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11.
Maurus Biedermann Konrad Grob Dieter Fr?hlich Werner Meier 《Zeitschrift für Lebensmitteluntersuchung und -Forschung A》1992,195(5):409-416
Summary On-line coupled liquid chromatography-gas chromatography-flame ionisation detection (LC-GC-FID) enables efficient and unambiguous determination of irradiation for some fat-containing foods (e.g. meat). Other products, however, contain interfering components or are contaminated, e.g., with mineral oil. Since more selective detection by mass spectrometry has limited success, the determination was improved by a more selective isolation of some key components among the fat degradation products, e.g. the dienes or trienes, by LC-LC-GC-FID. Applications are shown for soup mixes, some spices, fish, and shrimps.
Nachweis der Bestrahlung fetthaltiger Lebensmittel durch direkt gekoppelte LC-GC und LC-LC-GC
Zusammenfassung Die Bestrahlung einiger fetthaltiger Lebensmittel, z. B. Fleisch, kann mit direkt gekoppelter LC-GC-FID rationell und eindeutig nachgewiesen werden. In anderen Proben wird die Analyse aber durch Inhaltsstoffe des Produktes oder durch Verunreinigungen (z. B. mit Mineralöl) gestört. Da selektivere Detektion durch Massenspektrqmetrie wenig verspricht, wurde der Nachweis durch selektivere Isolierung von Schlüsselkomponenten unter den Bestrahlungsprodukten, z. B. der Diene oder Triene, mittels LC-LC-GC yerbessert. Anwendungen werden gezeigt für Suppenpulver, einige Gewürze, Fisch und Garnelen.相似文献
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The time-of-flight method is studied using coincident annihilation gamma rays with an energy of 511 keV to find the distance from a surface at which they are scattered back for detection. The gamma rays have a good penetration ability, which makes the method suitable for industrial circumstances in which the range is rendered opaque to light by flue gas and aerosols. An accuracy of 1 cm over a distance of 2 m can be obtained by increasing the averaging time by the square of the lengthening factor. The density of the surface can be studied by recording the width of the distribution of the surface measurements. This measurement needs a prolonged averaging time, but the thickness of the slag layer on top of a steel melt can be measured with a maximum error of 1.5 cm at short distances, for example 相似文献
14.
A dielectric model comprising band gap transitions and free electron excitations (Drude model) is successfully applied to simulate transmittance spectra of ZnO films doped with 0.5%, 1% and 2% Al. The Drude formula contains a frequency-dependent damping term in order to get a good fit in the visible spectral region. Useful physical parameters obtained from the fit are electron density and mobility within the grains, film thickness, band gap and refractive index. The optically determined film thickness agrees with that obtained with the stylus method within 2%. The optically determined electronic parameters are compared with those obtained by electrical measurements. Contrary to thin In2O3:Sn films, the Drude mobility inside the grains is similar to the direct current Hall mobility indicating more perfect film growth without forming pronounced grain boundaries. Maximum value is 35 cm2/V s. The effective electron mass is estimated to be about 0.6 of the free electron mass. The refractive index at 550 nm decreases with increasing electron density. 相似文献
15.
Dieter Ullmann 《NTM》2006,14(1):1-8
A lot of publications on the acoustics of theatres and churches were published around the turn of the 18th to the 19th century.The
authors were architects who were interested in acoustical problems. Chladni was the first physicist who published on the acoustics
of rooms, he introduced the term “reverberation” into this field. His publications on this subject are reviewed. They have
been the basis for the great progress of room acoustics since 1900.
Zum 250. Geburtstag des Gelehrten 相似文献
Zum 250. Geburtstag des Gelehrten 相似文献
16.
Slab casting for hot rolled steel and strip casting using the twin roll casting (TRC) method are compared in terms of inclusions evolution. There are differences of the processes, mainly the use of casting flux in CC of slabs, or pool shapes and sizes in terms of TRC, particularly when roll diameters vary. The inclusion evolution of alumina in a low carbon steel grade was estimated. By modelling particle growth rate, coagulation and deposition, an ‘agglomeration index’ was created to describe the probability of clogging in the SEN. Similarly the growth of secondary alumina precipitation during cooling of the melt in the pool by Stokes collision and turbulent collision was estimated in terms of forming large particles which are able to float‐up. Influences of melt superheat or caster size were taken into account. 相似文献
17.
Alexander Babich Konstantinos Mavrommatis Dieter Senk Heinrich Wilhelm Gudenau 《国际钢铁研究》2004,75(7):428-432
This contribution deals with advanced educational technologies needed to equip customers from higher education institutions, research and industry with efficient tools supporting their work and operating new skills‐training methods. The challenges are reducing the training costs, improving quality and increasing the number of graduates in engineering departments. The concept of a Virtual Lab based on the combination of various teaching methods and tools is presented. Principles of mathematisation in metallurgical education and training are discussed. An example of online course designed in the form of Virtual Lab is demonstrated. 相似文献
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Chunsheng Lu Robert Danzer Franz Dieter Fischer 《Journal of the American Ceramic Society》2002,85(6):1640-1642
The influence of threshold stress on the estimation of the Weibull statistics is discussed in terms of the Akaike information criterion. Numerical simulations show that, if sample data are limited in number and threshold stress is not too large, the two-parameter Weibull distribution is still a preferred choice. For example, the fit of strength data of glass and ceramics to the two- and three-parameter Weibull distributions is compared. 相似文献
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