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31.
32.
Anthraquinone [1, 2-C] methylisoxazole is synthesized from 2-ethylanthraquinone through nitration and treating with oleum. The different methods of 2-ethylanthraquinone nitrated were discussed. The optimum conditions were determined. The structure of the product was confirmed by MS and 1H NMR. 相似文献
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Qiyong Han Xiaodong Zhang Dong Chen Pengfei Wang 《Metallurgical and Materials Transactions B》1988,19(4):617-622
The equilibrium Ca3P2(s) = 3[Ca] + 2[P] was studied at 1600 ° by equilibrating liquid iron, saturated with Ca3P2, and contained in a TiN crucible, with Ca vapor. The source of Ca was liquid Ca contained in an Mo crucible, and the vapor
pressure of Ca was varied by varying the position of the Mo crucible in the temperature gradient of a vertical tube furnace.
A least-squares analysis of the data gave and. The simultaneous equilibria CaO(s) = [Ca] + [O] and CaS(s) = [Ca] + [S] were studied at 1600 ° by equilibrating liquid iron, contained in a pressed and sintered CaO-CaS crucible with
Ca vapor. The advantage of this technique is that two equilibrium constants,K
cas andK
cao, and two interaction coefficients, and can be determined from one set of experiments. It was determined that, at 1600 °,K
cas = 5.9 × 10−8
K
cao = 5.5 × 10−9,, and.
Formerly Graduate Students 相似文献
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Silicon - In this paper, an analytical model for negative capacitance double gate field effect transistor (NC-DG-FET) is proposed. This model includes interface traps and temperature effects, which... 相似文献
39.
H. B. Wu Z. T. Fan N. Y. Huang X. P. Dong X. F. Tian 《Journal of Materials Engineering and Performance》2005,14(1):132-135
The magnesium (Mg) alloy low-pressure expendable pattern casting (EPC) process is a newly developed casting technique combining
the advantages of both EPC and low-pressure casting. In this article, metal filling and the effect of the flow quantity of
inert gas on the filling rate in the low-pressure EPC process are investigated. The results showed that the molten Mg alloy
filled the mold cavity with a convex front laminar flow and the metal-filling rate increased significantly with increasing
flow quantity when flow quantity was below a critical value. However, once the flow quantity exceeded a critical value, the
filling rate increased slightly. The influence of the flow quantity of inert gas on melt-filling rate reveals that the mold
fill is controlled by flow quantity for a lower filling rate, and, subsequently, controlled by the evaporation of polystyrene
and the evaporation products for higher metal velocity. Meanwhile, the experimental results showed that the melt-filling rate
significantly affected the flow profile, and the filling procedure for the Mg alloy in the low-pressure EPC process. A slower
melt-filling rate could lead to misrun defects, whereas a higher filling rate results in folds, blisters, and porosity. The
optimized filling rate with Mg alloy casting is 140 to 170 mm/s in low-pressure EPC. 相似文献
40.