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91.
92.
Sang Cheol Lee Won Kook Lee 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1992,55(3):251-261
The extraction of penicillin G from simulated media was performed by water/oil/water (w/o/w) emulsion liquid membranes (ELMs) and studied under various operational conditions in a batch system. The degree of extraction achieved was between 80% and 95% under specific conditions. A concentration of greater than nine times the initial concentration of penicillin G in the external phase was obtained in the internal phase. The pH of the internal aqueous solution, containing a basic salt, was theoretically calculated on the basis of the amount of penicillin G transported into the internal phase. The calculated results agreed with the experimental data well and were used to select a suitable type and concentration of a basic salt in the internal phase to give a pH within the range 5 to 8 where penicillin G was stable after the termination of extraction. The extraction of penicillin G was successfully performed by the ELM process with sodium carbonate in the internal phase. 相似文献
93.
94.
In this paper damage propagation during metal forming process is investigated with the concept of continuum damage mechanics. An isotropic damage model based on the theory of materials of type N is adopted to describe the damage process of a ductile material with large elasto-viscoplastic deformation. To solve the finite elasto-viscoplasticity problem, a reasonable kinematic strain measure for largely deformed solids is used and the damage constitutive equations based on thermodynamical framework are developed. The stiffness degradation of the loaded material is chosen as a damage measure. An extended interior penalty method is used to impose the contact condition on the boundary. The highly nonlinear equilibrium equations are reduced to the incremental weak form and approximated by the total Lagrangian finite element method. The displacement control method along with the modified Riks' continuation technique based on displacement parameter is used to solve the incremental iterative equations. As numerical examples, upsetting, backward extrusion and punch problems are simulated and the results of damage propagation and J2 stress contours with and without damage are presented. For punch problems, spring back and residual stresses are also presented. 相似文献
95.
We propose an asymmetric integral imaging method to adjust the resolution and depth of a three‐dimensional image. Our method is obtained by use of two lenticular sheets with different pitches fabricated under the same F/#. The asymmetric integral imaging is the generalized version of integral imaging, including both conventional integral imaging and one‐dimensional integral imaging. We present experimental results to test and verify the performance of our method computationally. 相似文献
96.
Summary Cyclic tris(ethylene terephthalate) (CTET) was separated from oligomeric extract of poly(ethylene terephthalate) by the conventional solvent separation method. The structure of CTET was characterized by differential scanning calorimetry, X-ray diffraction, and scanning electron microscopy. It is shown that the double melting behavior of meltcrystallized CTET is attributed to the morphological change created by heat-treatment. The effect of the morphological change on the crystal structure of CTET was also examined. 相似文献
97.
Experimental investigation of natural convection from a horizontal ice surface melting in pure water
Byung-Ha Kim Seung-Hwan Cho Kap-Jong Riu 《Journal of Mechanical Science and Technology》1991,5(2):93-103
A study on natural convection from a horizontal ice surface melting in pure water was conducted experimentally for the ambient
water temperature from 2▿C to 10°C. Natural convection flow around upward-or downward-facing horizontal ice plate was divided
into three regions according to the temperature variation of ambient water. The flow patterns of three regions were no flow,
two-dimensional steady laminar flow and unsteady flow. Mean Nusselt number for the upward-facing surface had its maximum value
at about 3°C of ambient water temperature. However, in the case of the downward-facing surface it increased as the ambient
water temperature increased. 相似文献
98.
An analog front‐end circuit for ISO/IEC 14443‐compatible radio frequency identification (RFID) interrogators was designed and fabricated by using a 0.25 µm double‐poly CMOS process. The fabricated chip was operated using a 3.3 Volt single‐voltage supply. The results of this work could be provided as reusable IPs in the form of hard or firm IPs for designing single‐chip ISO/IEC 14443‐compatible RFID interrogators. 相似文献
99.
Buhwan Jeong Hyunbo Cho 《The International Journal of Advanced Manufacturing Technology》2006,28(9-10):1006-1011
In order to efficiently and effectively control an overall process in the process industry, a few important parameters should be identified from high-dimensional, non-linear, and correlated data. Feature selection techniques can be employed to extract a subset of process parameters relevant to product quality. The performance of these techniques depends on the precision of the prediction model formulated to quantify the relationship between the process parameters and the quality characteristics. Although the neural network-based partial least squares (NNPLS) method has been proven to be effective in prediction models for the aforementioned industrial process data, feature selection techniques appropriate for NNPLS models have yet to appear. Here, several techniques for scoring the relevance of process parameters to product quality are proposed and validated by applying three datasets. These experiments show that the proposed techniques can discriminate relevant process parameters from irrelevant ones. 相似文献
100.
The deoxidation equilibrium for Al in Ni-Fe alloys was studied in the equilibrium experiments between CaO-Al2O3 slags and Fe-30, 50 and 70 % Ni alloys at 1873 K. By using the values for the first and second order interaction parameters between oxygen and nickel in liquid iron and those between oxygen and iron in liquid nickel, the effect of Ni on the activity coefficient of Al in liquid iron and that of Fe on the activity coefficient of Al in liquid nickel were determined in the whole composition range of Ni-Fe alloys. The oxygen contents in Ni-Fe alloys calculated by the iterative method based on pure iron were in good agreement with those based on pure nickel in the range of [% Al] < 0.03. From this fact, it was found that the Wagner's approximation relating to the multi-component solution was applicable to the deoxidation equilibrium in the whole composition range of Ni-Fe alloys in the restricted concentration of a deoxidizer. 相似文献