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271.
The total syntheses of 9(Z),12(E)- and 9(E),12(Z)-octadecadienoic acids have been carried out. A useful intermediate in both
syntheses, 8-bromo-octanoic acid, recently has become available from commercial sources. This compound has been used to expedite
the preparation of these isomers. The remaining carbon atoms were derived from propargyl alcohol along with either 1-heptyne
or acetylene and 1-bromopentane. Because the overall yield for each sequence was roughly 15% and there were no extraordinary
reaction conditions in any of the synthetic steps, the compounds could be prepared readily in multiple gram quantities. The
syntheses of the two compounds were supported by data from a variety of spectroscopic techniques. 相似文献
272.
Alkali-metal carbonate salts meet the requirements for high-temperature solar central receiver systems, but because of their corrosiveness they present special problems in the design of storage tanks. In order to reduce corrosion and temperature sufficiently to retain strength in the storage containing wall, internal and thermal insulation is required. We present design options and operation criteria for sensible-heat, molten-salt storage with internal insulation. 相似文献
273.
Measurements of frequencies and spatial correlations of coherent structures in rod bundle flows 总被引:2,自引:2,他引:0
Cross-wire anemometry was used to identify and characterize coherent flow pulsations in isothermal air flow near the gap regions of a five-rod bundle with a design pitch-to-diameter ratio of 1.149 and contained in a quasi-trapezoidal duct. It was confirmed that such pulsations are quasi-periodic and contribute significantly to the velocity fluctuations across the gap. The frequency of pulsations was found to decrease with diminishing rod–wall gap size in the range between 0.015D and 0.250D, where D is the rod diameter. The pulsations in a rod–wall gap and an adjacent rod–rod gap were strongly coupled and occurred at the same frequency as one rod was displaced towards the duct wall. 相似文献
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G. F. Molokanov 《Journal of Computer and Systems Sciences International》2006,45(2):331-335
The year 2006 marks the ninetieth anniversary of the air navigation (later called navigation) service of the Air Forces of this country. The history of air navigation is investigated, and an opinion about its modern state and directions of further development is presented. 相似文献
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280.
A synthesis procedure for generating current conveyor active filters is presented, and a novel network which realises the general 2nd-order voltage transfer function is given.<> 相似文献