化尾矿处理至满足氰渣规范回填利用污染控制要求。结果表明：该含砷氰化尾矿回填利用污染控制技术工艺为压滤调浆搅拌洗涤+臭氧氧化+酸化溶砷+铁盐固砷,最佳参数为原矿浆压滤后加水调浆,矿浆浓度40%,臭氧投加量0.66 g/L,酸化溶砷pH值3、曝气量0.1 m³/h、反应时间2 h,铁盐固砷七水合硫酸亚铁投加量20.0 g/L、反应时间1 h。研究结果为该黄金生产企业含砷氰化尾矿回填利用提供了技术支撑。     

GCrl5轴承钢精炼渣对夹杂物祛除行为的研究

通过建立的夹杂物穿越钢渣界面运动模型,研究了精炼渣对夹杂物的吸附现象。结果表明,夹杂物 粒径、表面张力和熔渣粘度是影响夹杂物冲破钢渣界面的重要参数,大型夹杂物中粒径和熔渣粘度起决定作用,而 ≤ 20㎛ 级别的小型夹杂物中仅表面张力起决定作用;大型夹杂物冲破钢渣界面的能力远大于小型夹杂物。针对 小型夹杂物难以吸附的问题,运用了夹杂物运动模型和熔渣、钢液表面张力模型,研究了表面张力对吸附过程的影 响。结果表明,直径≤ 122.9 ㎛尺寸的夹杂物均无法穿越钢渣界面,回弹至钢液一侧,由此得出：无法通过调整精 炼渣用以吸附≤ 122.9 ㎛夹杂物以达到进一步降低钢中氧含量的目的。     

离心铸造汽缸套白斑产生机理

针对离心铸造汽缸套的白斑特征，以模拟试验手段探寻原因。用金属凝固理论解释白斑形成机理。经过装车试用，验证了白斑对摩擦性能的影响。     

添加硫酸锰对化学镀Co-Fe-P合金结构禾口磁性台皂的影响

借助扫描电镜、能谱分析、X射线衍射和振动样品磁强计研究了添加硫酸锰对Co-Fe-P合金沉积速率、结构和磁性能的影响.结果表明,少量的硫酸锰有利于Co-Fe-P镀层的沉积,但过量时会降低沉积速率.当镀液中添加的硫酸锰浓度小于0.02 mol-L-1时对镀层组成几乎没有影响,但随着其浓度进一步增大至0.04 mol·L-1,镀层组成发生显著的变化.硫酸锰对该镀层具有整平作用,而且可使镀层中颗粒细化;硫酸锰有利于镀层形成非晶或微晶态结构.硫酸锰还可以改善Co-Fe-P合金膜的磁性能.     

A NEW ELECTROMAGNETIC IMAGING SCHEME

ＡＮＥＷＥＬＥＣＴＲＯＭＡＧＮＥＴＩＣＩＭＡＧＩＮＧＳＣＨＥＭＥ①ＺｈａｎｇＲｏｎｇｆｅｎｇ，ＨｅＪｉｓｈａｎＣｏｌｅｇｅｏｆＲｅｓｏｕｒｃｅ，ＥｎｖｉｒｏｎｍｅｎｔａｎｄＣｉｖｉｌＥｎｇｉｎｅｒｉｎｇ，ＣｅｎｔｒａｌＳｏｕｔｈＵｎｉｖｅｒｓｉｔｙｏ...