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111.
Andrei Kholkin Anna Morozovska Dmitry Kiselev Igor Bdikin Brian Rodriguez Pingping Wu Alexei Bokov Zuo‐Guang Ye Brahim Dkhil Long‐Qing Chen Marija Kosec Sergei V. Kalinin 《Advanced functional materials》2011,21(11):1977-1987
Relaxor ferroelectrics are a prototypical example of ferroic systems in which interplay between atomic disorder and order parameters gives rise to emergence of unusual properties, including non‐exponential relaxations, memory effects, polarization rotations, and broad spectrum of bias‐ and temperature‐induced phase transitions. Despite more than 40 years of extensive research following the original discovery of ferroelectric relaxors by the Smolensky group, the most basic aspect of these materials – the existence and nature of order parameter – has not been understood thoroughly. Using extensive imaging and spectroscopic studies by variable‐temperature and time resolved piezoresponse force microscopy, we find that the observed mesoscopic behavior is consistent with the presence of two effective order parameters describing dynamic and static parts of polarization, respectively. The static component gives rise to rich spatially ordered systems on the ~100 nm length scales, and are only weakly responsive to electric field. The surface of relaxors undergoes a mesoscopic symmetry breaking leading to the freezing of polarization fluctuations and shift of corresponding transition temperature. 相似文献
112.
113.
Alexei Lisitsa 《Journal of Automated Reasoning》2013,51(4):431-451
In this paper we investigate to what extent a very simple and natural “reachability as deducibility” approach, originating in research on formal methods for security, is applicable to the automated verification of large classes of infinite state and parameterized systems. In this approach the verification of a safety property is reduced to the purely logical problem of finding a countermodel for a first-order formula. This task is delegated then to generic automated finite model building procedures. A finite countermodel, if found, provides with a concise representation for a system invariant sufficient to establish the safety. In this paper we first present a detailed case study on the verification of a parameterized mutual exclusion protocol. Further we establish the relative completeness of the finite countermodel finding method (FCM) for a class of parameterized linear arrays of finite automata with respect to known methods based on monotonic abstraction and symbolic backward reachability. The practical efficiency of the method is illustrated on a set of verification problems taken from the literature using Mace4 model finding procedure. 相似文献
114.
Tian‐Long Zhao Alexei A. Bokov Jingen Wu Hongli Wang Chun‐Ming Wang Yang Yu Chun‐Lei Wang Kaiyang Zeng Zuo‐Guang Ye Shuxiang Dong 《Advanced functional materials》2019,29(12)
Here, novel ferroelectric ceramics of (0.95 ? x)BiScO3‐xPbTiO3‐0.05Pb(Sn1/3Nb2/3)O3 (BS‐xPT‐PSN) of complex perovskite structure are reported with compositions near the morphotropic phase boundary (MPB), and which exhibit a piezoelectric coefficient d33 = 555 pC N?1, a large‐signal coefficient ≈ 1200 pm V?1 at room temperature, and a high Curie temperature TC of 408 °C. More interestingly, this ternary system exhibits a giant and stable piezoelectric response at 200 °C with a large‐signal ≈ 2500 pm V?1, matching that of the costly relaxor‐based piezoelectric single crystals at room temperature. The mechanisms of such giant piezoelectricity and its characteristic temperature dependence are attributed to the spontaneous polarization rotation and extension under an electric field and the MPB‐related phase transition. The findings reveal that the BS‐xPT‐PSN ceramics constitute a new family of high‐performance piezoelectric materials suitable for electromechanical transducers that can be operated at high temperatures (at 200 °C, or higher). 相似文献
115.
Mario G. Toledo Khriscia S. Utria Freddy A. González Juan P. Zuñiga Alexei V. Saveliev 《International Journal of Hydrogen Energy》2012
Rich and ultrarich combustion of natural gas in a porous medium composed of aleatory coal particles and alumina spheres was studied experimentally to evaluate the suitability of the concept for hydrogen and syngas production. Temperature, velocity and chemical products of the combustion waves were recorded experimentally in two stages: (1) natural gas in an inert porous medium at filtration velocities of 12, 15 and 19 cm/s for equivalence ratios (φ) from φ = 1.0 to φ = 3.8; (2) natural gas in a porous medium composed of coal and alumina particles for a range of volume coal fractions from 0 to 75% at φ = 2.3, and a filtration velocity of 15 cm/s. It was observed that the flame temperatures and hydrogen yields were increased with the increase of filtration velocity in inert porous media. In hybrid porous media the flame temperature decreased with an increase of coal fraction, and hydrogen and carbon monoxide were dominant partial oxidation products. Syngas yield in hybrid filtration combustion was found to be essentially higher than for the inert porous medium case. The maximum hydrogen conversion for the hybrid coal and alumina bed was ∼55% for a volumetric coal content of 75%. 相似文献
116.
Kudryavtsev AN Krasitskaya VV Petunin AI Burakov AY Frank LA 《Analytical chemistry》2012,84(7):3119-3124
Novel dual-analyte single-well bioluminescence immunoassay (BLIA) for total and IgG-bound prolactins was developed on the base of Ca(2+)-regulated photoprotein obelin mutants with altered color and kinetics of bioluminescence signal as reporters. The mutants W92F-H22E and Y138F were chemically conjugated with monoclonal mouse anti-hPRL and anti-hIgG immunoglobulins and thus displayed signals from total prolactin and IgG-bounded prolactin (macroprolactin) correspondingly. Bioluminescence of the reporters was simultaneously triggered by a single injection of Ca(2+) solution and discriminated via bioluminescent signal spectral and time resolution. The developed microplate-based immunoassay allows detection of two prolactin forms in crude serum without additional manipulations (e.g., gel chromatography or PEG-precipitation). Total prolactin bioluminescence immunoassay in standard, control, and clinical sera offers high sensitivity and reproducibility. The BLIA results show good correlation with those obtained by RIA and immunoassay after gel chromatography. 相似文献
117.
The flame synthesis of carbon nanotubes (CNTs) coupled with application of moderate electric fields is studied experimentally as a means to control CNTs growth rates and morphology. The nanotubes are grown on a conductive metal-based catalytic probe positioned at the fuel side of the opposed flow oxy-flame. The probe was connected to an external voltage source to generate radial electric fields on its surface. At low applied voltages (from 0.3 to 2 V), the effect of the electric field on alignment and growth rate enhancement revealed the generation of vertically aligned carbon nanotube (VACNT) arrays with uniform distribution of CNT diameters. Further increases of the applied voltage resulted in structural modifications of the generated nanotubes. In particular, helically coiled CNTs were observed at applied voltages of 3 V. At higher voltages the arrays contained multi-walled CNTs with fascinating modified morphologies such as Y, T, and multi-junction patterns. Analysis of the samples generated at applied voltage of 5 V showed the presence of particle sprouting and early CNT junctions in the form of small bumps extruding from the outer surface of the CNTs. Analysis of material samples synthesized at 12 and 25 V showed the presence of fully branched CNT structures. 相似文献
118.
Fiber-optic photoacoustic sources for nondestructive testing and biomedical applications are described. The photoacoustic sources consist of a pulsed laser, a fiber-optic cable, and a generation head. The generation head is a miniature hermetically sealed chamber, which can be embedded into solid structures or immersed in liquid media. The face of the chamber acts as a target for laser irradiation. Bulk ultrasonic waves generated inside of the target are transmitted into the medium. The proposed systems offer wide ultrasonic range (0.5-15 MHz), easy control over directivity of the ultrasonic beam, high efficiency of generation, and the ability to operate in a harsh environment. Sources with different radiation patterns with respect to the optical axis of the fiber, such as normal, sideways, as well as focused, have been devised. We present a proof-of-concept experiment using these sources in combination with fiber-optic ultrasonic receivers. 相似文献
119.
The results of numerical simulation of inelastic scattering by microspheres with the use of a dipole model are presented. The formulas that are derived speed up the computation, thereby permitting larger-sized microspheres to be studied. The angular scattering cross section and depolarization are calculated for a wide range of size parameters as well as for different orientations of incident wave polarization. Calculations performed with small incremental changes in size permit the influence of morphology-dependent resonance (MDR) on the power and angular distribution of scattered radiation to be studied. TM and TE types of MDR produce enhanced scattering of the incident wave with vertical and horizontal polarization; the corresponding shape of the phase function becomes oscillatory. Special attention is paid to the simulation of backward scattering by water droplets, which is important for Raman lidar applications. 相似文献
120.
Simulation of high-resolution x-ray zone plates 总被引:1,自引:0,他引:1
Kurokhtin AN Popov AV 《Journal of the Optical Society of America. A, Optics, image science, and vision》2002,19(2):315-324
A full-wave approach to quantitative characterization of x-ray zone plate lenses is proposed. Distributed focusing efficiency eta(z) of a multifocus optical element is defined as the energy flux through the Airy disk of a reference perfect lens with variable focal length z. Maxima of this function characterize diffraction efficiencies and spatial resolution of the zone plate foci. The parabolic wave equation is used to take into account diffraction effects inside the optical element. Rough and fuzzy interface models are introduced to describe realistic zone profiles. Numerical simulation reveals the limited capability of zone width reduction to improve the zone plate imaging performance. The possibilities of second-order focus enhancement by optimization of the zone plate thickness, line-to-space ratio, and zone tilt are studied numerically. 相似文献