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Methylated-β-cyclodextrin (Me-β-CD) was used to complex the photoinitiator, 2,2-dimethoxy-2-phenyl acetophenone (DMPA), yielding a water-soluble host/guest complex. The comparative studies demonstrated that the Me-β-CD complexed DMPA exhibited a high photoreactivity identical to the uncomplexed DMPA, while the CD complex obviously influenced the products of primary photolysis of DMPA and the photopolymerization kinetics due to the steric effect of CD on the subsequent initiation reactions. The photopolymerization rate of acrylamide can be described by the equation: Rp=K[2a]0.62[M]1.37[I]0.5[Me-β-CD]0. The mechanism of polymerization was also discussed. 相似文献
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Stress analysis of spontaneous Sn whisker growth 总被引:5,自引:0,他引:5
K. N. Tu Chih Chen Albert T. Wu 《Journal of Materials Science: Materials in Electronics》2007,18(1-3):269-281
Spontaneous Sn whisker growth is a surface relief phenomenon of creep, driven by a compressive stress gradient. No externally
applied stress is required for the growth, and the compressive stress is generated within, from the chemical reaction between
Sn and Cu to form the intermetallic compound Cu6Sn5 at room temperature. To obtain the compressive stress gradient, a break of the protective oxide on the Sn surface is required
because the free surface of the break is stress-free. Thus, spontaneous Sn whisker growth is unique that stress relaxation
accompanies stress generation. One of the whisker challenging issues in understanding and in finding effective methods to
prevent spontaneous Sn whisker growth is to develop accelerated tests of whisker growth. Use of electromigration on short
Sn stripes can facilitate this. The stress distribution around the vicinity and the root of a whisker can be obtained by using
the micro-beam X-ray diffraction utilizing synchrotron radiation. A discussion of how to prevent spontaneous Sn whisker growth
by blocking both stress generation and stress relaxation is given. 相似文献
38.
Skim and whole milk powders were manufactured at lab scale by spray freeze drying (SFD), using liquid nitrogen as the cryogen. The polydispersity of droplet/particle sizes was limited using an encapsulator nozzle to atomize the feed. Particle morphology was examined using a scanning electron microscope. Samples were compared with equivalent spray-dried powders in tests of wettability and dissolution in water. The spray freeze-dried powders were found to be highly porous, with a uniform structure of pores throughout the entire particles. When tested in water, SFD skim milk powders wetted roughly three times as fast as industrially spray-dried agglomerated skim milk powders and were observed to dissolve rapidly by breaking down into smaller particles. 相似文献
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Wei Li Zhang Wei Pan Bin Luo Xi Hua Zou Meng Yao Wang 《Photonics Technology Letters, IEEE》2008,20(9):712-714
A theoretical construction of one-to-many (OTM) and many-to-one (MTO) chaos synchronization communications using semiconductor lasers is presented. One center laser provides strong injections (strong link) to other side lasers, and the side lasers also provide weak injections (weak link) to the center one. Simulation results show that the side lasers synchronize with the center laser through injection-locking. In addition, messages transmitted via the strong links or the weak links experience strong chaos pass filtering, enabling us to realize OTM and MTO communications. 相似文献