介质黏度对离心泵性能的影响

为了获得介质黏度对离心泵性能的影响规律,采用CFD方法对输送3种不同黏度介质的同一台离心泵进行了数值模拟.外特性结果分析表明,清水介质下扬程及效率实验和模拟结果之间的偏差随流量的增大而减小;不同黏度介质下离心泵的外特性曲线的趋势基本一致,即随着介质黏度的增大,效率下降,扬程减小,功率增大;不同黏度下功率换算系数Kp>1,流量换算系数Kq<1,扬程换算系数Kh<1,效率换算系数Kη<1.泵内部静压分析表明,随着介质黏度增大,泵进出口压差减小,泵内流动损失增大.     

SiCp/2024铝基复合材料的超塑性变形行为研究

对经过热处理和冷轧后的体积分数为17％，尺寸为3．5μm的SiC颗粒增强2024铝合金薄板在753－853K范围内进行了超塑性实验研究. 结果在813K时以10^-1/S的变形速率下获得了259％的最大延伸率，最大应力敏感系数为0．25复合材料的变形激活能值在753－793K范围内为144kJ/mol，在813－853K内为202kJ/mol，接近纯铝的晶格扩散激活能值142kJ/mol。复合材料的变形机制主要为基体晶粒滑动机制。     

Magnetic and mechanical properties of FeSi alloys with high Si content

The chemical vapor（CVD） deposition-diffusion method was applied to prepare FeSi alloys with high silicon content up to 6.5%. In spite of various deposition and post-annealing, the sample remains α-Fe bcc structure. The cross section of the composition was analyzed to evaluate the Si content and distribution before and after annealing. The results show that the soft magnetic properties are improved by increasing the silicon content. For the samples containing about 6.5% Si, the coercivity decreases to 60 from 237.3 A/m of the original. It is also obtained that, in addition to the Si content, Si distribution has a large influence on the core loss due to the effect of resistivity. The micro-hardnesses were also evaluated along the cross-section after various annealings.     

喷射共沉积SiCp／6066A1复合材料的组织性能增强颗粒捕获机制

研究了喷射共沉积SiCp/6066Al基复合材料增强颗粒的捕获机制，以及复合材料在加工过程中组织、性能的变化。结果表明：喷射沉积过程中，平均粒度为10μm的SiCp颗粒基本上可以被6066铝合金完全捕获；复合材料平行挤压方向轧制的致密度和强度高于垂直挤压方向轧制的，平行轧向的强度高于垂直轧向的。     

Synthesis and electrochemical properties of Th-doped LiMn2O4 powders for lithium-ion batteries

To improve the cycle performance of eco-friendly and cost-effective spinel LiMN2O4 as the Li secondary batteries, the Th-doped LiThxMn1-xO4 spinel powers were synthesized by solid-state method. The starting materials, Li2CO3,MnO2 and Th(NO3)4·4H2O, were mixed uniformly using a traditional ball milling, which resulted in a uniform particle size distribution in the mixed powers. Tests of X-ray diffraction, SEM, impedance spectra and charge-discharge were carried out for LiThxMn1-xO4 cathode materials. Results show that the synthesized LiTh0.01Mn1.99O4 material exhibits standard spinel structure, regular particle morphology and excellent property of charge-discharge for big current. The capacity retention of the material modified by doping Th is more than 85.1% of the first discharge specific capacity of 111.5 mAh·g -1 after 20 cycles at the current rate 1C, while the pristine LiMN2O4 is only 57% of the first discharge specific capacity of 110.2 mAh·g-1 after the same cycles at the same current rate.     

下喷式环流反应器环隙气含率影响因素

下喷式环流反应器是一种用于强化气-液两相反应过程的新型装置，虽然已在工业上有了较广泛的应用，但对其理论研究远未成熟，其工业装置的设计仍依赖于实验和经验。本文借助实验室自制实验装置，对下喷式环流反应器环隙气含率的影响规律进行了研究。首先，对喷射器的吸气量进行了测量，获得了不同条件下喷射器最大吸气量的性能曲线；在此基础上，分别研究了气相流量、液相流量以及喷射器安装位置对环隙气含率的影响规律。结果表明：气相流量和液相流量对气含率具有重要的影响，随着气相流量和液相流量的增大，气含率快速提高，而喷嘴位置对气含率的影响相对较小；考虑到增加气相流量和液相流量所需要的能耗和设备代价，通过增加液相流量来达到提高气含率的目的是优选方案。     

长春新碱治疗糖尿病肾病大鼠的实验研究

目的验证长春新碱对糖尿病肾病大鼠的治疗作用。方法用链脲佐菌素(STZ)诱导大鼠糖尿病模型。将模型大鼠分为治疗组与非治疗组,治疗组给予长春新碱(VCR)0.2 mg/kg,尾静脉注射,每周2次,观察给药后大鼠血糖、尿蛋白、肾功能、肾重,体重等值的改变以及肾脏病理的改善情况。结果 治疗组大鼠尿蛋白明显减少,肾重/体重低于非治疗组。光镜下观察治疗组肾脏病理学变化情况有明显改善。结论长春新碱可降低糖尿病肾病大鼠的尿蛋白并改善糖尿病肾病早期病理损害。     

亚磷酸工业生产方法的研究

本文详细介绍了亚磷酸的合成方法和工艺流程,其中还介绍了优级亚磷酸中杂质的去除方法.     

高炉下部的液泛和流态化

为了阐明高炉下部是否会发生液泛,模拟高炉滴落带的流动条件进行了气液两相逆流的流体力学实验.将Sherwood液泛图纵坐标的液泛因子乘以密度校正系数解决了密度对液泛速度的影响,并提出了新的液泛图和关联式.新关联方法与实验数据吻合很好.通过比较流化速度和液泛速度大小,提出了在一定流动条件下用来区分液泛和流态化的简图.结果表明,高炉滴落区发生渣的液泛,而不是焦炭床的流态化.