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991.
郑立霞 《武汉理工大学学报(材料科学英文版)》2009,24(3):415-417
The deformation resistance effect of polyacrylonitrile (PAN)-based carbon fibers was investigated, and the variatipn law of
electrical resistivity under tensile stress was analyzed. The results show that the gauge factor (fractional change in resistance
per unit strain) of PAN-based carbon fibers is 1.38, which is lower than that of the commonly-used resistance strain gauge.
These may due to that the electrical resistivity of carbon fibers decreases under tensile stress. In addition when the carbon
fibers are stretched, the change of its resistance is caused by fiber physical dimension and the change of electric resistivity,
and mainly caused by the change of physical dimension. The mechanical properties of carbon fiber monofilament were also measured.
Funded by the National Natural Science Foundation of China (No. 10672128 and 50878170) 相似文献
992.
王智宇 《武汉理工大学学报(材料科学英文版)》2009,24(5):698-701
A simple sonochemical route for the surface coating of titanium dioxide on cadmium sulfide nanocrystal was reported. After
2 h ultrasonic irradiation treatment, the mixture of CdS nanocrystals and tetrabutyl titanate in an aqueous medium yielded
CdS/TiO2 nanocrystals composites with core/shell structure. The thickness of TiO2 layer with smooth interface could be easily controlled via changing the concentration of the precursors and the time of irradiation.
The core/shell nanocrysrals were characterized by X-ray diffraction, transmission electron microscope and UV-vis spectrometry
techniques. The prepared semiconductor composites with particular band structure present appealing properties especially in
photochemical activity. 相似文献
993.
何庆复 《武汉理工大学学报(材料科学英文版)》2009,24(3):428-431
Behaviour of hardening and serration yield of a Fe-Ni-Cr alloy under isothermal cycling (ISC) and out-phase TMF was studied
on the basis of varied hysteresis loops. Cycling hardening and serrated yielding for ISC depend on the temperature and the
total strain range, stronger hardening with serrated yielding at higher strain range under ISC at 600 °C, but no hardening
and serrated yielding occurred under ISC at 800 °C. Stronger hardening with stress serration occurred at the thermal path
going to the lowest temperature, no stress serration occurred at the highest temperature under the out-phase. The hardening
also depends on the total strain range, higher total strain range with lower cycling temperature resulted in a stronger hardening
and remarkable serration yielding behavior. Weaker hardening without serrated yielding occurred at near 800 °C may due to
an obvious cycling stress drop under out-phase TMF. Change in the shape of the hysteresis loops also expresses the degree
of the damage of the tested alloy under out-phase and ISC. 相似文献
994.
章桥新 《武汉理工大学学报(材料科学英文版)》2009,24(6):871-874
Silver powder was fabricated by spray pyrolysis, using 2%–20% AgNO3 solution, 336–500 mL/h flux of AgNO3 solution, 0.28–0.32 MPa flux of carrier gas and in the 620–820 °C temperature range. The effects of furnace set temperature,
concentration of AgNO3 aqueous solution, flux of AgNO3 aqueous solution as well as carrier gas on the morphology and particle size distribution of silver powder, were investigated.
The experimental results showed that with the high concentration of AgNO3 aqueous solution, the average grain size of silver decreased with the increasing of furnace set temperature. But the gain
size distribution was not homogenous, the discontinuous grain growth occurred. With the low concentration of AgNO3 aqueous solution, the higher furnace set temperature made the nano sliver grains sintered together to grow. Nano silver powder
about 100 nm was fabricated by spray pyrolysis, using 2wt% AgNO3 solutions, 336 mL/h flux of AgNO3 aqueous solution, 0.32 MPa flux of carrier gas at 720 °C furnace set temperature. 相似文献
995.
贺海燕 《武汉理工大学学报(材料科学英文版)》2009,24(3):359-362
Fatigue-free Bi3.2La0.8Ti3O12 ferroelectric thin films were successfully prepared on p-Si (100) substrates using metalorganic solution deposition process. The orientation and formation of 5-layers thin films
were studied under different processing conditions using XRD. Experimental results indicate that increase in annealing time
at 700 °C after preannealing for 10 min at 400 °C can remarkably increase (200)-orientation of the films derived from the
precursor solutions with two contents of citric acid. Meanwhile, high content of citric acid increases the film thickness
and is conducive to the a-orientation of the films with the preannealing, and low concentration of the solution is conducive to the c-orientation of
the films without the preannealing. 相似文献
996.
A series of dimer acid-based polyamides were synthesized by melt-polycondensation of dimer acid and various aromatic diamines,
and were characterized by Fourier transform infrared spectrum (FT-IR) and nuclear magnetic resonance (1H NMR). The physical properties of the polyamides, such as glass transition temperature, melting temperature, decomposition
temperature and mechanical properties were also investigated. The polyamides’ intrinsic viscosity ranges from 1.8 dL·g−1 to 2.2 dL·g−1, and the melting temperature ranges from 140 °C to 181 °C. The glass transition temperatures, observed from dynamic mechanical
analysis, fall in the range of 34.8–48.2 °C. The physical and mechanical properties of the resultant polyamides are similar
to those of the PA1212. The heat resistance and mechanical properties of poly (4, 4′-diphenylsulfone dimeramide) (PSD) and
poly(4, 4′-diphenyl dimeramide) (PPDI) are comparable to those of PA1212. 相似文献
997.
The catalysts of air electrode were prepared by sintering the active carbon loaded with manganese nitrate and potassium permanganate
at 360 °C The air electrode was made up of a catalyst layer, a waterproof and gas-permeable layer, a current collecting substrate
and a second waterproof and gas-permeable layer. The cell was assembled by the air electrode, pure magnesium anode and 10%
NaCl solution used as electrolyte. The microstructures of air electrodes before and after discharging were characterized by
SEM. The electrochemical behaviors of the air electrodes were determined by means of polarization curves, volt-ampere curves
and constant current discharge curves. The polarization voltage of air electrode is—173 mV (vs SCE) at the current density of 50 mA/cm2. The air electrodes exhibits good activity and stability in neutral electrolyte. The magnesium-air cell could work at 5 W
for more than 7 h. 相似文献
998.
MA制备GdSiGeDy合金系室温磁制冷性能研究 总被引:1,自引:0,他引:1
机械合金化(MA)是一种材料固态非平衡加工新技术.本文主要探讨稀土元素Dy在机械合金化工艺条件下对磁制冷合金GdSiGe磁熵变的影响,发现用机械合金化制备的GdSiGeDy合金系室温磁制冷材料不仅有光滑的磁熵变曲线,而且研究表明,由于元素Dy的加入在磁熵变达到单质Gd的两倍情况下大量减少使用昂贵元素Ge的结果,具有明显经济效益. 相似文献
999.
ZHANG Chuan-xiang DUAN Yu-ling XING Bao-lin ZHAN Liang QIAO Wen-ming LING Li-cheng 《中国矿业大学学报(英文版)》2009,19(3):295-299
Nitrogen-containing carbons were prepared by modification of activated carbons. The modified carbons were used as electrode materials with improved electrochemical performance. Precursor anthracite was activated by KOH (KOH: anthracite= 1:1), modified by melamine or urea and then treated at 1173 K to obtain the modified carbons. The porous structure, the chemical composition and the electrochemical characteristics of the carbons were investigated by nitrogen sorption, XPS and electrochemical methods respectively. Electrochemical experiments were performed in an organic electrolytic solution of 1 M (C2H5)4NBF4/PC.The samples modified by the different methods showed differences in chemical composition that introduced varying degrees of electrochemical performance enhancement. The presence of nitrogen enhanced the electron donor properties and the surface wettability of the activated carbons: this ensured a sufficient utilization of the exposed surface for charge storage. 相似文献
1000.
SHEN Zhong-yan XIAO An-chen CHEN Zhi-yong DING Wei-xing CHEN Han-lin WANG Liang 《中国矿业大学学报(英文版)》2009,19(1):108-114
The Late Cretaceous tectonic upheaval was an important event during the evolution of the Qaidam Basin, resulting in the omission of the Upper Cretaceous in the whole basin and unconformities between the Paleogene sequence and pre-K2 strata. Inte-grating geological and geophysical data, two different groups of Late Cretaceous faults were recognized in the study area, one group consisting of E-W extending strike-slip faults (e.g., the Maxian and Yema-Jinan faults in the Mahai area, which caused an E-W omission zone of Mesozoic), while the other one has NW-SE thrust faults, resulting in NW-SE fold-and-thrust belts. Consid-ering the different strikes and scale of these two groups, a simple-shear model has been employed to explain this structural phe-nomenon. The NW-SE thrust faults were thought to be subsidiary to the E-W strike-slip faults. Putting this into the framework of the Cretaceous paleogeographic environment of central Asia, it is inferred that this tectonic event of the Qaidam Basin is a response to the continuous northward drifting of the India plate. 相似文献